The present invention provides fungicidal 4-substituted-3-{phenyl[(heterocyclylmethoxy)imino]methyl}-1,2,4-oxadiazol-5(4H)-one derivatives of formula (I) [structure] wherein A represents a pyridyl or thiazole group and X1, Y1 to Y5 represent independently different substituents.

Description

446 parts

›CROSS-REFERENCE TO RELATED APPLICATION(S) · 1 of 15

The present application is a 35 U.S.C. §371 national phase conversion of PCT/EP2012/067596 filed on Sep. 10, 2012, which claims priority of European Application No. 11356012.2 filed on Sep. 12, 2011 and U.S. Provisional Application No. 61/545,306 filed on Oct. 10, 2011. Applicants claim priority to each of the foregoing patent applications. The PCT International Application was published in the English language.

The present invention relates to 4-substituted-3-{phenyl[(heterocyclylmethoxy)imino]methyl}-1,2,4-oxadiazol-5(4H)-one derivatives, their process of preparation, their use as fungicide active agents, particularly in the form of fungicide compositions, and methods for the control of phytopathogenic fungi, notably of plants, using these compounds or compositions.

In European patent application no 1184382, there are disclosed certain heterocyclyloxime derivatives of the following chemical structure:

that are excluded from the scope of the present invention.

In world patent application WO2009/130193, there are disclosed certain hydroximoyl-heterocycles derivatives of the following chemical structure:

with

Q is a phenyl ring, L1 a methylene linker and A an heterocycle.

It is always of high-interest in agriculture to use novel pesticide compounds in order to avoid or to control the development of resistant strains to the active ingredients. It is also of high-interest to use novel compounds being more active than those already known, with the aim of decreasing the amounts of active compound to be used, whilst at the same time maintaining effectiveness at least equivalent to the already known compounds. We have now found a new family of compounds which possess the above mentioned effects or advantages.

Accordingly, the present invention provides 4-substituted-3-{phenyl[(heterocyclylmethoxy)imino]methyl}-1,2,4-oxadiazol-5(4H)-one derivatives of formula (I)

wherein

X 1 represents a hydrogen atom, a formyl group, substituted or non-substituted C 1 -C 8 -alkyl, substituted or non-substituted C 3 -C 8 -cycloalkyl, a substituted or non-substituted C 2 -C 8 -alkenyl, substituted or non-substituted C 2 -C 8 -alkynyl, substituted or non-substituted C 1 -C 8 -alkylcarbonyl; A is selected in the list consisting of A 1 and A 2 :

wherein

Z 1 represents a hydrogen atom, a halogen atom, a nitro group, an amino group, an hydroxyamino group, a cyano group, a carboxylic acid group, substituted or non-substituted C 1 -C 8 -alkoxyamino group, substituted or non-substituted C 1 -C 8 -alkylaminosubstituted or non-substituted C 3 -C 10 -cycloalkylamino, substituted or non-substituted C 3 -C 10 -cycloalkenylamino, substituted or non-substituted C 5 -C 12 -fused bicycloalkylamino, substituted or non-substituted C 5 -C 12 -fused bicycloalkenylamino, substituted or non-substituted di-C 1 -C 8 -alkylamino, substituted or non-substituted phenylamino, substituted or non-substituted heterocyclylamino, or a group of formula QC(═U)NR a

wherein

Q represents a hydrogen atom, substituted or non-substituted C 1 -C 8 -alkyl, substituted or non-substituted C 3 -C 8 -cycloalkyl, a substituted or non-substituted C 2 -C 8 -alkenyl, substituted or non-substituted C 3 -C 8 -cycloalkenyl, substituted or non-substituted C 2 -C 8 -alkynyl, substituted or non-substituted C 1 -C 8 -alkoxy, substituted or non-substituted C 2 -C 8 -alkenyloxy, substituted or non-substituted C 2 -C 8 -alkynyloxy, substituted or non-substituted C 1 -C 8 -alkylamino, substituted or non-substituted C 1 -C 8 -alkylsulfenyl, substituted or non-substituted C 2 -C 8 -alkenylsulfenyl, substituted or non-substituted C 2 -C 8 -alkynylsulfenyl, substituted or non-substituted arylsulfenyl, substituted or non-substituted aryl, substituted or non-substituted heterocyclyl, substituted or non-substituted C 5 -C 12 -fused bicycloalkyl, substituted or non-substituted C 5 -C 12 -fused bicycloalkenyl, substituted or non-substituted C 5 -C 12 -benzofused carbocyclyl, substituted or non-substituted C 5 -C 12 -benzofused heterocyclyl, substituted or non-substituted cycloalkoxy; substituted or non-substituted cycloalkenyloxy, substituted or non-substituted aryloxy; substituted or non-substituted heterocyclyloxy, substituted or non-substituted C 5 -C 12 -fused bicycloalkoxy, substituted or non-substituted C 5 -C 12 -fused bicycloalkenyloxy, substituted or non-substituted C 5 -C 12 -benzofused carbocyclyloxy, substituted or non-substituted C 5 -C 12 -benzofused heterocyclyloxy; U represents a oxygen atom or a sulfur atom; R a represents a hydrogen atom, a hydroxy group, substituted or non-substituted C 1 -C 8 -alkyl, substituted or non-substituted C 3 -C 8 -cycloalkyl, a substituted or non-substituted C 2 -C 8 -alkenyl, substituted or non-substituted C 2 -C 8 -alkynyl, substituted or non-substituted C 1 -C 8 -alkoxy, substituted or non-substituted C 3 -C 10 -cycloalkenyl, substituted or non-substituted C 5 -C 12 -fused bicycloalkyl, substituted or non-substituted C 5 -C 12 -fused bicycloalkenyl, substituted or non-substituted aryl, or substituted or non-substituted heterocyclyl, substituted or non-substituted C 1 -C 8 -alkylcarbonyl, substituted or non-substituted aryloxycarbonyl, substituted or non-substituted C 1 -C 8 -alkoxycarbonyl; Z 2 , Z 3 and Z 4 independently represent a hydrogen atom, a halogen atom, substituted or non-substituted C 1 -C 8 -alkyl, substituted or non-substituted C 3 -C 8 -cycloalkyl, a C 2 -C 8 -alkenyl, substituted or non-substituted C 2 -C 8 -alkynyl, substituted or non-substituted C 1 -C 8 -alkoxy;

Y 1 to Y 5 independently represent a hydrogen atom, a halogen atom, a nitro group, a a cyano group, a substituted or non-substituted carbaldehyde O—(C 1 -C 8 -alkyl)oxime, a pentafluoro-λ 6 -sulfenyl group, substituted or non-substituted C 1 -C 8 -alkyl, substituted or non-substituted C 3 -C 8 -cycloalkyl, substituted or non-substituted C 1 -C 8 -halogenoalkyl having 1 to 5 halogen atoms, a C 2 -C 8 -alkenyl, substituted or non-substituted C 2 -C 8 -alkynyl, substituted or non-substituted C 1 -C 8 -alkoxy, substituted or non-substituted C 1 -C 8 -halogenoalkoxy having 1 to 5 halogen atoms, substituted or non-substituted C 1 -C 8 -alkylsulfenyl, substituted or non-substituted C 2 -C 8 -alkenyloxy, substituted or non-substituted C 3 -C 8 -alkynyloxy, substituted or non-substituted N—(C 1 -C 8 -alkoxy)-C 1 -C 8 -alkanimidoyl, substituted or non-substituted N—(C 1 -C 8 -alkoxy)-C 1 -C 8 -halogenoalkanimidoyl having 1 to 5 halogen atoms, substituted or non-substituted C 1 -C 8 -alkoxycarbonyl, substituted or non-substituted C 1 -C 8 -alkylcarbonyloxy, substituted or non-substituted C 1 -C 8 -alkylsulfinyl, substituted or non-substituted C 1 -C 8 -alkylsulfonyl, substituted or non-substituted phenoxy, substituted or non-substituted phenylsulfenyl, substituted or non-substituted aryl, substituted or non-substituted tri(C 1 -C 8 -alkyl)-silyloxy, substituted or non-substituted tri(C 1 -C 8 -alkyl)-silyl, substituted or non-substituted heterocyclyl, substituted or non-substituted heterocyclyloxy;

›CROSS-REFERENCE TO RELATED APPLICATION(S) · 2 of 15

as well as salts, N-oxides, metallic complexes and metalloidic complexes thereof or (E) and (Z) isomers and mixtures thereof.

Any of the compounds according to the invention can exist as one or more stereoisomers depending on the number of stereogenic units (as defined by the IUPAC rules) in the compound. The invention thus relates equally to all the stereoisomers, and to the mixtures of all the possible stereoisomers, in all proportions. The stereoisomers can be separated according to the methods which are known per se by the man ordinary skilled in the art.

Notably, the stereostructure of the oxime moiety present in the 4-substituted-3-{phenyl[(heterocyclylmethoxy)imino]methyl}-1,2,4-oxadiazol-5(4H)-one derivative of formula (I) includes (E) or (Z) isomer, and these stereoisomers form part of the present invention.

According to the invention, the following generic terms are generally used with the following meanings:

halogen means fluorine, chlorine, bromine or iodine; heteroatom can be nitrogen, oxygen or sulfur; unless indicated otherwise, a group or a substituent that is substituted according to the invention can be substituted by one or more of the following groups or atoms: a halogen atom, a nitro group, a hydroxy group, a cyano group, an amino group, a sulfenyl group, a pentafluoro- 6 -sulfenyl group, a formyl group, a carbaldehyde O—(C 1 -C 8 -alkyl)oxime, a formyloxy group, a formylamino group, a formylamino group, a (hydroxyimino)-C 1 -C 6 -alkyl group, a C 1 -C 8 -alkyl, a tri(C 1 -C 8 -alkyl)silyl, C 3 -C 8 -cycloalkyl, C 3 -C 8 -cycloalkenyl, a C 1 -C 8 -halogenoalkyl having 1 to 5 halogen atoms, a C 1 -C 8 -halogenocycloalkyl having 1 to 5 halogen atoms, a C 2 -C 8 -alkenyl, a C 2 -C 8 -alkynyl, a C 2 -C 8 -alkenyloxy, a C 2 -C 8 -alkynyloxy, a C 1 -C 8 -alkylamino, a di-C 1 -C 8 -alkylamino, a C 1 -C 8 -alkoxy, a C 1 -C 8 -halogenoalkoxy having 1 to 5 halogen atoms, a C 1 -C 8 -alkylsulfenyl, a C 1 -C 8 -halogenoalkylsulfenyl having 1 to 5 halogen atoms, a C 2 -C 8 -halogenoalkenyloxy having 1 to 5 halogen atoms, a C 3 -C 8 -halogenoalkynyloxy having 1 to 5 halogen atoms, a C 1 -C 8 -alkylcarbonyl, a C 1 -C 8 -halogenoalkylcarbonyl having 1 to 5 halogen atoms, a C 1 -C 8 -alkylcarbamoyl, a di-C 1 -C 8 -alkylcarbamoyl, a N—C 1 -C 8 -alkyloxycarbamoyl, a C 1 -C 8 -alkoxycarbamoyl, a N—C 1 -C 8 -alkyl-C 1 -C 8 -alkoxycarbamoyl, a C 1 -C 8 -alkoxycarbonyl, a C 1 -C 8 -halogenoalkoxycarbonyl having 1 to 5 halogen atoms, a C 1 -C 8 -alkylcarbonyloxy, a C 1 -C 8 -halogenoalkylcarbonyloxy having 1 to 5 halogen atoms, a C 1 -C 8 -alkylcarbonylamino, a C 1 -C 8 -halogenoalkylcarbonylamino having 1 to 5 halogen atoms, C 1 -C 8 -alkoxycarbonylamino, C 1 -C 8 -halogenoalkoxycarbonylamino having 1 to 5 halogen atoms, a C 1 -C 8 -alkylaminocarbonyloxy, a di-C 1 -C 8 -alkylaminocarbonyloxy, a C 1 -C 8 -alkyloxycarbonyloxy, a (C 1 -C 6 -alkoxyimino)-C 1 -C 6 -alkyl, a (C 1 -C 6 -alkenyloxyimino)-C 1 -C 6 -alkyl, a (C 1 -C 6 -alkynyloxyimino)-C 1 -C 6 -alkyl, (benzyloxyimino)-C 1 -C 6 -alkyl, C 1 -C 8 -alkoxyalkyl, C 1 -C 8 -halogenoalkoxyalkyl having 1 to 5 halogen atoms, benzyloxy, benzylsulfenyl, benzylamino, phenoxy, phenylsulfenyl, or phenylamino, an aryl group, an heterocyclyl group; or a group or a substituent that is substituted according to the invention can be substituted in a way that substituting groups form together a substituted or non-substituted, saturated or partially saturated 3-, 4-, 5-, 6-, 7-, 8-, 9-, 10-, or 11-membered cycle, which can be a carbocycle or a heterocycle comprising up to 4 heteroatoms selected from the list consisting of N, O, and S the term “aryl” means phenyl or naphthyl; the term “heterocyclyl” means fused or non-fused, saturated or unsaturated, 4-, 5-, 6-, 7-, 8-, 9-, 10-, 11- or 12-membered ring comprising up to 4 heteroatoms selected in the list consisting of N, O, S.

Preferred compounds of formula (I) according to the invention are those wherein X 1 represents a hydrogen atom, substituted or non-substituted C 1 -C 8 -alkyl, substituted or non-substituted C 3 -C 8 -cycloalkyl or a substituted or non-substituted C 2 -C 8 -alkenyl.

More preferred compounds of formula (I) according to the invention are those wherein X 1 represents a hydrogen atom, a methyl group, an ethyl group, a n-propyl group, an isopropyl group or a cyclopropyl group.

Even more preferred compounds of formula (I) according to the invention are those wherein X 1 represents a hydrogen atom or a methyl group.

Other preferred compounds of formula (I) according to the invention are those wherein A represents A 1 .

Other preferred compounds of formula (I) according to the invention are those wherein Z 1 represents a hydrogen atom, a halogen atom, a nitro group, an amino group, an hydroxyamino group, substituted or non-substituted C 1 -C 8 -alkoxyamino group, substituted or non-substituted C 1 -C 8 -alkylamino, substituted or non-substituted C 3 -C 10 -cycloalkylamino, substituted or non-substituted C 3 -C 10 -cycloalkenylamino, substituted or non-substituted C 5 -C 12 -fused bicycloalkylamino, substituted or non-substituted C 5 -C 12 -fused bicycloalkenylamino, substituted or non-substituted di-C 1 -C 8 -alkylamino, substituted or non-substituted phenylamino, substituted or non-substituted heterocyclylamino, or a group of formula QC(═U)NR a .

More preferred compounds of formula (I) according to the invention are those wherein Z 1 represents a hydrogen atom, a halogen atom, a nitro group, an amino group, substituted or non-substituted C 1 -C 8 -alkoxyamino group, substituted or non-substituted C 1 -C 8 -alkylamino, substituted or non-substituted C 3 -C 10 -cycloalkylamino, or a group of formula QC(═U)NR a .

Even more preferred compounds of formula (I) according to the invention are those wherein Z 1 represents an amino group, or a group of formula QC(═U)NR a .

When Z 1 represents a group of formula QC(═U)NR a , other preferred compounds of formula (I) according to the invention are those wherein U represents an oxygen atom.

›CROSS-REFERENCE TO RELATED APPLICATION(S) · 3 of 15

When Z 1 represents a group of formula QC(═U)NR a , other preferred compounds of formula (I) according to the invention are those wherein R a represents a hydrogen atom, a hydroxy group, substituted or non-substituted C 1 -C 8 -alkyl, substituted or non-substituted C 3 -C 8 -cycloalkyl, substituted or non-substituted C 1 -C 8 -alkoxy.

When Z 1 represents a group of formula QC(═U)NR a , more preferred compounds of formula (I) according to the invention are those wherein R a represents a hydrogen atom.

When Z 1 represents a group of formula QC(═U)NR a , other preferred compounds of formula (I) according to the invention are those wherein Q represents a substituted or non-substituted C 1 -C 8 -alkyl, substituted or non-substituted C 3 -C 8 -cycloalkyl, substituted or non-substituted C 2 -C 8 -alkynyl, substituted or non-substituted C 1 -C 8 -alkoxy, substituted or non-substituted C 2 -C 8 -alkenyloxy, substituted or non-substituted C 2 -C 8 -alkynyloxy, substituted or non-substituted C 1 -C 8 -alkylsulfenyl, substituted or non-substituted aryl, substituted or non-substituted heterocyclyl, substituted or non-substituted C 3 -C 8 -cycloalkoxy.

When Z 1 represents a group of formula QC(═U)NR a , more preferred compounds of formula (I) according to the invention are those wherein Q represents a substituted or non-substituted C 4 -C 8 -alkyl, substituted or non-substituted C 3 -C 8 -cycloalkyl, substituted or non-substituted C 4 -C 8 -alkynyl, substituted or non-substituted C 4 -C 8 -alkoxy, substituted or non-substituted C 4 -C 8 -alkenyloxy, substituted or non-substituted C 4 -C 8 -alkynyloxy, substituted or non-substituted C 3 -C 8 -alkylsulfenyl, substituted or non-substituted aryl, substituted or non-substituted heterocyclyl.

When Z 1 represents a group of formula QC(═U)NR a , even more preferred compounds of formula (I) according to the invention are those wherein Q represents a substituted or non-substituted C 4 -C 8 -alkyl, substituted or non-substituted C 4 -C 8 -alkynyl, substituted or non-substituted C 4 -C 8 -alkoxy, substituted or non-substituted C 4 -C 8 -alkenyloxy, substituted or non-substituted C 4 -C 8 -alkynyloxy, substituted or non-substituted aryl, substituted or non-substituted heterocyclyl.

When Z 1 represents a group of formula QC(═U)NR a , and when Q represents a substituted or non-substituted C 4 -C 8 -alkyl, substituted or non-substituted C 3 -C 8 -cycloalkyl, substituted or non-substituted C 4 -C 8 -alkynyl, substituted or non-substituted C 4 -C 8 -alkoxy, substituted or non-substituted C 4 -C 8 -alkenyloxy, substituted or non-substituted C 4 -C 8 -alkynyloxy, substituted or non-substituted C 3 -C 8 -alkylsulfenyl, substituted or non-substituted aryl, substituted or non-substituted heterocyclyl, other preferred compounds of formula (I) according to the invention are those wherein substituents are chosen in the list of a halogen atom, a cyano group, a (hydroxyimino)-C 1 -C 6 -alkyl group, a C 1 -C 8 -alkyl, C 3 -C 8 -cycloalkyl, a C 2 -C 8 -alkenyl, a C 2 -C 8 -alkynyl, a C 2 -C 8 -alkenyloxy, a C 2 -C 8 -alkynyloxy, a C 1 -C 8 -alkoxy, a C 1 -C 8 -alkylsulfenyl, a (C 1 -C 6 -alkoxyimino)-C 1 -C 6 -alkyl, a (C 1 -C 6 -alkenyloxyimino)-C 1 -C 6 -alkyl, a (C 1 -C 6 -alkynyloxyimino)-C 1 -C 6 -alkyl, (benzyloxyimino)-C 1 -C 6 -alkyl, C 1 -C 8 -alkoxyalkyl, benzyloxy, benzylsulfenyl, phenoxy, phenylsulfenyl, an aryl group or an heterocyclyl group, or wherein substituents form together a substituted or non-substituted, saturated or partially saturated 3-, 4-, 5-, 6-, 7-, 8-, 9-, 10-, or 11-membered cycle, which can be a carbocycle or a heterocycle comprising up to 4 heteroatoms selected from the list consisting of N, O, and S.

When Z 1 represents a group of formula QC(═U)NR a , and when Q represents a substituted or non-substituted C 4 -C 8 -alkyl, substituted or non-substituted C 3 -C 8 -cycloalkyl, substituted or non-substituted C 4 -C 8 -alkynyl, substituted or non-substituted C 4 -C 8 -alkoxy, substituted or non-substituted C 4 -C 8 -alkenyloxy, substituted or non-substituted C 4 -C 8 -alkynyloxy, substituted or non-substituted C 3 -C 8 -alkylsulfenyl, substituted or non-substituted aryl, substituted or non-substituted heterocyclyl, more preferred compounds of formula (I) according to the invention are those wherein substituents are chosen in the list of a halogen atom, a cyano group, a (hydroxyimino)-C 1 -C 6 -alkyl group, a C 1 -C 8 -alkyl, C 3 -C 8 -cycloalkyl, a C 2 -C 8 -alkenyl, a C 2 -C 8 -alkynyl, a C 2 -C 8 -alkenyloxy, a C 2 -C 8 -alkynyloxy, a C 1 -C 8 -alkoxy, a C 1 -C 8 -alkylsulfenyl, (benzyloxyimino)-C 1 -C 6 -alkyl, C 1 -C 8 -alkoxyalkyl, benzyloxy, phenoxy, an aryl group or an heterocyclyl group or wherein substituents form together a saturated or partially saturated 3-, 4-, 5-, 6-membered cycle, which can be a carbocycle or a heterocycle comprising up to 4 heteroatoms selected from the list consisting of N, O, and S.

Other preferred compounds of formula (I) according to the invention are those wherein Z 2 , Z 3 and Z 4 independently represent a hydrogen atom, a halogen atom, substituted or non-substituted C 1 -C 8 -alkyl. More preferred compounds of formula (I) according to the invention are those wherein Z 2 , Z 3 and Z 4 independently represent a hydrogen atom.

Other preferred compounds of formula (I) according to the invention are those wherein Y 1 to Y 5 independently represent a hydrogen atom, a halogen atom, substituted or non-substituted C 1 -C 8 -alkyl, substituted or non-substituted C 3 -C 8 -cycloalkyl, substituted or non-substituted C 1 -C 8 -halogenoalkyl having 1 to 5 halogen atoms, substituted or non-substituted C 1 -C 8 -alkoxy.

More preferred compounds of formula (I) according to the invention are those wherein Y 1 to Y 5 independently represent a hydrogen atom, a halogen atom, methyl, ethyl, isopropyl, isobutyl, tertbutyl, trifluoromethyl, difluoromethyl, allyl, ethynyl, propargyl, cyclopropyl, methoxy or trifluoromethoxy. Even more preferred compounds of formula (I) according to the invention are those wherein Y 1 to Y 5 independently represent a hydrogen atom or fluorine atom.

›CROSS-REFERENCE TO RELATED APPLICATION(S) · 4 of 15

The above mentioned preferences with regard to the substituents of the compounds of formula (I) according to the invention can be combined in various manners. These combinations of preferred features thus provide sub-classes of compounds according to the invention. Examples of such sub-classes of preferred compounds according to the invention can combine:

preferred features of A with preferred features of one or more of X 1 , Y 1 to Y 5 and Z 1 to Z 4 ; preferred features of X 1 with preferred features of one or more of A, Y 1 to Y 5 and Z 1 to Z 4 ; preferred features of Y 1 with preferred features of one or more of A, X 1 , Y 2 to Y 5 and Z 1 to Z 4 ; preferred features of Y 2 with preferred features of one or more of A, X 1 , Y 1 , Y 3 to Y 5 and Z 1 to Z 4 ; preferred features of Y 3 with preferred features of one or more of A, X 1 , Y 1 , Y 2 , Y 4 , Y 5 and Z 1 to Z 4 ; preferred features of Y 4 with preferred features of one or more of A, X 1 , Y 1 to Y 3 , Y 5 and Z 1 to Z 4 ; preferred features of Y 5 with preferred features of one or more of A, X 1 , Y 1 to Y 4 and Z 1 to Z 4 ; preferred features of Z 1 with preferred features of one or more of X 1 , Y 1 to Y 5 , A and Z 2 to Z 4 ; preferred features of Z 2 with preferred features of one or more of X 1 , Y 1 to Y 5 , A, Z 1 and Z 3 to Z 4 ; preferred features of Z 3 with preferred features of one or more of X 1 , Y 1 to Y 5 , A, Z 4 and Z 1 to Z 2 ; preferred features of Z 4 with preferred features of one or more of X 1 , Y 1 to Y 5 , A and Z 1 to Z 3 ;

In these combinations of preferred features of the substituents of the compounds according to the invention, the said preferred features can also be selected among the more preferred features of each of A, X 1 , Y 1 to Y 5 and Z 1 so as to form most preferred subclasses of compounds according to the invention.

The present invention also relates to a process for the preparation of compounds of formula (I). Thus, according to a further aspect of the present invention, there is a provided a process P1 for the preparation of compounds of formula (I) from compounds of formula (II), by a reaction of nucleophilic substitution on compounds of formula (III) to yield to a compound of formula (IV), according to known methods, optionally in the presence of a base, according to known methods; followed by the addition of hydroxylamine or an hydroxylamine salt on compounds of formula (IV) to yield to a compound of formula (V), optionally in the presence of a base, optionally in the presence of an acid, according to known methods; followed by a reaction of cyclization of compounds of formula (V) to yield to a compound of formula (Ia), with a phosgene equivalent, optionally in the presence of a base, according to known methods; followed by a reaction of alkylation of compounds of formula (Ia) to yield to a compound of formula (I), with an alkylating agent of formula X 1 -LGa, optionally in the presence of a base, according to known methods.

In such a case there is provided a process P1 according to the invention and such a process P1 can be illustrated by the following reaction scheme:

wherein Y 1 , Y 2 , Y 3 , Y 4 , Y 5 , A and X 1 are as herein-defined and LG and LGa independently represent a leaving group. Suitable leaving groups can be selected in the list consisting of a halogen atom or other customary nucleofugal groups such as triflate, mesylate, or tosylate.

Suitable acids for the transformation of compounds of formula (IV) into compounds of formula (V) can be chosen as being a mineral acid such as hydrogen chloride and sulfuric acid, and an organic acid such as formic acid and acetic acid.

Suitable phosgene equivalent for the conversion of compounds of formula (V) into a compound of formula (I) can be chosen as being phosgene, diphosgene, triphosgene, carbonyl di-imidazole, a chlorformate derivative, such as ethyl chloroformate and 4-nitrophenoxy-chloroformate.

Compounds of formula (II) and (III) are commercially available or are easily accessible to the skilled worker in the art. Examples of preparation can be found in world patent application WO2009/130193. Compounds of formula X 1 -LGa are commercially available.

According to the invention, there is provided a further process P2 for the preparation of compounds of formula (Ic) from compounds of formula (Ib).

For the compounds of formula (Ib) according to the invention if Z 1 represents —NHR a , process P1 according to the invention can be completed by a further step comprising the additional modification of this group, notably by a reaction of acylation, alkoxycarbonylation, alkylaminocarbonylation, (thio)acylation, alkoxy(thio)carbonylation, alkylsuphenyl(thio)carbonylation or alkylamino(thio)carbonylation to yield to a compound of formula (Ic), according to known methods. In such a case there is provided a process P2 according to the invention and such a process P2 can be illustrated by the following reaction scheme:

Wherein

Y 1 , Y 2 , Y 3 , Y 4 , Y 5 , X 1 , U, R a and Q are as herein-defined and A b represents A wherein Z 1 represents —NHR a ; A, represents A wherein Z 1 represents a group of formula QC(═U)NR a and LG′ represents a leaving group.

Suitable leaving groups can be selected in the list consisting of a halogen atom or other customary nucleofugal groups such as alcoolate, hydroxide or cyanide.

According to the invention, there is provided a further process P3 for the preparation of compounds of formula (Ie) from compounds of formula (Id), by a reaction of nucleophilic substitution to yield to a compound of formula (Ie), according to known methods, optionally in the presence of a catalyst notably a transition metal catalyst, such as palladium salts or complexes for example palladium (II) chloride, palladium (II) acetate, tetrakis-(triphenylphosphine) palladium(0), bis-(triphenylphosphine) palladium dichloride (II), tris(dibenzylideneacetone) dipalladium(0), bis(dibenzylideneacetone) palladium(0) or 1,1′-bis(diphenylphosphino)ferrocene-palladium (II) chloride. As an alternative the palladium complex is directly generated in the reaction mixture by separately adding to the reaction mixture a palladium salt and a complex ligand such as a phosphine, for example triethylphosphine, tri-tart-butylphosphine, tricyclohexylphosphine, 2-(dicyclohexylphosphine)biphenyl, 2-(di-tert-butylphosphin)biphenyl, 2-(dicyclohexylphosphine)-2′-(N,N-dimethylamino)-biphenyl, triphenylphosphine, tris-(o-tolyl)phosphine, sodium 3-(diphenylphosphino)benzolsulfonate, tris-2-(methoxyphenyl)phosphine, 2,2′-bis-(diphenylphosphine)-1,1′-binaphthyl, 1,4-bis-(diphenylphosphine)butane, 1,2-bis-(diphenylphosphine)ethane, 1,4-bis-(dicyclohexylphosphine)butane, 1,2-bis-(dicyclohexylphosphine)ethane, 2-(dicyclohexylphosphine)-2′-(N,N-dimethylamino)-biphenyl, bis(diphenylphosphino)ferrocene, tris-(2,4-tart-butylphenyl)-phosphite, (R)-(−)-1-[(S)-2-(diphenylphosphino)ferrocenyl]ethyldi-tert-butylphosphine, (S)-(+)-1-[(R)-2-(diphenylphosphino)ferrocenyl]ethyldicyclohexylphosphine, (R)-(−)-1-[(S)-2-(diphenylphosphino)ferrocenyl]ethyldicyclohexylphosphine, (S)-(+)-1-[(R)-2-(diphenylphosphino)ferrocenyl]ethyldi-t-butylphosphine, optionally in the presence of a base such as an inorganic or an organic base; preferably an alkaline earth metal or alkali metal hydride, hydroxide, amide, alcoholate, acetate, carbonate or hydrogen carbonate, such as sodium hydride, sodium amide, lithiium diisopropylamide, sodium methanolate, sodium ethanolate, potassium tert-butanolate, sodium acetate, potassium acetate, calcium acetate, sodium hydroxide, potassium hydroxide, sodium carbonate, potassium carbonate, potassium bicarbonate, sodium bicarbonate, cesium carbonate or ammonium carbonate; and also tertiary amine, such as trimethylamine, triethylamine (TEA), tributylamine, N,N-dimethylaniline, N,N-dimethyl-benzylamine, N,N-diisopropyl-ethylamine (DIPEA), pyridine, N-methylpiperidine, N-methylmorpholine, N,N-dimethylaminopyridine, diazabicyclooctane (DABCO), diazabicyclononene (DBN) or diazabicycloundecene (DBU), according to known methods. In such a case there is provided a process P3 according to the invention and such a process P3 can be illustrated by the following reaction scheme:

›CROSS-REFERENCE TO RELATED APPLICATION(S) · 5 of 15

wherein

Y 1 , Y 2 , Y 3 , Y 4 , Y 5 and X 1 are as herein-defined and A d represents A wherein Z 1 represents a halogen atom; A e represents A wherein Z 1 represents an amino group, a cyano group, substituted or non-substituted C 1 -C 8 -alkoxyamino group, substituted or non-substituted C 1 -C 8 -alkylamino, substituted or non-substituted C 3 -C 10 -cycloalkylamino, substituted or non-substituted C 3 -C 10 -cycloalkenylamino, substituted or non-substituted C 5 -C 12 -fused bicycloalkylamino, substituted or non-substituted C 5 -C 12 -fused bicycloalkenylamino, substituted or non-substituted di-C 1 -C 8 -alkylamino, substituted or non-substituted phenylamino, substituted or non-substituted heterocyclylamino, or a group of formula QC(═O)NHR a .

According to the invention, there is provided a further process P4 for the preparation of compounds of formula (Ig) from compounds of formula (If).

For the compounds of formula (If) according to the invention, A f represents A wherein Z 1 represents a group of formula QC(═O)NR a , process P1 according to the invention can be completed by a further step comprising the additional modification of this group, notably by a reaction of thiocarbonylation in the presence of a thiocarbonylating agent such as 2,4-bis(4-methoxyphenyl)-1,3,2,4-dithiadiphosphetane 2,4-disulfide, phosphorus pentasulfide, sulfur to yield to a compound of formula (Ig), according to known methods. In such a case there is provided a process P4 according to the invention and such a process P4 can be illustrated by the following reaction scheme:

Wherein

Y 1 , Y 2 , Y 3 , Y 4 , Y 5 , X 1 , R a and Q are as herein-defined; A f represents A wherein Z 1 represents a group of formula QC(═O)NR a and A g represents A wherein Z 1 represents a group of formula QC(═S)NR a .

The present invention also relates to a process for the preparation of compounds of formula (I). Thus, according to a further aspect of the present invention, there is a provided a process P5 for the preparation of compounds of formula (I) from compounds of formula (VI), by a reaction of oxidation compounds of formula (VI) in a presence of a suitable oxidizing agent to yield to a compound of compounds of formula (VII), followed by a condensation of compounds of formula (VIII), optionally under microwave irradiation, optionally in the presence of a dehydrating agent, such as molecular sieves, to yield to compounds of formula (I), according to known methods. In such a case there is provided a process P5, according to the invention and such a process P5 can be illustrated by the following reaction scheme:

wherein Y 1 , Y 2 , Y 3 , Y 4 , Y 5 , A and X 1 are as herein-defined.

Examples of oxidations at the methylene position between a phenyl ring and an heterocycle to yield an oxo substituent are known and can be found for example in Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999) (1982), (12), 2995-3006. Suitable oxidizing agents for carrying out the first step of process P5 according to the invention can be inorganic and organic peroxides such as hydrogen peroxide and benzoyl peroxide, metallic and metalloïdic oxides such as manganese (IV) oxide, chromium (VI) oxide, oxygen optionally in the presence of singlet oxygen activator, halogenating agents in an aqueous medium such as bleach.

Compounds of formula (VI) are easily accessible to the skilled worker in the art. Examples of preparation can be found in Annali di Chimica (Rome, Italy), (1963), 53(10), 1405-10

Examples of condensations of compounds of formula (VIII) with compounds of formula (VIII) can be found in world patent application WO2010/000841.

Compounds of formula (VIII) are easily accessible to the skilled worker in the art. Examples of preparation can be found in world patent application WO2010/000841.

According to the invention, there is provided a further process P6 for the preparation of compounds of formula (Ii) from compounds of formula (Ih), by a reaction of alkylation, according to known methods. In such a case there is provided a process P6 according to the invention and such a process P6 can be illustrated by the following reaction scheme:

Wherein

Y 1 , Y 2 , Y 3 , Y 4 , Y 5 , X 1 are as herein-defined A h represents A wherein Z 1 represents an amino, substituted or non-substituted C 1 -C 8 -alkylamino or a group of formula —NHC(═O)Q wherein Q is as herein defined A i represents A wherein Z 1 represents substituted or non-substituted C 1 -C 8 -alkylamino, substituted or non-substituted C 3 -C 10 -cycloalkylamino, substituted or non-substituted C 3 -C 10 -cycloalkenylamino, substituted or non-substituted C 5 -C 12 -fused bicycloalkylamino, substituted or non-substituted C 5 -C 12 -fused bicycloalkenylamino, substituted or non-substituted di-C 1 -C 8 -alkylamino, substituted or non-substituted heterocyclylamino, or a group of formula QC(═U)NR R represents optionally substituted C 1 -C 8 -alkyl, C 2 -C 8 -alkenyl, C 2 -C 8 -alkynyl, C 3 -C 10 -cycloalkyl, C 3 -C 10 -cycloalkenyl, C 3 -C 10 -fused bicycloalkyl, C 5 -C 12 -fused bicycloalkenyl LG″ represents a leaving group.

Suitable leaving groups can be selected in the list consisting of a halogen atom or other customary nucleofugal groups such as alcoolate, hydroxide or cyanide.

According to the invention, there is provided a further process P7 for the preparation of compounds of formula (Ik) from compounds of formula (Il), by a reaction of deprotection, according to known methods. In such a case there is provided a process P7 according to the invention and such a process P7 can be illustrated by the following reaction scheme:

Wherein

Y 1 , Y 2 , Y 3 , Y 4 , Y 5 , X 1 are as herein-defined A j represents A wherein Z 1 represents a group of formula Z 1 a -PG wherein Z 1 a represents a substituted or non-substituted C 1 -C 8 -alkoxyamino, substituted or non-substituted C 1 -C 8 -alkylamino, a substituted or non-substituted C 2 -C 8 -alkenylamino, substituted or non-substituted C 2 -C 8 -alkynylamino, substituted or non-substituted C 3 -C 10 -cycloalkylamino, substituted or non-substituted C 3 -C 10 -cycloalkenylamino, substituted or non-substituted C 5 -C 12 -fused bicycloalkylamino, substituted or non-substituted C 5 -C 12 -fused bicycloalkenylamino, substituted or non-substituted di-C 1 -C 8 -alkylamino, substituted or non-substituted phenylamino, substituted or non-substituted heterocyclylamino and PG represents a protecting group such as a formyl group, C 1 -C 8 -alkylcarbonyl, C 1 -C 8 -alkoxycarbonyl, C 1 -C 8 -alkoxy-C 1 -C 2 -alkyl, tri(C 1 -C 8 -alkyl)silyl-C 1 -C 2 -alkyl, tri(C 1 -C 8 -alkyl)silyloxy-C 1 -C 2 -alkyl; A k represents A wherein Z 1 represents Z 1 a ;

›CROSS-REFERENCE TO RELATED APPLICATION(S) · 6 of 15

Amino-protecting groups and related methods of cleavage thereof are known and can be found in T. W. Greene and P. G. M. Wuts, Protective Group in Organic Chemistry, 3 rd ed., John Wiley & Sons.

According to the invention, there is provided a further process P8 for the preparation of compounds of formula (Im) from compounds of formula (Il), by a reaction of amino-reduction, in the presence of a reducing agent, such as hydrogen gas or an hydride derivative, in particular sodium cyanoborohydride, according to known methods. In such a case there is provided a process P8 according to the invention and such a process P8 can be illustrated by the following reaction scheme:

Where

Y 1 , Y 2 , Y 3 , Y 4 , Y 5 , X 1 are as herein-defined; A i represents A wherein Z 1 represents an amino group, a substituted or non-substituted C 1 -C 8 -alkylamino; A m represents A wherein Z 1 represents a substituted or non-substituted C 1 -C 8 -alkylamino, substituted or non-substituted di-C 1 -C 8 -alkylamino.

According to the invention, there is provided a further process P9 for the preparation of compounds of formula (Io) from compounds of formula (In) according to the following reaction scheme in either one or two steps.

Wherein

Y 1 , Y 2 , Y 3 , Y 4 , Y 5 , X 1 , R a and Q are as herein-defined and A b represents A wherein Z 1 represents —NHR a ; A c represents A wherein Z 1 represents a group of formula QC(═U)NR a and LG′ represents a leaving group.

Wherein

Y 1 , Y 2 , Y 3 , Y 4 , Y 5 , X 1 , R a are as herein-defined;

A n represents A wherein Z 1 represents —NHR a ;

A o represents A wherein Z 1 represents Q′C(═O)NR a wherein Q′ represents substituted or non-substituted C 1 -C 8 -alkoxy, substituted or non-substituted C 2 -C 8 -alkenyloxy, substituted or non-substituted C 2 -C 8 -alkynyloxy, substituted or non-substituted C 1 -C 8 -alkylsulfenyl, substituted or non-substituted C 2 -C 8 -alkenylsulfenyl, substituted or non-substituted C 2 -C 8 -alkynylsulfenyl, substituted or non-substituted arylsulfenyl, substituted or non-substituted cycloalkoxy; substituted or non-substituted cycloalkenyloxy, substituted or non-substituted aryloxy; substituted or non-substituted heterocyclyloxy, substituted or non-substituted C 5 -C 12 -fused bicycloalkoxy, substituted or non-substituted C 5 -C 12 -fused bicycloalkenyloxy, substituted or non-substituted C 5 -C 12 -benzofused carbocyclyloxy, substituted or non-substituted C 5 -C 12 -benzofused heterocyclyloxy;

LG 1 and LG 2 represent leaving groups

Suitable leaving groups can be selected in the list consisting of a halogen atom or other customary nucleofugal groups such as imidazole, halogenophenoxide or the likes.

According to the invention, processes P1 to P9 can be performed if appropriate in the presence of a solvent and if appropriate in the presence of a base.

According to the invention, processes P1 and P2 can be performed if appropriate in the presence of a catalyst. Suitable catalyst can be chosen as being 4-dimethyl-aminopyridine, 1-hydroxy-benzotriazole or dimethylformamide.

In case LG′ represents a hydroxy group, the process P2 according to the present invention can be performed in the presence of condensing agent. Suitable condensing agent can be chosen as being acid halide former, such as phosgene, phosphorous tri-bro-mide, phosphorous trichloride, phosphorous pentachloride, phosphorous trichloride oxide or thionyl chloride; anhydride former, such as ethyl chloroformate, methyl chloroformate, isopropyl chloroformate, isobutyl chloroformate or methanesulfonyl chloride; carbodiimides, such as N,N′-dicyclohexylcarbodiimide (DCC) or other customary condensing agents, such as phosphorous pentoxide, polyphosphoric acid, N,N′-carbonyl-diimidazole, 2-ethoxy-N-ethoxycarbonyl-1,2-dihydroquinoline (EEDQ), triphenylphosphine/tetrachloromethane, 4-(4,6-dimethoxy[1.3.5]triazin-2-yl)-4-methylmorpholinium chloride hydrate or bromo-tripyrrolidino-phosphonium-hexafluorophosphate.

Suitable solvents for carrying out processes P1 to P9 according to the invention are customary inert organic solvents. Preference is given to using optionally halogenated aliphatic, alicyclic or aromatic hydrocarbons, such as petroleum ether, hexane, heptane, cyclohexane, methylcyclohexane, benzene, toluene, xylene or decalin; chlorobenzene, dichlorobenzene, dichloromethane, chloroform, carbon tetrachloride, dichlorethane or trichlorethane; ethers, such as diethyl ether, diisopropyl ether, methyl tert-butyl ether, methyl tert-amyl ether, dioxane, tetrahydrofuran, 1,2-dimethoxyethane, 1,2-diethoxyethane or anisole; nitriles, such as acetonitrile, propionitrile, n- or iso-butyronitrile or benzonitrile; amides, such as N,N-dimethylformamide, N,N-dimethylacetamide, N-methylformanilide, N-methylpyrrolidone or hexamethylphosphoric triamide; esters, such as methyl acetate or ethyl acetate, sulfoxides, such as dimethyl sulfoxide or sulfones, such as sulfolane.

Suitable bases for carrying out processes P1 to P9 according to the invention are inorganic and organic bases which are customary for such reactions. Preference is given to using alkaline earth metal, alkali metal hydride, alkali metal hydroxides or alkali metal alkoxides, such as sodium hydroxide, sodium hydride, calcium hydroxide, potassium hydroxide, potassium tert-butoxide or other ammonium hydroxide, alkali metal carbonates, such as sodium carbonate, potassium carbonate, potassium bicarbonate, sodium bicarbonate, cesium carbonate, alkali metal or alkaline earth metal acetates, such as sodium acetate, potassium acetate, calcium acetate and also tertiary amines, such as trimethylamine, triethylamine, diisopropylethylamine, tributylamine. N,N-dimethylaniline, pyridine, N-methylpiperidine. N,N-dimethylaminopyridine, 1,4-diazabicyclo[2.2.2]octane (DABCO), 1,5-diazabicyclo[4.3.0]non-5-ene (DBN) or 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU).

If carrying out processes P1 to P9, according to the invention, the reaction temperature can independently be varied within a relatively wide range. Generally, process P1 according to the invention is carried out at temperatures between −20° C. and 160° C.

›CROSS-REFERENCE TO RELATED APPLICATION(S) · 7 of 15

Processes P1 to P9 according to the invention are generally independently carried out under atmospheric pressure. However, it is also possible to operate under elevated or reduced pressure.

Work-up is carried out by customary methods. Generally, the reaction mixture is treated with water and the organic phase is separated off and, after drying, concentrated under reduced pressure. If appropriate, the remaining residue can be freed by customary methods, such as chromatography or recrystallization, from any impurities that can still be present.

Compounds according to the invention can be prepared according to the above described processes. It will nevertheless be understood that, on the basis of his general knowledge and of available publications, the skilled worker will be able to adapt these processes according to the specifics of each of the compounds according to the invention that is desired to be synthesised.

The compounds of formula (IV) can be advantageously prepared according to the method described in WO2011/080254, hereby incorporated by reference.

In a further aspect, if A is as herein-described, the present invention relates to compounds of formula (V) useful as intermediate compounds or materials for the process of preparation according to the invention.

The present invention thus provides compounds of formula (V) wherein Y 1 , Y 2 , Y 3 , Y 4 , Y 5 and A are as herein-defined.

In a further aspect, if X 1 represents substituted or non-substituted C 1 -C 8 -alkyl, the present invention relates to compounds of formula (VII) useful as intermediate compounds or materials for the process of preparation according to the invention.

The present invention thus provides compounds of formula (VII) wherein Y 1 , Y 2 , Y 3 , Y 4 , Y 5 are as herein-defined and X 1 represents substituted or non-substituted C 1 -C 8 -alkyl.

In a further aspect, the present invention also relates to a fungicide composition comprising an effective and non-phytotoxic amount of an active compound of formula (I).

The expression “effective and non-phytotoxic amount” means an amount of composition according to the invention which is sufficient to control or destroy the fungi present or liable to appear on the crops and which does not entail any appreciable symptom of phytotoxicity for the said crops. Such an amount can vary within a wide range depending on the fungus to be controlled, the type of crop, the climatic conditions and the compounds included in the fungicide composition according to the invention. This amount can be determined by systematic field trials, which are within the capabilities of a person skilled in the art.

Thus, according to the invention, there is provided a fungicide composition comprising, as an active ingredient, an effective amount of a compound of formula (I) as herein defined and an agriculturally acceptable support, carrier or filler.

According to the invention, the term “support” denotes a natural or synthetic organic or inorganic compound with which the active compound of formula (I) is combined or associated to make it easier to apply, notably to the parts of the plant. This support is thus generally inert and should be agriculturally acceptable. The support can be a solid or a liquid. Examples of suitable supports include clays, natural or synthetic silicates, silica, resins, waxes, solid fertilisers, water, alcohols, in particular butanol organic solvents, mineral and plant oils and derivatives thereof. Mixtures of such supports can also be used.

The composition according to the invention can also comprise additional components. In particular, the composition can further comprise a surfactant. The surfactant can be an emulsifier, a dispersing agent or a wetting agent of ionic or non-ionic type or a mixture of such surfactants. Mention can be made, for example, of polyacrylic acid salts, lignosulfonic acid salts, phenolsulfonic or naphthalenesulfonic acid salts, polycondensates of ethylene oxide with fatty alcohols or with fatty acids or with fatty amines, substituted phenols (in particular alkylphenols or arylphenols), salts of sulfosuccinic acid esters, taurine derivatives (in particular alkyl taurates), phosphoric esters of polyoxyethylated alcohols or phenols, fatty acid esters of polyols and derivatives of the above compounds containing sulfate, sulfonate and phosphate functions. The presence of at least one surfactant is generally essential if the active compound and/or the inert support are water-insoluble and if the vector agent for the application is water. Preferably, surfactant content can be comprised from 5% to 40% by weight of the composition.

Optionally, additional components can also be included, e.g. protective colloids, adhesives, thickeners, thixotropic agents, penetration agents, stabilisers, sequestering agents. More generally, the active compounds can be combined with any solid or liquid additive, which complies with the usual formulation techniques.

In general, the composition according to the invention can contain from 0.05 to 99% by weight of active compound, preferably 10 to 70% by weight.

Compositions according to the invention can be used in various forms and formulations such as aerosol dispenser, capsule suspension, cold fogging concentrate, dustable powder, emulsifiable concentrate, emulsion oil in water, emulsion water in oil, encapsulated granule, fine granule, flowable concentrate for seed treatment, gas (under pressure), gas generating product, granule, hot fogging concentrate, macrogranule, microgranule, oil dispersible powder, oil miscible flowable concentrate, oil miscible liquid, paste, plant rodlet, powder for dry seed treatment, seed coated with a pesticide, soluble concentrate, soluble powder, solution for seed treatment, suspension concentrate (flowable concentrate), ultra low volume (ULV) liquid, ultra low volume (ULV) suspension, water dispersible granules or tablets, water dispersible powder for slurry treatment, water soluble granules or tablets, water soluble powder for seed treatment and wettable powder. These compositions include not only compositions which are ready to be applied to the plant or seed to be treated by means of a suitable device, such as a spraying or dusting device, but also concentrated commercial compositions which must be diluted before application to the crop.

›CROSS-REFERENCE TO RELATED APPLICATION(S) · 8 of 15

The compounds according to the invention can also be mixed with one or more insecticide, fungicide, bactericide, attractant, acaricide or pheromone active substance or other compounds with biological activity. The mixtures thus obtained have a broadened spectrum of activity. The mixtures with other fungicide compounds are particularly advantageous. The composition according to the invention comprising a mixture of a compound of formula (I) with a bactericide compound can also be particularly advantageous.

The formulations can be prepared in a manner known per se, for example by mixing the active ingredients with at least one customary extender, solvent or diluent, adjuvant, emulsifier, dispersant, and/or binder or fixative, wetting agent, water repellent, if appropriate desiccants and UV stabilizers and, if appropriate, dyes and pigments, antifoams, preservatives, inorganic and organic thickeners, adhesives, gibberellins and also further processing auxiliaries and also water. Depending on the formulation type to be prepared further processing steps are necessary, e.g. wet grinding, dry grinding and granulation.

The inventive active ingredients may be present as such or in their (commercial) formulations and in the use forms prepared from these formulations as a mixture with other (known) active ingredients, such as insecticides, attractants, sterilants, bactericides, acaricides, nematicides, fungicides, growth regulators, herbicides, fertilizers, safeners, biologicals and/or semiochemicals.

The present invention further relates to the use of compounds of the formula (I) as herein defined for the control of phytopathogenic fungi.

The present invention further relates to the use of compounds of the formula (I) as herein defined for the treatment of transgenic plants.

The present invention further relates to the use of compounds of the formula (I) as herein defined for the treatment of seed and of seed of transgenic plants.

The present invention further relates to a process for producing compositions for controlling phytopathogenic harmful fungi, characterized in that derivatives of the formula (I) as herein defined are mixed with extenders and/or surfactants.

According to another object of the present invention, there is provided a method for controlling the phytopathogenic fungi of plants, crops or seeds, characterized in that an agronomically effective and substantially non-phytotoxic quantity of a pesticide composition according to the invention is applied as seed treatment, foliar application, stem application, drench or drip application (chemigation) to the seed, the plant or to the fruit of the plant or to soil or to inert substrate (e.g. inorganic substrates like sand, rockwool, glasswool; expanded minerals like perlite, vermiculite, zeolite or expanded clay), Pumice. Pyroclastic materials or stuff, synthetic organic substrates (e.g. polyurethane) organic substrates (e.g. peat, composts, tree waste products like coir, wood fibre or chips, tree bark) or to a liquid substrate (e.g. floating hydroponic systems, Nutrient Film Technique, Aeroponics) wherein the plant is growing or wherein it is desired to grow.

The expression “are applied to the plants to be treated” is understood to mean, for the purposes of the present invention, that the pesticide composition which is the subject of the invention can be applied by means of various methods of treatment such as:

spraying onto the aerial parts of the said plants a liquid comprising one of the said compositions, dusting, the incorporation into the soil of granules or powders, spraying, around the said plants and in the case of trees injection or daubing, coating or film-coating the seeds of the said plants with the aid of a plant-protection mixture comprising one of the said compositions.

The method according to the invention can either be a curing, preventing or eradicating method. In this method, a composition used can be prepared beforehand by mixing the two or more active compounds according to the invention.

According to an alternative of such a method, it is also possible to apply simultaneously, successively or separately compounds (A) and (B) so as to have the conjugated (A)/(B) effects, of distinct compositions each containing one of the two or three active ingredients (A) or (B).

The dose of active compound usually applied in the method of treatment according to the invention is generally and advantageously

for foliar treatments: from 0.1 to 10,000 g/ha, preferably from 10 to 1,000 g/ha, more preferably from 50 to 300 g/ha; in case of drench or drip application, the dose can even be reduced, especially while using inert substrates like rockwool or perlite; for seed treatment: from 2 to 200 g per 100 kilogram of seed, preferably from 3 to 150 g per 100 kilogram of seed; for soil treatment: from 0.1 to 10,000 g/ha, preferably from 1 to 5,000 g/ha.

The doses herein indicated are given as illustrative Examples of method according to the invention. A person skilled in the art will know how to adapt the application doses, notably according to the nature of the plant or crop to be treated.

Under specific conditions, for example according to the nature of the phytopathogenic fungus to be treated or controlled, a lower dose can offer adequate protection. Certain climatic conditions, resistance or other factors like the nature of the phytopathogenic fungi or the degree of infestation, for example, of the plants with these fungi, can require higher doses of combined active ingredients. The optimum dose usually depends on several factors, for example on the type of phytopathogenic fungus to be treated, on the type or level of development of the infested plant, on the density of vegetation or alternatively on the method of application.

Without it being limiting, the crop treated with the pesticide composition or combination according to the invention is, for example, grapevine, but this could be cereals, vegetables, lucerne, soybean, market garden crops, turf, wood, tree or horticultural plants.

›CROSS-REFERENCE TO RELATED APPLICATION(S) · 9 of 15

The method of treatment according to the invention can also be useful to treat propagation material such as tubers or rhizomes, but also seeds, seedlings or seedlings pricking out and plants or plants pricking out. This method of treatment can also be useful to treat roots. The method of treatment according to the invention can also be useful to treat the over-ground parts of the plant such as trunks, stems or stalks, leaves, flowers and fruit of the concerned plant.

Among the plants that can be protected by the method according to the invention, mention can be made of cotton; flax; vine; fruit or vegetable crops such as Rosaceae sp. (for instance pip fruit such as apples and pears, but also stone fruit such as apricots, almonds and peaches). Ribesioidae sp., Juglandaceae sp., Betulaceae sp., Anacardiaceae sp., Fagaceae sp., Moraceae sp., Oleaceae sp., Actimidaceae sp., Lauraceae sp., Musaceae sp. (for instance banana trees and plantins). Rubiaceae sp., Theaceae sp., Sterculiceae sp., Rutaceae sp. (for instance lemons oranges and grapefruit); Solanaceae sp. (for instance tomatoes). Liliaceae sp., Asteraceae sp. (for instance lettuces). Umbelliferae sp., Cruciferae sp., Chenopodiaceae sp., Cucurbitaceae sp., Papilionaceae sp. (for instance peas). Rosaceae sp. (for instance strawberries); major crops such as Graminae sp. (for instance maize, lawn or cereals such as wheat, rice, barley and triticale). Asteraceae sp. (for instance sunflower). Cruciferae sp. (for instance colza). Fabacae sp. (for instance peanuts). Papilionaceae sp. (for instance soybean). Solanaceae sp. (for instance potatoes). Chenopodiaceae sp. (for instance beetroots); horticultural and forest crops; as well as genetically modified homologues of these crops.

The method of treatment according to the invention can be used in the treatment of genetically modified organisms (GMOs), e.g. plants or seeds. Genetically modified plants (or transgenic plants) are plants in which a heterologous gene has been stably integrated into the genome. The expression “heterologous gene” essentially means a gene which is provided or assembled outside the plant and when introduced in the nuclear, chloroplastic or mitochondrial genome gives the transformed plant new or improved agronomic or other properties by expressing a protein or polypeptide of interest or by downregulating or silencing other gene(s) which are present in the plant (using for example, antisense technology, co suppression technology or RNA interference—RNAi-technology). A heterologous gene that is located in the genome is also called a transgene. A transgene that is defined by its particular location in the plant genome is called a transformation or transgenic event.

Depending on the plant species or plant cultivars, their location and growth conditions (soils, climate, vegetation period, diet), the treatment according to the invention may also result in superadditive (“synergistic”) effects. Thus, for example, reduced application rates and/or a widening of the activity spectrum and/or an increase in the activity of the active compounds and compositions which can be used according to the invention, better plant growth, increased tolerance to high or low temperatures, increased tolerance to drought or to water or soil salt content, increased flowering performance, easier harvesting, accelerated maturation, higher harvest yields, bigger fruits, larger plant height, greener leaf color, earlier flowering, higher quality and/or a higher nutritional value of the harvested products, higher sugar concentration within the fruits, better storage stability and/or processability of the harvested products are possible, which exceed the effects which were actually to be expected.

At certain application rates, the active compound combinations according to the invention may also have a strengthening effect in plants. Accordingly, they are also suitable for mobilizing the defense system of the plant against attack by unwanted phytopathogenic fungi and/or microorganisms and/or viruses. This may, if appropriate, be one of the reasons of the enhanced activity of the combinations according to the invention, for example against fungi. Plant-strengthening (resistance-inducing) substances are to be understood as meaning, in the present context, those substances or combinations of substances which are capable of stimulating the defense system of plants in such a way that, when subsequently inoculated with unwanted phytopathogenic fungi and/or microorganisms and/or viruses, the treated plants display a substantial degree of resistance to these unwanted phytopathogenic fungi and/or microorganisms and/or viruses. In the present case, unwanted phytopathogenic fungi and/or microorganisms and/or viruses are to be understood as meaning phytopathogenic fungi, bacteria and viruses. Thus, the substances according to the invention can be employed for protecting plants against attack by the abovementioned pathogens within a certain period of time after the treatment. The period of time within which protection is effected generally extends from 1 to 10 days, preferably 1 to 7 days, after the treatment of the plants with the active compounds.

Plants and plant cultivars which are preferably to be treated according to the invention include all plants which have genetic material which impart particularly advantageous, useful traits to these plants (whether obtained by breeding and/or biotechnological means).

Plants and plant cultivars which are also preferably to be treated according to the invention are resistant against one or more biotic stresses, i.e. said plants show a better defense against animal and microbial pests, such as against nematodes, insects, mites, phytopathogenic fungi, bacteria, viruses and/or viroids.

Plants and plant cultivars which may also be treated according to the invention are those plants which are resistant to one or more abiotic stresses. Abiotic stress conditions may include, for example, drought, cold temperature exposure, heat exposure, osmotic stress, flooding, increased soil salinity, increased mineral exposure, ozon exposure, high light exposure, limited availability of nitrogen nutrients, limited availability of phosphorus nutrients, shade avoidance.

›CROSS-REFERENCE TO RELATED APPLICATION(S) · 10 of 15

Plants and plant cultivars which may also be treated according to the invention, are those plants characterized by enhanced yield characteristics. Increased yield in said plants can be the result of, for example, improved plant physiology, growth and development, such as water use efficiency, water retention efficiency, improved nitrogen use, enhanced carbon assimilation, improved photosynthesis, increased germination efficiency and accelerated maturation. Yield can furthermore be affected by improved plant architecture (under stress and non-stress conditions), including but not limited to, early flowering, flowering control for hybrid seed production, seedling vigor, plant size, internode number and distance, root growth, seed size, fruit size, pod size, pod or ear number, seed number per pod or ear, seed mass, enhanced seed filling, reduced seed dispersal, reduced pod dehiscence and lodging resistance. Further yield traits include seed composition, such as carbohydrate content, protein content, oil content and composition, nutritional value, reduction in anti-nutritional compounds, improved processability and better storage stability.

Plants that may be treated according to the invention are hybrid plants that already express the characteristic of heterosis or hybrid vigor which results in generally higher yield, vigor, health and resistance towards biotic and abiotic stress factors. Such plants are typically made by crossing an inbred male-sterile parent line (the female parent) with another inbred male-fertile parent line (the male parent). Hybrid seed is typically harvested from the male sterile plants and sold to growers. Male sterile plants can sometimes (e.g. in corn) be produced by detasseling, i.e. the mechanical removal of the male reproductive organs (or males flowers) but, more typically, male sterility is the result of genetic determinants in the plant genome. In that case, and especially when seed is the desired product to be harvested from the hybrid plants it is typically useful to ensure that male fertility in the hybrid plants is fully restored. This can be accomplished by ensuring that the male parents have appropriate fertility restorer genes which are capable of restoring the male fertility in hybrid plants that contain the genetic determinants responsible for male-sterility. Genetic determinants for male sterility may be located in the cytoplasm. Examples of cytoplasmic male sterility (CMS) were for instance described in Brassica species (W0 1992/005251, WO 1995/009910, WO 1998/27806, WO 2005/002324, WO 2006/021972 and U.S. Pat. No. 6,229,072). However, genetic determinants for male sterility can also be located in the nuclear genome. Male sterile plants can also be obtained by plant biotechnology methods such as genetic engineering. A particularly useful means of obtaining male-sterile plants is described in WO 1989/10396 in which, for example, a ribonuclease such as barnase is selectively expressed in the tapetum cells in the stamens. Fertility can then be restored by expression in the tapetum cells of a ribonuclease inhibitor such as barstar (e.g. WO 1991/002069).

Plants or plant cultivars (obtained by plant biotechnology methods such as genetic engineering) which may be treated according to the invention are herbicide-tolerant plants, i.e. plants made tolerant to one or more given herbicides. Such plants can be obtained either by genetic transformation, or by selection of plants containing a mutation imparting such herbicide tolerance.

Herbicide-tolerant plants are for example glyphosate-tolerant plants, i.e. plants made tolerant to the herbicide glyphosate or salts thereof. Plants can be made tolerant to glyphosate through different means. For example, glyphosate-tolerant plants can be obtained by transforming the plant with a gene encoding the enzyme 5-enolpyruvylshikimate-3-phosphate synthase (EPSPS). Examples of such EPSPS genes are the AroA gene (mutant CT7) of the bacterium Salmonella typhimurium (Comai at al., Science (1983), 221, 370-371), the CP4 gene of the bacterium Agrobacterium sp. (Barry et al., Curr. Topics Plant Physiol. (1992), 7, 139-145), the genes encoding a Petunia EPSPS (Shah et al., Science (1986), 233, 478-481), a Tomato EPSPS (Gasser et al., J. Biol. Chem. (1988), 263, 4280-4289), or an Eleusine EPSPS (WO 2001/66704). It can also be a mutated EPSPS as described in for example EP-A0837044. WO 2000/066746, WO 2000/066747 or WO 2002/026995. Glyphosate-tolerant plants can also be obtained by expressing a gene that encodes a glyphosate oxido-reductase enzyme as described in U.S. Pat. No. 5,776,760 and U.S. Pat. No. 5,463,175. Glyphosate-tolerant plants can also be obtained by expressing a gene that encodes a glyphosate acetyl transferase enzyme as described in for example WO 2002/036782, WO 2003/092360, WO 2005/012515 and WO 2007/024782. Glyphosate-tolerant plants can also be obtained by selecting plants containing naturally-occurring mutations of the above-mentioned genes, as described in for example WO 2001/024615 or WO 2003/013226.

Other herbicide resistant plants are for example plants that are made tolerant to herbicides inhibiting the enzyme glutamine synthase, such as bialaphos, phosphinothricin or glufosinate. Such plants can be obtained by expressing an enzyme detoxifying the herbicide or a mutant glutamine synthase enzyme that is resistant to inhibition. One such efficient detoxifying enzyme is an enzyme encoding a phosphinothricin acetyltransferase (such as the bar or pat protein from Streptomyces species). Plants expressing an exogenous phosphinothricin acetyltransferase are for example described in U.S. Pat. No. 5,561,236; U.S. Pat. No. 5,648,477; U.S. Pat. No. 5,646,024; U.S. Pat. No. 5,273,894; U.S. Pat. No. 5,637,489; U.S. Pat. No. 5,276,268; U.S. Pat. No. 5,739,082; U.S. Pat. No. 5,908,810 and U.S. Pat. No. 7,112,665.

Further herbicide-tolerant plants are also plants that are made tolerant to the herbicides inhibiting the enzyme hydroxyphenylpyruvatedioxygenase (HPPD). Hydroxyphenylpyruvatedioxygenases are enzymes that catalyze the reaction in which para-hydroxyphenylpyruvate (HPP) is transformed into homogentisate. Plants tolerant to HPPD-inhibitors can be transformed with a gene encoding a naturally-occurring resistant HPPD enzyme, or a gene encoding a mutated HPPD enzyme as described in WO 1996/038567, WO 1999/024585 and WO 1999/024586. Tolerance to HPPD-inhibitors can also be obtained by transforming plants with genes encoding certain enzymes enabling the formation of homogentisate despite the inhibition of the native HPPD enzyme by the HPPD-inhibitor. Such plants and genes are described in WO 1999/034008 and WO 2002/36787. Tolerance of plants to HPPD inhibitors can also be improved by transforming plants with a gene encoding an enzyme prephenate dehydrogenase in addition to a gene encoding an HPPD-tolerant enzyme, as described in WO 2004/024928.

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Still further herbicide resistant plants are plants that are made tolerant to acetolactate synthase (ALS) inhibitors. Known ALS-inhibitors include, for example, sulfonylurea, imidazolinone, triazolopyrimidines, pyrimidinyloxy(thio)benzoates, and/or sulfonylaminocarbonyltriazolinone herbicides. Different mutations in the ALS enzyme (also known as acetohydroxyacid synthase, AHAS) are known to confer tolerance to different herbicides and groups of herbicides, as described for example in Tranel and Wright, Weed Science (2002), 50, 700-712, but also, in U.S. Pat. No. 5,605,011, U.S. Pat. No. 5,378,824, U.S. Pat. No. 5,141,870, and U.S. Pat. No. 5,013,659. The production of sulfonylurea-tolerant plants and imidazolinone-tolerant plants is described in U.S. Pat. No. 5,605,011; U.S. Pat. No. 5,013,659; U.S. Pat. No. 5,141,870; U.S. Pat. No. 5,767,361; U.S. Pat. No. 5,731,180; U.S. Pat. No. 5,304,732; U.S. Pat. No. 4,761,373; U.S. Pat. No. 5,331,107; U.S. Pat. No. 5,928,937; and U.S. Pat. No. 5,378,824; and international publication WO 1996/033270. Other imidazolinone-tolerant plants are also described in for example WO 2004/040012, WO 2004/106529, WO 2005/020673, WO 2005/093093, WO 2006/007373, WO 2006/015376, WO 2006/024351, and WO 2006/060634. Further sulfonylurea- and imidazolinone-tolerant plants are also described in for example WO 2007/024782.

Other plants tolerant to imidazolinone and/or sulfonylurea can be obtained by induced mutagenesis, selection in cell cultures in the presence of the herbicide or mutation breeding as described for example for soybeans in U.S. Pat. No. 5,084,082, for rice in WO 1997/41218, for sugar beet in U.S. Pat. No. 5,773,702 and WO 1999/057965, for lettuce in U.S. Pat. No. 5,198,599, or for sunflower in WO 2001/065922.

Plants or plant cultivars (obtained by plant biotechnology methods such as genetic engineering) which may also be treated according to the invention are insect-resistant transgenic plants, i.e. plants made resistant to attack by certain target insects. Such plants can be obtained by genetic transformation, or by selection of plants containing a mutation imparting such insect resistance.

An “insect-resistant transgenic plant”, as used herein, includes any plant containing at least one transgene comprising a coding sequence encoding:

1) an insecticidal crystal protein from Bacillus thuringiensis or an insecticidal portion thereof, such as the insecticidal crystal proteins listed by Crickmore et al., Microbiology and Molecular Biology Reviews (1998), 62, 807-813, updated by Crickmore et al. (2005) at the Bacillus thuringiensis toxin nomenclature, online at: http://www.lifesci.sussex.ac.uk/Home/Neil_Crickmore/Bt/), or insecticidal portions thereof, e.g., proteins of the Cry protein classes Cry1Ab, Cry1Ac, Cry1F, Cry2Ab, Cry3Aa, or Cry3Bb or insecticidal portions thereof; or 2) a crystal protein from Bacillus thuringiensis or a portion thereof which is insecticidal in the presence of a second other crystal protein from Bacillus thuringiensis or a portion thereof, such as the binary toxin made up of the Cry34 and Cry35 crystal proteins (Moellenbeck et al., Nat. Biotechnol. (2001), 19, 668-72; Schnepf et al., Applied Environm. Microbiol. (2006), 71, 1765-1774); or 3) a hybrid insecticidal protein comprising parts of different insecticidal crystal proteins from Bacillus thuringiensis , such as a hybrid of the proteins of 1) above or a hybrid of the proteins of 2) above, e.g., the Cry1A.105 protein produced by corn event MON98034 (WO 2007/027777); or 4) a protein of any one of 1) to 3) above wherein some, particularly 1 to 10, amino acids have been replaced by another amino acid to obtain a higher insecticidal activity to a target insect species, and/or to expand the range of target insect species affected, and/or because of changes introduced into the encoding DNA during cloning or transformation, such as the Cry3Bb1 protein in corn events MON863 or MON88017, or the Cry3A protein in corn event MIR604; 5) an insecticidal secreted protein from Bacillus thuringiensis or Bacillus cereus , or an insecticidal portion thereof, such as the vegetative insecticidal (VIP) proteins listed at: http://www.lifesci.sussex.ac.uk/home/Neil_Crickmore/Bt/vip.html, e.g., proteins from the VIP3Aa protein class; or 6) a secreted protein from Bacillus thuringiensis or Bacillus cereus which is insecticidal in the presence of a second secreted protein from Bacillus thuringiensis or B. cereus , such as the binary toxin made up of the VIP1A and VIP2A proteins (WO 1994/21795); or 7) a hybrid insecticidal protein comprising parts from different secreted proteins from Bacillus thuringiensis or Bacillus cereus , such as a hybrid of the proteins in 1) above or a hybrid of the proteins in 2) above; or 8) a protein of any one of 1) to 3) above wherein some, particularly 1 to 10, amino acids have been replaced by another amino acid to obtain a higher insecticidal activity to a target insect species, and/or to expand the range of target insect species affected, and/or because of changes introduced into the encoding DNA during cloning or transformation (while still encoding an insecticidal protein), such as the VIP3Aa protein in cotton event COT102.

Of course, an insect-resistant transgenic plant, as used herein, also includes any plant comprising a combination of genes encoding the proteins of any one of the above classes 1 to 8. In one embodiment, an insect-resistant plant contains more than one transgene encoding a protein of any one of the above classes 1 to 8, to expand the range of target insect species affected when using different proteins directed at different target insect species, or to delay insect resistance development to the plants by using different proteins insecticidal to the same target insect species but having a different mode of action, such as binding to different receptor binding sites in the insect.

Plants or plant cultivars (obtained by plant biotechnology methods such as genetic engineering) which may also be treated according to the invention are tolerant to abiotic stresses. Such plants can be obtained by genetic transformation, or by selection of plants containing a mutation imparting such stress resistance. Particularly useful stress tolerance plants include:

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a. plants which contain a transgene capable of reducing the expression and/or the activity of poly(ADP-ribose)polymerase (PARP) gene in the plant cells or plants as described in WO 2000/004173 or WO2006/045633 or PCT/EP07/004142. b. plants which contain a stress tolerance enhancing transgene capable of reducing the expression and/or the activity of the PARG encoding genes of the plants or plants cells, as described e.g. in WO 2004/090140. c. plants which contain a stress tolerance enhancing transgene coding for a plant-functional enzyme of the nicotinamide adenine dinucleotide salvage synthesis pathway including nicotinamidase, nicotinate phosphoribosyltransferase, nicotinic acid mononucleotide adenyl transferase, nicotinamide adenine dinucleotide synthetase or nicotine amide phosphoribosyltransferase as described e.g. in WO2006/032469 or WO 2006/133827 or PCT/EP07/002,433.

Plants or plant cultivars (obtained by plant biotechnology methods such as genetic engineering) which may also be treated according to the invention show altered quantity, quality and/or storage-stability of the harvested product and/or altered properties of specific ingredients of the harvested product such as:

1) transgenic plants which synthesize a modified starch, which in its physical-chemical characteristics, in particular the amylase content or the amylose/amylopectin ratio, the degree of branching, the average chain length, the side chain distribution, the viscosity behaviour, the gelling strength, the starch grain size and/or the starch grain morphology, is changed in comparison with the synthesised starch in wild type plant cells or plants, so that this is better suited for special applications. Said transgenic plants synthesizing a modified starch are disclosed, for example, in EP 0571427, WO 1995/004826, EP 0719338, WO 1996/15248, WO 1996/19581, WO 1996/27674, WO 1997/11188, WO 1997/26362, WO 1997/32985, WO 1997/42328, WO 1997/44472, WO 1997/45545, WO 1998/27212, WO 1998/40503, WO99/58688, WO 1999/58690, WO 1999/58654, WO 2000/008184, WO 2000/008185, WO 2000/008175, WO 2000/28052, WO 2000/77229, WO 2001/12782, WO 2001/12826, WO 2002/101059, WO 2003/071860, WO 2004/056999, WO 2005/030942, WO 2005/030941, WO 2005/095632, WO 2005/095617, WO 2005/095619, WO 2005/095618, WO 2005/123927, WO 2006/018319, WO 2006/103107, WO 2006/108702, WO 2007/009823, WO 2000/22140, WO 2006/063862, WO 2006/072603, WO 2002/034923, EP 06090134.5, EP 06090228.5, EP 06090227.7, EP 07090007.1, EP 07090009.7, WO 2001/14569, WO 2002/79410, WO 2003/33540, WO 2004/078983, WO 2001/19975, WO 1995/26407, WO 1996/34968, WO 1998/20145, WO 1999/12950, WO 1999/66050, WO 1999/53072, U.S. Pat. No. 6,734,341, WO 2000/11192, WO 1998/22604, WO 1998/32326, WO 2001/98509, WO 2001/98509, WO 2005/002359, U.S. Pat. No. 5,824,790, U.S. Pat. No. 6,013,861, WO 1994/004693, WO 1994/009144, WO 1994/11520, WO 1995/35026, WO 1997/20936. 2) transgenic plants which synthesize non starch carbohydrate polymers or which synthesize non starch carbohydrate polymers with altered properties in comparison to wild type plants without genetic modification. Examples are plants producing polyfructose, especially of the inulin and levan-type, as disclosed in EP 0663956, WO 1996/001904, WO 1996/021023, WO 1998/039460, and WO 1999/024593, plants producing alpha 1,4 glucans as disclosed in WO 1995/031553, US 2002/031826, U.S. Pat. No. 6,284,479, U.S. Pat. No. 5,712,107, WO 1997/047806, WO 1997/047807, WO 1997/047808 and WO 2000/014249, plants producing alpha-1,6 branched alpha-1,4-glucans, as disclosed in WO 2000/73422, plants producing alternan, as disclosed in WO 2000/047727, EP 06077301.7, U.S. Pat. No. 5,908,975 and EP 0728213, 3) transgenic plants which produce hyaluronan, as for example disclosed in WO 2006/032538, WO 2007/039314, WO 2007/039315, WO 2007/039316, JP 2006/304779, and WO 2005/012529.

a) Plants, such as cotton plants, containing an altered form of cellulose synthase genes as described in WO 1998/000549 b) Plants, such as cotton plants, containing an altered form of rsw2 or rsw3 homologous nucleic acids as described in WO2004/053219 c) Plants, such as cotton plants, with increased expression of sucrose phosphate synthase as described in WO 2001/017333 d) Plants, such as cotton plants, with increased expression of sucrose synthase as described in WO02/45485 e) Plants, such as cotton plants, wherein the timing of the plasmodesmatal gating at the basis of the fiber cell is altered, e.g. through downregulation of fiberselective β 1,3-glucanase as described in WO2005/017157 f) Plants, such as cotton plants, having fibers with altered reactivity, e.g. through the expression of N-acteylglucosaminetransferase gene including nodC and chitinsynthase genes as described in WO2006/136351

Plants or plant cultivars (that can be obtained by plant biotechnology methods such as genetic engineering) which may also be treated according to the invention are plants, such as oilseed rape or related Brassica plants, with altered oil profile characteristics. Such plants can be obtained by genetic transformation or by selection of plants contain a mutation imparting such altered oil characteristics and include:

a) Plants, such as oilseed rape plants, producing oil having a high oleic acid content as described e.g. in U.S. Pat. No. 5,969,169, U.S. Pat. No. 5,840,946 or U.S. Pat. No. 6,323,392 or U.S. Pat. No. 6,063,947 b) Plants such as oilseed rape plants, producing oil having a low linolenic acid content as described in U.S. Pat. No. 6,270,828, U.S. Pat. No. 6,169,190 or U.S. Pat. No. 5,965,755 c) Plant such as oilseed rape plants, producing oil having a low level of saturated fatty acids as described e.g. in U.S. Pat. No. 5,434,283 or U.S. patent application Ser. No. 12/668,303

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Plants or plant cultivars (that can be obtained by plant biotechnology methods such as genetic engineering) which may also be treated according to the invention are plants, such as oilseed rape or related Brassica plants, with altered seed shattering characteristics. Such plants can be obtained by genetic transformation, or by selection of plants contain a mutation imparting such altered seed shattering characteristics and include plants such as oilseed rape plants with delayed or reduced seed shattering as described in U.S. Patent Application 61/135,230, WO 2009/068313 and WO 2010/006732.

Plants or plant cultivars (that can be obtained by plant biotechnology methods such as genetic engineering) which may also be treated according to the invention are plants, such as Tobacco plants, with altered post-translational protein modification patterns, for example as described in WO 2010/121818 and WO 2010/145846.

Particularly useful transgenic plants which may be treated according to the invention are plants containing transformation events, or combination of transformation events, that are the subject of petitions for non-regulated status, in the United States of America, to the Animal and Plant Health Inspection Service (APHIS) of the United States Department of Agriculture (USDA) whether such petitions are granted or are still pending. At any time this information is readily available from APHIS (4700 River Road, Riverdale, Md. 20737, USA), for instance on its internet site (URL http://www.aphis.usda.gov/brs/not_reg.html). On the filing date of this application the petitions for nonregulated status that were pending with APHIS or granted by APHIS were those which contains the following information:

Petition: the identification number of the petition. Technical descriptions of the transformation events can be found in the individual petition documents which are obtainable from APHIS, for example on the APHIS website, by reference to this petition number. These descriptions are herein incorporated by reference. Extension of Petition: reference to a previous petition for which an extension is requested. Institution: the name of the entity submitting the petition. Regulated article: the plant species concerned. Transgenic phenotype: the trait conferred to the plants by the transformation event. Transformation event or line: the name of the event or events (sometimes also designated as lines or lines) for which nonregulated status is requested. APHIS documents: various documents published by APHIS in relation to the Petition and which can be requested with APHIS.

Additional particularly useful plants containing single transformation events or combinations of transformation events are listed for example in the databases from various national or regional regulatory agencies (see for example http://gmoinfo.jrc.it/gmp browse.aspx and http://www.agbios.com/dbase.php).

Particularly useful transgenic plants which may be treated according to the invention are plants containing transformation events, or a combination of transformation events, and that are listed for example in the databases for various national or regional regulatory agencies including Event 1143-14A (cotton, insect control, not deposited, described in WO 2006/128569); Event 1143-51B (cotton, insect control, not deposited, described in WO 2006/128570); Event 1445 (cotton, herbicide tolerance, not deposited, described in US-A 2002-120964 or WO 02/034946); Event 17053 (rice, herbicide tolerance, deposited as PTA-9843, described in WO 2010/117737); Event 17314 (rice, herbicide tolerance, deposited as PTA-9844, described in WO 2010/117735); Event 281-24-236 (cotton, insect control—herbicide tolerance, deposited as PTA-6233, described in WO 2005/103266 or US-A 2005-216969); Event 3006-210-23 (cotton, insect control-herbicide tolerance, deposited as PTA-6233, described in US-A 2007-143876 or WO 2005/103266); Event 3272 (corn, quality trait, deposited as PTA-9972, described in WO 2006/098952 or US-A 2006-230473); Event 40416 (corn, insect control-herbicide tolerance, deposited as ATCC PTA-11508, described in WO 2011/075593); Event 43A47 (corn, insect control-herbicide tolerance, deposited as ATCC PTA-11509, described in WO 2011/075595); Event 5307 (corn, insect control, deposited as ATCC PTA-9561, described in WO 2010/077816); Event ASR-368 (bent grass, herbicide tolerance, deposited as ATCC PTA-4816, described in US-A 2006-162007 or WO 2004/053062); Event B16 (corn, herbicide tolerance, not deposited, described in US-A 2003-126634); Event BPS-CV127-9 (soybean, herbicide tolerance, deposited as NCIMB No. 41603, described in WO 2010/080829); Event CE43-67B (cotton, insect control, deposited as DSM ACC2724, described in US-A 2009-217423 or WO2006/128573); Event CE44-69D (cotton, insect control, not deposited, described in US-A 2010-0024077); Event CE44-69D (cotton, insect control, not deposited, described in WO 2006/128571); Event CE46-02A (cotton, insect control, not deposited, described in WO 2006/128572); Event COT102 (cotton, insect control, not deposited, described in US-A 2006-130175 or WO 2004/039986); Event COT202 (cotton, insect control, not deposited, described in US-A 2007-067868 or WO 2005/054479); Event COT203 (cotton, insect control, not deposited, described in WO 2005/054480); Event DAS40278 (corn, herbicide tolerance, deposited as ATCC PTA-10244, described in WO 2011/022469); Event DAS-59122-7 (corn, insect control-herbicide tolerance, deposited as ATCC PTA 11384, described in US-A 2006-070139); Event DAS-59132 (corn, insect control-herbicide tolerance, not deposited, described in WO 2009/100188); Event DAS68416 (soybean, herbicide tolerance, deposited as ATCC PTA-10442, described in WO 2011/066384 or WO 2011/066360); Event DP-098140-6 (corn, herbicide tolerance, deposited as ATCC PTA-8296, described in US-A 2009-137395 or WO 2008/112019); Event DP-305423-1 (soybean, quality trait, not deposited, described in US-A 2008-312082 or WO 2008/054747); Event DP-32138-1 (corn, hybridization system, deposited as ATCC PTA-9158, described in US-A 2009-0210970 or WO 2009/103049); Event DP-356043-5 (soybean, herbicide tolerance, deposited as ATCC PTA-8287, described in US-A 2010-0184079 or WO 2008/002872); Event EE-1 (brinjal, insect control, not deposited, described in WO 2007/091277); Event F1117 (corn, herbicide tolerance, deposited as ATCC 209031, described in US-A 2006-059581 or WO 98/044140); Event GA21 (corn, herbicide tolerance, deposited as ATCC 209033, described in US-A 2005-086719 or WO 98/044140); Event GG25 (corn, herbicide tolerance, deposited as ATCC 209032, described in US-A 2005-188434 or WO 98/044140); Event GHB119 (cotton, insect control-herbicide tolerance, deposited as ATCC PTA-8398, described in WO 2008/151780); Event GHB614 (cotton, herbicide tolerance, deposited as ATCC PTA-6878, described in US-A 2010-050282 or WO 2007/017186); Event GJ11 (corn, herbicide tolerance, deposited as ATCC 209030, described in US-A 2005-188434 or WO 98/044140); Event GM RZ13 (sugar beet, virus resistance, deposited as NCIMB-41601, described in WO 2010/076212); Event H7-1 (sugar beet, herbicide tolerance, deposited as NCIMB 41158 or NCIMB 41159, described in US-A 2004-172669 or WO 2004/074492); Event JOPLIN1 (wheat, disease tolerance, not deposited, described in US-A 2008-064032); Event LL27 (soybean, herbicide tolerance, deposited as NCIMB41658, described in WO 2006/108674 or US-A 2008-320616); Event LL55 (soybean, herbicide tolerance, deposited as NCIMB 41660, described in WO 2006/108675 or US-A 2008-196127); Event LLcotton25 (cotton, herbicide tolerance, deposited as ATCC PTA-3343, described in WO 03/013224 or US-A 2003-097687); Event LLRICE06 (rice, herbicide tolerance, deposited as ATCC-23352, described in U.S. Pat. No. 6,468,747 or WO 00/026345); Event LLRICE601 (rice, herbicide tolerance, deposited as ATCC PTA-2600, described in US-A 2008-2289060 or WO 00/026356); Event LY038 (corn, quality trait, deposited as ATCC PTA-5623, described in US-A 2007-028322 or WO 2005/061720); Event MIR162 (corn, insect control, deposited as PTA-8166, described in US-A 2009-300784 or WO 2007/142840); Event MIR604 (corn, insect control, not deposited, described in US-A 2008-167456 or WO 2005/103301); Event MON15985 (cotton, insect control, deposited as ATCC PTA-2516, described in US-A 2004-250317 or WO 02/100163); Event MON810 (corn, insect control, not deposited, described in US-A 2002-102582); Event MON863 (corn, insect control, deposited as ATCC PTA-2605, described in WO 2004/011601 or US-A 2006-095986); Event MON87427 (corn, pollination control, deposited as ATCC PTA-7899, described in WO 2011/062904); Event MON87460 (corn, stress tolerance, deposited as ATCC PTA-8910, described in WO 2009/111263 or US-A 2011-0138504); Event MON87701 (soybean, insect control, deposited as ATCC PTA-8194, described in US-A 2009-130071 or WO 2009/064652); Event MON87705 (soybean, quality trait-herbicide tolerance, deposited as ATCC PTA-9241, described in US-A 2010-0080887 or WO 2010/037016); Event MON87708 (soybean, herbicide tolerance, deposited as ATCC PTA9670, described in WO 2011/034704); Event MON87754 (soybean, quality trait, deposited as ATCC PTA-9385, described in WO 2010/024976); Event MON87769 (soybean, quality trait, deposited as ATCC PTA-8911, described in US-A 2011-0067141 or WO 2009/102873); Event MON88017 (corn, insect control-herbicide tolerance, deposited as ATCC PTA-5582, described in US-A 2008-028482 or WO 2005/059103); Event MON88913 (cotton, herbicide tolerance, deposited as ATCC PTA-4854, described in WO 2004/072235 or US-A 2006-059590); Event MON89034 (corn, insect control, deposited as ATCC PTA-7455, described in WO 2007/140256 or US-A 2008-260932); Event MON89788 (soybean, herbicide tolerance, deposited as ATCC PTA-6708, described in US-A 2006-282915 or WO 2006/130436); Event MS11 (oilseed rape, pollination control-herbicide tolerance, deposited as ATCC PTA-850 or PTA-2485, described in WO 01/031042); Event MS8 (oilseed rape, pollination control-herbicide tolerance, deposited as ATCC PTA-730, described in WO 01/041558 or US-A 2003-188347); Event NK603 (corn, herbicide tolerance, deposited as ATCC PTA-2478, described in US-A 2007-292854); Event PE-7 (rice, insect control, not deposited, described in WO 2008/114282); Event RF3 (oilseed rape, pollination control-herbicide tolerance, deposited as ATCC PTA-730, described in WO 01/041558 or US-A 2003-188347); Event RT73 (oilseed rape, herbicide tolerance, not deposited, described in WO 02/036831 or US-A 2008-070260); Event T227-1 (sugar beet, herbicide tolerance, not deposited, described in WO 02/44407 or US-A 2009-265817); Event T25 (corn, herbicide tolerance, not deposited, described in US-A 2001-029014 or WO 01/051654); Event T304-40 (cotton, insect control-herbicide tolerance, deposited as ATCC PTA-8171, described in US-A 2010-077501 or WO 2008/122406); Event T342-142 (cotton, insect control, not deposited, described in WO 2006/128568); Event TC1507 (corn, insect control-herbicide tolerance, not deposited, described in US-A 2005-039226 or WO 2004/099447); Event VIP1034 (corn, insect control-herbicide tolerance, deposited as ATCC PTA-3925, described in WO 03/052073), Event 32316 (corn, insect control-herbicide tolerance, deposited as PTA-11507, described in WO 2011/084632), Event 4114 (corn, insect control-herbicide tolerance, deposited as PTA-11506, described in WO 2011/084621).

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The composition according to the invention can also be used against fungal diseases liable to grow on or inside timber. The term “timber” means all types of species of wood and all types of working of this wood intended for construction, for example solid wood, high-density wood, laminated wood and plywood. The method for treating timber according to the invention mainly consists in contacting one or more compounds according to the invention or a composition according to the invention; this includes for example direct application, spraying, dipping, injection or any other suitable means.

Among the diseases of plants or crops that can be controlled by the method according to the invention, mention can be made of:

Powdery mildew diseases such as:

Blumeria diseases, caused for example by Blumeria graminis; Podosphaera diseases, caused for example by Podosphaera leucotricha; Sphaerotheca diseases, caused for example by Sphaerotheca fuliginea; Uncinula diseases, caused for example by Uncinula necator;

Rust diseases such as:

Gymnosporangium diseases, caused for example by Gymnosporangium sabinae; Hemileia diseases, caused for example by Hemileia vastatrix; Phakopsora diseases, caused for example by Phakopsora pachyrhizi or Phakopsora meibomiae; Puccinia diseases, caused for example by Puccinia recondita; Uromyces diseases, caused for example by Uromyces appendiculatus;

Oomycete diseases such as:

Bremia diseases, caused for example by Bremia lactucae; Peronospora diseases, caused for example by Peronospora pisi or P. brassicae; Phytophthora diseases, caused for example by Phytophthora infestans; Plasmopara diseases, caused for example by Plasmopara viticola; Pseudoperonospora diseases, caused for example by Pseudoperonospora humuli or Pseudoperonospora cubensis; Pythium diseases, caused for example by Pythium ultimum;

Leafspot, leaf blotch and leaf blight diseases such as:

Alternaria diseases, caused for example by Alternaria solani; Cercospora diseases, caused for example by Cercospora beticola; Cladiosporum diseases, caused for example by Cladiosporium cucumerinum; Cochliobolus diseases, caused for example by Cochliobolus sativus; Colletotrichum diseases, caused for example by Colletotrichum lindemuthanium; Cycloconium diseases, caused for example by Cycloconium oleaginum; Diaporthe diseases, caused for example by Diaporthe citri; Elsinoe diseases, caused for example by Elsinoe fawcettii; Gloeosporium diseases, caused for example by Gloeosporium laeticolor; Glomerella diseases, caused for example by Glomerella cingulata; Guignardia diseases, caused for example by Guignardia bidwelli; Leptosphaeria diseases, caused for example by Leptosphaeria maculans; Leptosphaeria nodorum; Magnaporthe diseases, caused for example by Magnaporthe grisea; Mycosphaerella diseases, caused for example by Mycosphaerella graminicola; Mycosphaerella arachidicola; Mycosphaerella fijiensis; Phaeosphaeria diseases, caused for example by Phaeosphaeria nodorum; Pyrenophora diseases, caused for example by Pyrenophora teres; Ramularia diseases, caused for example by Ramularia collo - cygni; Rhynchosporium diseases, caused for example by Rhynchosporium secalis; Septoria diseases, caused for example by Septoria apii or Septoria lycopercisi; Typhula diseases, caused for example by Typhula incamata; Venturia diseases, caused for example by Venturia inaequalis;

Root and stem diseases such as:

Corticium diseases, caused for example by Corticium graminearum; Fusarium diseases, caused for example by Fusarium oxysporum; Gaeumannomyces diseases, caused for example by Gaeumannomyces graminis; Rhizoctonia diseases, caused for example by Rhizoctonia solani; Tapesia diseases, caused for example by Tapesia acuformis; Thielaviopsis diseases, caused for example by Thielaviopsis basicola;

Ear and panicle diseases such as:

Alternaria diseases, caused for example by Alternaria spp.; Aspergillus diseases, caused for example by Aspergillus flavus; Cladosporium diseases, caused for example by Cladosporium spp.; Claviceps diseases, caused for example by Claviceps purpurea; Fusarium diseases, caused for example by Fusarium culmorum; Gibberella diseases, caused for example by Gibberella zeae; Monographella diseases, caused for example by Monographella nivalis;

Smut and bunt diseases such as:

Sphacelotheca diseases, caused for example by Sphacelotheca reiliana; Tilletia diseases, caused for example by Tilletia caries; Urocystis diseases, caused for example by Urocystis occulta; Ustilago diseases, caused for example by Ustilago nuda;

Fruit rot and mould diseases such as:

Aspergillus diseases, caused for example by Aspergillus flavus; Botrytis diseases, caused for example by Botrytis cinerea; Penicillium diseases, caused for example by Penicillium expansum; Sclerotinia diseases, caused for example by Sclerotinia sclerotiorum; Verticilium diseases, caused for example by Verticilium alboatrum;

Seed and soilborne decay, mould, wilt, rot and damping-off diseases:

Alternaria diseases, caused for example by Altemaria brassicicola Aphanomyces diseases, caused for example by Aphanomyces euteiches Ascochyta diseases, caused for example by Ascochyta lentis Aspergillus diseases, caused for example by Aspergillus flavus Cladosporium diseases, caused for example by Cladosporium herbarum Cochliobolus diseases, caused for example by Cochliobolus sativus (Conidiaform: Drechslera, Bipolaris Syn: Helminthosporium ); Colletotrichum diseases, caused for example by Colletotrichum coccodes; Fusarium diseases, caused for example by Fusarium culmorum; Gibberella diseases, caused for example by Gibberella zeae; Macrophomina diseases, caused for example by Macrophomina phaseolina Monographella diseases, caused for example by Monographella nivalis; Penicillium diseases, caused for example by Penicillium expansum Phoma diseases, caused for example by Phoma lingam Phomopsis diseases, caused for example by Phomopsis sojae; Phytophthora diseases, caused for example by Phytophthora cactorum; Pyrenophora diseases, caused for example by Pyrenophora graminea Pyricularia diseases, caused for example by Pyricularia oryzae; Pythium diseases, caused for example by Pythium ultimum; Rhizoctonia diseases, caused for example by Rhizoctonia solani; Rhizopus diseases, caused for example by Rhizopus oryzae Sclerotium diseases, caused for example by Sclerotium rolfsii; Septoria diseases, caused for example by Septoria nodorum; Typhula diseases, caused for example by Typhula incamata; Verticillium diseases, caused for example by Verticillium dahliae;

›CROSS-REFERENCE TO RELATED APPLICATION(S) · 15 of 15

Canker, broom and dieback diseases such as:

Nectria diseases, caused for example by Nectria galligena;

Blight diseases such as:

Monilinia diseases, caused for example by Monilinia laxa;

Leaf blister or leaf curl diseases such as:

Taphrina diseases, caused for example by Taphrina deformans;

Decline diseases of wooden plants such as:

Esca diseases, caused for example by Phaemoniella clamydospora; Eutypa dyeback, caused for example by Eutypa lata; Dutch elm disease, caused for example by Ceratocystsc ulmi;

Diseases of flowers and Seeds such as:

Botrytis diseases, caused for example by Botrytis cinerea;

Diseases of tubers such as:

Rhizoctonia diseases, caused for example by Rhizoctonia solani Helminthosporium diseases, caused for example by Helminthosporium solani.

The compounds according to the invention can also be used for the preparation of composition useful to curatively or preventively treat human or animal fungal diseases such as, for example, mycoses, dermatoses, trichophyton diseases and candidiases or diseases caused by Aspergillus spp., for example Aspergillus fumigatus.

The various aspects of the invention will now be illustrated with reference to the following table 1 of compound examples and the following preparation or efficacy examples.

The following table 1 illustrates in a non limiting manner examples of compounds according to the invention.

In table 1 we use the following abbreviations for specified claimed elements “A1” and “A2” of the generic structure (I) of the invention:

We describe the double bond geometry of the examples of table 1 as shown here:

I (E)

I (Z)

I (U)

Measurement of log P values was performed according EEC directive 79/831 Annex V.A8 by HPLC (High Performance Liquid Chromatography) on reversed phase columns with the following methods: [a] Measurement of LC-MS was done at pH 2.7 with 0.1% formic acid in water and with acetonitrile (contains 0.1% formic acid) as eluent with a linear gradient from 10% acetonitrile to 95% acetonitrile. Calibration was done with not branched alkan2-ones (with 3 to 16 carbon atoms) with known log P-values (measurement of log P values using retention times with linear interpolation between successive alkanones). lambda-maX-values were determined using UV-spectra from 200 nm to 400 nm and the peak values of the chromatographic signals.

NMR-Peak Lists

1H-NMR data of selected examples are written in form of 1H-NMR-peak lists. To each signal peak are listed the δ-value in ppm and the signal intensity in round brackets. Between the δ-value-signal intensity pairs are semicolons as delimiters.

The peak list of an example has therefore the form:

δ 1 (intensity 1 ); δ 2 (intensity 2 ); . . . ; δ i (intensity i ); . . . ; δ n (intensity n )

NMR Peak List Table 1

›Examples426

›Example 1, Solvent: DMSO, Spectrometer: 499.93 MHz

7.7706 (0.59); 7.7438 (4.33); 7.7288 (4.77); 7.5449 (0.82); 7.5304 (2.27); 7.5160 (2.14); 7.4914 (3.65); 7.4760 (4.63); 7.4616 (1.97); 7.4219

(0.60); 7.4140 (1.79); 7.4072 (1.18); 7.3987 (2.87); 7.3831 (1.80); 6.5450 (2.86); 6.5306 (2.81); 6.4357 (2.85); 6.4192 (2.83); 6.0594 (6.23);

5.7816 (0.67); 5.2149 (9.25); 3.8061 (2.02); 3.4478 (3.34); 3.1218 (16.00); 2.5112 (0.36); 1.9897 (0.98); 1.1684 (0.52)

›Example 2, Solvent: DMSO, Spectrometer: 499.93 MHz

10.1848 (2.68); 7.8340 (0.41); 7.8171 (2.04); 7.8092 (2.38); 7.8049 (4.86); 7.7925 (0.52); 7.7304 (2.61); 7.7200 (0.87); 7.7161 (3.25); 7.7132

(2.46); 7.5673 (0.55); 7.5649 (0.37); 7.5570 (0.44); 7.5526 (1.61); 7.5485 (0.57); 7.5404 (0.83); 7.5379 (1.32); 7.5354 (0.74); 7.5019 (2.27);

7.4992 (1.12); 7.4945 (0.53); 7.4890 (1.84); 7.4864 (3.15); 7.4752 (0.60); 7.4720 (1.29); 7.4701 (0.87); 7.1088 (1.26); 7.1041 (1.26); 7.0969

(1.13); 7.0922 (1.23); 5.3400 (6.66); 4.1044 (2.03); 4.0909 (4.22); 4.0775 (2.01); 3.9490 (1.03); 3.3400 (81.74); 3.3162 (1.90); 3.0753 (16.00);

2.5194 (2.79); 2.5159 (5.86); 2.5123 (8.04); 2.5086 (5.91); 2.5051 (2.84); 1.6318 (0.90); 1.6267 (0.73); 1.6181 (1.44); 1.6095 (0.75); 1.6044

(1.04); 1.5907 (0.33); 1.3485 (1.15); 1.3403 (1.83); 1.3343 (3.86); 1.3274 (2.69); 1.3199 (2.61); 1.3080 (0.47); 0.9041 (1.80); 0.8992 (1.09);

0.8901 (4.83); 0.8758 (1.55); 0.7455 (0.48); 0.7313 (0.97); 0.7167 (0.46)

›Example 3, Solvent: DMSO, Spectrometer: 499.93 MHz

10.3221 (2.70); 7.8439 (0.69); 7.8271 (1.82); 7.8132 (2.25); 7.8065 (2.30); 7.8042 (2.59); 7.7899 (0.89); 7.7876 (0.69); 7.7313 (2.88); 7.7206

(0.96); 7.7168 (3.44); 7.7140 (2.62); 7.5687 (0.36); 7.5666 (0.59); 7.5643 (0.41); 7.5562 (0.49); 7.5518 (1.75); 7.5479 (0.61); 7.5395 (0.86);

7.5371 (1.36); 7.5348 (0.79); 7.5014 (2.47); 7.4859 (3.37); 7.4746 (0.61); 7.4715 (1.36); 7.1244 (1.53); 7.1222 (1.55); 7.1106 (1.49); 7.1084

(1.47); 5.3445 (6.98); 4.1960 (2.15); 4.1827 (4.65); 4.1693 (2.20); 4.0453 (0.95); 4.0310 (0.96); 4.0168 (0.33); 3.3394 (10.40); 3.3158 (0.46);

3.0794 (16.00); 2.9191 (1.40); 2.9138 (2.99); 2.9086 (1.44); 2.5789 (1.32); 2.5736 (1.41); 2.5656 (2.78); 2.5603 (2.73); 2.5522 (1.41); 2.5470

(1.27); 2.5192 (1.44); 2.5157 (2.92); 2.5122 (3.96); 2.5086 (2.93); 2.5052 (1.43); 1.9989 (4.08); 1.2525 (0.88); 1.2416 (0.43); 1.1980 (1.09);

1.1838 (2.15); 1.1695 (1.06); 0.8802 (0.51); 0.8666 (1.42); 0.8523 (0.63)

›Example 4, Solvent: DMSO, Spectrometer: 499.93 MHz

7.7446 (3.01); 7.7343 (1.08); 7.7303 (3.49); 7.7274 (2.72); 7.5671 (0.40); 7.5648 (0.64); 7.5624 (0.51); 7.5550 (0.54); 7.5500 (1.77); 7.5458

(0.74); 7.5380 (1.00); 7.5355 (1.54); 7.5330 (0.99); 7.5076 (2.63); 7.4950 (1.98); 7.4922 (3.49); 7.4813 (0.74); 7.4781 (1.41); 7.4759 (0.98);

7.4708 (0.32); 7.0072 (3.79); 6.6393 (3.47); 5.1287 (6.93); 3.3423 (7.56); 3.0610 (16.00); 2.5195 (0.60); 2.5160 (1.19); 2.5124 (1.61); 2.5088

(1.24); 2.5055 (0.65); 1.9990 (1.19); 1.1984 (0.33); 1.1841 (0.64)

›Example 5, Solvent: DMSO, Spectrometer: 400.13 MHz

10.1669 (3.24); 7.8318 (0.50); 7.8107 (2.28); 7.8007 (2.67); 7.7955 (5.24); 7.7800 (0.66); 7.7267 (2.91); 7.7088 (3.58); 7.7051 (2.67); 7.5666

(0.54); 7.5548 (0.45); 7.5483 (1.75); 7.5428 (0.62); 7.5301 (1.52); 7.4995 (2.65); 7.4803 (3.35); 7.4627 (1.30); 7.1047 (1.40); 7.0989 (1.39);

7.0899 (1.27); 7.0841 (1.35); 5.3335 (7.04); 4.1468 (1.93); 4.1298 (4.09); 4.1128 (2.01); 3.3279 (116.65); 3.0694 (16.00); 2.5155 (20.77);

2.5113 (40.74); 2.5069 (54.41); 2.5025 (40.18); 2.3339 (0.36); 1.7244 (1.24); 1.6879 (2.13); 1.6484 (1.50); 1.6310 (0.97); 1.6032 (0.68); 1.5377

(0.90); 1.5207 (2.62); 1.5036 (2.95); 1.4868 (1.20); 1.4125 (0.38); 1.4042 (0.46); 1.3960 (0.53); 1.3861 (0.55); 1.3781 (0.51); 1.3695 (0.50);

1.3613 (0.41); 1.2526 (0.44); 1.2221 (0.95); 1.1924 (1.39); 1.1656 (1.61); 1.1514 (0.63); 1.1439 (0.80); 1.1140 (0.48); 0.9629 (0.59); 0.9341

(1.29); 0.9043 (1.16); 0.8809 (0.48)

›Example 6, Solvent: DMSO, Spectrometer: 400.13 MHz

10.1987 (3.02); 7.8363 (0.49); 7.8152 (2.33); 7.8063 (2.70); 7.8005 (5.45); 7.7855 (0.64); 7.7274 (2.92); 7.7095 (3.63); 7.7058 (2.67); 7.5662

(0.57); 7.5631 (0.41); 7.5543 (0.50); 7.5479 (1.77); 7.5423 (0.64); 7.5329 (1.08); 7.5297 (1.56); 7.5265 (0.90); 7.4995 (2.64); 7.4838 (1.99);

7.4803 (3.33); 7.4666 (0.69); 7.4627 (1.34); 7.4596 (0.86); 7.1087 (1.39); 7.1025 (1.38); 7.0941 (1.24); 7.0880 (1.33); 5.8795 (0.66); 5.8705

(0.38); 5.8631 (0.38); 5.8538 (0.97); 5.8369 (1.00); 5.8276 (0.43); 5.8202 (0.42); 5.8111 (0.78); 5.7947 (0.39); 5.7612 (1.46); 5.3376 (7.02);

5.0854 (0.55); 5.0814 (1.22); 5.0766 (1.29); 5.0726 (0.61); 5.0424 (0.53); 5.0385 (1.13); 5.0337 (1.18); 5.0297 (0.58); 5.0055 (1.28); 5.0031

(1.17); 5.0006 (1.14); 4.9801 (1.20); 4.9775 (1.09); 4.9751 (1.07); 4.1127 (2.11); 4.0961 (4.43); 4.0796 (2.18); 3.3305 (40.52); 3.0706 (16.00);

2.5155 (7.99); 2.5112 (15.37); 2.5068 (20.26); 2.5024 (14.84); 2.1528 (0.71); 2.1352 (1.78); 2.1182 (1.83); 2.1159 (1.84); 2.0991 (0.87); 1.7438

(0.62); 1.7270 (1.73); 1.7079 (2.23); 1.6904 (1.66); 1.6733 (0.57)

›Example 7, Solvent: DMSO, Spectrometer: 400.13 MHz

10.2520 (3.20); 7.8262 (0.66); 7.8052 (2.02); 7.7880 (3.89); 7.7829 (2.83); 7.7658 (0.83); 7.7279 (3.00); 7.7100 (3.67); 7.7063 (2.76); 7.5667

(0.56); 7.5636 (0.41); 7.5547 (0.48); 7.5483 (1.79); 7.5428 (0.66); 7.5332 (1.07); 7.5302 (1.56); 7.4998 (2.71); 7.4806 (3.42); 7.4669 (0.71);

7.4629 (1.37); 7.4599 (0.90); 7.3152 (9.49); 7.3043 (10.60); 7.2859 (0.54); 7.2827 (0.54); 7.2547 (0.43); 7.2454 (0.89); 7.2350 (1.32); 7.2241

(1.45); 7.2137 (0.79); 7.2021 (0.42); 7.1087 (1.55); 7.1049 (1.57); 7.0921 (1.47); 7.0883 (1.49); 5.7617 (5.40); 5.3363 (6.96); 4.3097 (1.95);

4.2925 (4.25); 4.2752 (2.06); 3.3342 (34.82); 3.0676 (16.00); 2.9561 (1.94); 2.9389 (3.94); 2.9217 (1.88); 2.5113 (12.99); 2.5069 (17.15);

2.5025 (12.65); 1.9933 (0.37)

›Example 8, Solvent: DMSO, Spectrometer: 400.13 MHz

10.5083 (2.38); 8.0760 (1.44); 8.0553 (1.72); 7.8355 (1.33); 7.8161 (1.97); 7.7959 (1.24); 7.7279 (2.88); 7.7100 (3.57); 7.7063 (2.65); 7.5683

(0.55); 7.5651 (0.40); 7.5564 (0.47); 7.5500 (1.75); 7.5444 (0.63); 7.5349 (1.04); 7.5317 (1.52); 7.5007 (2.62); 7.4815 (3.32); 7.4677 (0.67);

7.4638 (1.32); 7.1445 (1.98); 7.1261 (1.92); 5.7617 (1.80); 5.3578 (6.81); 3.3305 (52.69); 3.0573 (16.00); 2.5155 (10.46); 2.5113 (20.34);

2.5069 (27.02); 2.5025 (19.91); 2.3963 (1.83); 2.3779 (3.38); 2.3594 (2.01); 1.5833 (0.93); 1.5670 (1.45); 1.5494 (1.15); 1.5310 (0.46); 1.2683

(6.34); 1.2651 (6.26); 0.8766 (1.79); 0.8598 (5.70); 0.8425 (2.16)

›Example 9, Solvent: DMSO, Spectrometer: 400.13 MHz

12.1173 (2.55); 7.7390 (2.96); 7.7213 (3.56); 7.7176 (2.64); 7.5667 (0.50); 7.5636 (0.37); 7.5552 (0.41); 7.5483 (1.74); 7.5427 (0.60); 7.5335

(1.03); 7.5303 (1.57); 7.5051 (2.73); 7.4859 (3.34); 7.4724 (0.59); 7.4684 (1.25); 7.4650 (0.82); 7.2615 (4.30); 5.7612 (3.17); 5.3238 (6.70);

3.3346 (29.08); 3.0167 (16.00); 2.5111 (11.26); 2.5067 (14.95); 2.5024 (10.94); 2.4226 (1.84); 2.4042 (3.55); 2.3856 (2.02); 1.9928 (0.56);

1.5958 (0.97); 1.5790 (1.49); 1.5613 (1.14); 1.5430 (0.39); 1.2590 (6.75); 1.1781 (0.36); 0.8689 (1.89); 0.8599 (2.02); 0.8524 (5.93); 0.8351

(2.14)

›Example 10, Solvent: DMSO, Spectrometer: 400.13 MHz

12.5590 (1.60); 7.7403 (2.99); 7.7225 (3.67); 7.7188 (2.71); 7.5698 (0.58); 7.5667 (0.43); 7.5582 (0.50); 7.5515 (1.82); 7.5457 (0.69); 7.5366

(1.17); 7.5334 (1.66); 7.5074 (2.81); 7.4883 (3.46); 7.4747 (0.77); 7.4707 (1.40); 7.4674 (0.92); 7.3697 (4.69); 7.0148 (1.41); 6.9960 (1.86);

6.9939 (1.79); 6.9214 (0.33); 6.9149 (0.79); 6.9073 (0.97); 6.9001 (1.09); 6.8926 (1.62); 6.8884 (0.78); 6.8804 (0.96); 6.8733 (2.00); 6.8624

(5.17); 6.8583 (3.48); 6.8473 (1.45); 6.8435 (1.38); 6.8320 (0.37); 6.8274 (0.40); 6.8236 (0.37); 5.7612 (5.24); 5.3492 (6.42); 5.1539 (1.22);

5.1452 (2.37); 5.1356 (1.29); 4.4359 (2.83); 4.4333 (2.89); 4.4258 (3.48); 4.4034 (0.38); 4.0429 (0.50); 4.0252 (0.50); 3.3306 (35.81); 3.2961

(0.61); 3.0174 (16.00); 2.5153 (10.91); 2.5112 (20.83); 2.5068 (27.33); 2.5024 (19.99); 1.9938 (2.16); 1.2405 (0.35); 1.1972 (0.60); 1.1794

(1.16); 1.1616 (0.60)

›Example 11, Solvent: DMSO, Spectrometer: 400.13 MHz

12.3858 (1.35); 7.7445 (2.97); 7.7267 (3.64); 7.7230 (2.75); 7.5705 (0.54); 7.5676 (0.41); 7.5591 (0.46); 7.5522 (1.78); 7.5465 (0.67); 7.5374

(1.11); 7.5342 (1.65); 7.5089 (2.78); 7.4935 (1.99); 7.4898 (3.45); 7.4765 (0.75); 7.4723 (1.39); 7.4688 (0.97); 7.3613 (4.75); 7.1264 (0.72);

7.1081 (1.50); 7.0873 (1.38); 7.0804 (2.10); 7.0602 (2.42); 7.0391 (0.87); 6.8995 (2.03); 6.8791 (1.79); 6.8735 (1.39); 6.8549 (1.91); 6.8437

(0.76); 6.8409 (0.85); 6.8366 (1.03); 6.8339 (0.95); 6.8252 (0.93); 6.8226 (1.05); 6.8070 (1.35); 6.7868 (0.85); 5.3532 (6.46); 4.9141 (1.07);

4.9057 (1.24); 4.8938 (1.34); 4.8854 (1.16); 4.7823 (0.51); 4.7725 (0.59); 4.7660 (0.63); 4.7562 (0.53); 3.3355 (12.66); 3.3037 (0.88); 3.0259

(16.00); 2.8393 (0.37); 2.8332 (0.36); 2.8122 (0.70); 2.7920 (0.85); 2.7780 (0.65); 2.7664 (0.56); 2.7506 (0.33); 2.7264 (0.51); 2.7127 (1.04);

2.6981 (0.63); 2.6851 (0.42); 2.6713 (0.89); 2.6570 (0.64); 2.6377 (0.35); 2.5154 (9.57); 2.5113 (18.71); 2.5069 (24.93); 2.5025 (18.54); 2.2459

(0.49); 2.2373 (0.50); 2.2257 (0.53); 2.2173 (0.54); 2.2115 (0.77); 2.2029 (0.73); 2.1881 (0.42); 2.1535 (0.37); 2.1434 (0.39); 2.1393 (0.34);

2.1335 (0.37); 2.1294 (0.35); 2.1190 (0.51); 2.1045 (0.51); 2.0964 (0.73); 2.0828 (1.00); 2.0629 (1.15); 2.0478 (0.70); 2.0290 (0.42); 1.9938

(1.29); 1.1969 (0.35); 1.1791 (0.66); 1.1614 (0.34)

›Example 12, Solvent: DMSO, Spectrometer: 400.13 MHz

11.7576 (2.06); 7.7345 (3.08); 7.7167 (3.65); 7.7130 (2.74); 7.5665 (0.55); 7.5633 (0.42); 7.5548 (0.49); 7.5481 (1.79); 7.5426 (0.64); 7.5301

(1.62); 7.5040 (2.81); 7.4849 (3.46); 7.4674 (1.30); 7.4639 (0.97); 7.2555 (4.46); 5.7625 (2.56); 5.2861 (6.90); 4.1729 (0.33); 4.1617 (2.16);

4.1450 (4.50); 4.1283 (2.17); 3.3325 (76.53); 3.3085 (0.60); 3.0339 (16.00); 2.9930 (0.62); 2.5110 (32.54); 2.5067 (42.65); 2.5023 (31.20);

1.9936 (0.64); 1.6427 (1.23); 1.6256 (1.91); 1.6083 (1.33); 1.5910 (0.43); 1.3398 (1.29); 1.3306 (2.58); 1.3223 (4.17); 1.3130 (4.16); 1.3044

(2.61); 1.2388 (0.33); 1.1791 (0.38); 0.8967 (2.30); 0.8793 (6.15); 0.8616 (2.11)

›Example 13, Solvent: DMSO, Spectrometer: 400.13 MHz

12.1083 (2.32); 7.7383 (2.90); 7.7255 (1.04); 7.7205 (3.51); 7.7167 (2.62); 7.5682 (0.54); 7.5567 (0.47); 7.5497 (1.76); 7.5441 (0.65); 7.5349

(1.06); 7.5318 (1.60); 7.5068 (2.76); 7.4914 (1.91); 7.4876 (3.36); 7.4742 (0.69); 7.4701 (1.31); 7.4667 (0.87); 7.2592 (4.09); 5.7579 (2.07);

5.3244 (6.84); 3.3214 (68.27); 3.3016 (1.27); 3.0191 (16.00); 2.5157 (9.34); 2.5115 (18.35); 2.5070 (24.67); 2.5026 (18.27); 2.4986 (9.55);

2.4320 (2.28); 2.4136 (3.88); 2.3949 (2.39); 1.9935 (0.74); 1.6087 (0.56); 1.5905 (1.62); 1.5717 (2.29); 1.5532 (1.76); 1.5342 (0.75); 1.3431

(0.37); 1.3244 (1.27); 1.3055 (2.11); 1.2868 (2.15); 1.2686 (1.36); 1.2505 (0.58); 1.2402 (0.40); 1.1802 (0.44); 0.8973 (4.48); 0.8790 (8.83);

0.8606 (3.98)

›Example 14, Solvent: DMSO, Spectrometer: 400.13 MHz

11.7455 (1.91); 7.7336 (2.82); 7.7210 (1.05); 7.7159 (3.56); 7.7121 (2.61); 7.5665 (0.53); 7.5634 (0.40); 7.5550 (0.47); 7.5481 (1.75); 7.5424

(0.64); 7.5334 (1.07); 7.5301 (1.60); 7.5268 (0.91); 7.5045 (2.69); 7.4893 (1.90); 7.4854 (3.33); 7.4720 (0.69); 7.4679 (1.36); 7.4644 (1.02);

7.2529 (4.15); 5.7580 (2.45); 5.2874 (6.51); 4.1724 (2.20); 4.1558 (4.59); 4.1392 (2.30); 3.3209 (73.16); 3.0349 (16.00); 2.9949 (0.50); 2.5158

(9.29); 2.5114 (18.55); 2.5070 (25.08); 2.5025 (18.39); 2.4982 (9.44); 1.9936 (0.44); 1.6453 (0.50); 1.6283 (1.56); 1.6222 (0.70); 1.6108 (2.00);

1.5912 (1.74); 1.5746 (0.75); 1.4103 (0.35); 1.3917 (1.20); 1.3726 (1.96); 1.3538 (2.02); 1.3356 (1.25); 1.3173 (0.42); 0.9266 (4.37); 0.9082

(8.84); 0.8897 (3.94); 0.8633 (0.32)

›Example 15, Solvent: DMSO, Spectrometer: 400.13 MHz

10.4985 (2.11); 8.0751 (1.44); 8.0545 (1.70); 7.8356 (1.29); 7.8161 (1.88); 7.7961 (1.20); 7.7272 (2.76); 7.7144 (0.97); 7.7094 (3.46); 7.7057

(2.61); 7.5692 (0.51); 7.5661 (0.38); 7.5572 (0.42); 7.5508 (1.67); 7.5453 (0.61); 7.5359 (0.96); 7.5327 (1.48); 7.5294 (0.88); 7.5021 (2.54);

7.4866 (1.78); 7.4829 (3.20); 7.4693 (0.63); 7.4653 (1.27); 7.4622 (0.83); 7.1441 (1.91); 7.1258 (1.81); 5.7585 (0.87); 5.3585 (6.77); 3.3210

(97.01); 3.0587 (16.00); 2.5160 (11.84); 2.5117 (24.12); 2.5072 (33.05); 2.5027 (24.80); 2.4984 (13.08); 2.4063 (2.03); 2.3880 (3.54); 2.3693

(2.20); 1.5971 (0.49); 1.5789 (1.43); 1.5601 (2.05); 1.5416 (1.57); 1.5228 (0.68); 1.3517 (0.34); 1.3331 (1.17); 1.3142 (1.91); 1.2955 (1.96);

1.2774 (1.24); 1.2593 (0.44); 0.9054 (4.07); 0.8872 (8.23); 0.8687 (3.69)

›Example 16, Solvent: DMSO, Spectrometer: 400.13 MHz

10.1548 (2.83); 7.8327 (0.59); 7.8116 (2.03); 7.7959 (4.35); 7.7924 (3.17); 7.7759 (0.74); 7.7267 (2.82); 7.7138 (1.00); 7.7089 (3.49); 7.7052

(2.59); 7.5671 (0.53); 7.5641 (0.40); 7.5553 (0.44); 7.5487 (1.69); 7.5432 (0.60); 7.5338 (0.97); 7.5306 (1.49); 7.5273 (0.87); 7.5004 (2.57);

7.4849 (1.81); 7.4813 (3.23); 7.4677 (0.62); 7.4637 (1.29); 7.4606 (0.83); 7.1056 (1.39); 7.1010 (1.44); 7.0896 (1.30); 7.0850 (1.35); 5.7586

(1.43); 5.3364 (6.81); 3.9986 (4.32); 3.9809 (4.44); 3.3202 (133.08); 3.2974 (1.78); 3.2478 (0.43); 3.0711 (16.00); 2.5159 (16.66); 2.5115

(33.31); 2.5070 (45.25); 2.5026 (33.44); 2.4983 (17.30); 2.3338 (0.33); 2.2373 (0.37); 2.2185 (0.83); 2.2000 (1.13); 2.1813 (0.89); 2.1629 (0.42);

1.9939 (0.36); 1.7481 (0.34); 1.7322 (0.71); 1.7197 (0.96); 1.7006 (1.16); 1.6878 (0.84); 1.6717 (0.54); 1.6171 (0.72); 1.5969 (1.19); 1.5804

(1.17); 1.5547 (0.92); 1.5425 (0.64); 1.5349 (1.18); 1.5262 (1.00); 1.5159 (1.25); 1.4967 (0.78); 1.4864 (0.48); 1.3142 (0.44); 1.2981 (0.96);

1.2815 (1.16); 1.2673 (1.08); 1.2500 (1.00)

›Example 17, Solvent: DMSO, Spectrometer: 400.13 MHz

10.9907 (2.47); 8.1662 (1.80); 8.1457 (2.17); 7.9407 (1.37); 7.9212 (2.03); 7.9011 (1.38); 7.8921 (1.50); 7.8726 (1.77); 7.8651 (1.14); 7.8590

(1.18); 7.8401 (0.94); 7.8343 (1.10); 7.8302 (0.84); 7.7407 (2.86); 7.7228 (3.51); 7.7191 (2.65); 7.5985 (0.63); 7.5838 (0.80); 7.5781 (1.34);

7.5725 (0.86); 7.5693 (0.72); 7.5635 (1.45); 7.5587 (1.32); 7.5541 (2.01); 7.5484 (0.85); 7.5439 (1.09); 7.5391 (1.19); 7.5359 (1.67); 7.5063

(2.71); 7.4871 (3.43); 7.4792 (1.15); 7.4771 (1.12); 7.4697 (1.87); 7.4564 (1.22); 7.4505 (1.11); 7.4345 (0.58); 7.4298 (0.53); 7.2525 (1.99);

7.2341 (1.92); 5.7583 (2.56); 5.4273 (6.85); 4.0440 (0.46); 4.0262 (0.48); 3.3216 (62.10); 3.2635 (0.45); 3.0866 (16.00); 2.5157 (11.88); 2.5115

(23.07); 2.5070 (30.83); 2.5026 (22.71); 2.4984 (11.72); 1.9935 (2.00); 1.1980 (0.55); 1.1802 (1.07); 1.1624 (0.54)

›Example 18, Solvent: DMSO, Spectrometer: 400.13 MHz

10.1574 (2.74); 7.8335 (0.45); 7.8125 (2.33); 7.8044 (2.57); 7.7981 (5.52); 7.7835 (0.57); 7.7261 (2.75); 7.7133 (1.00); 7.7083 (3.46); 7.7046

(2.53); 7.5668 (0.53); 7.5551 (0.45); 7.5486 (1.70); 7.5430 (0.59); 7.5337 (0.99); 7.5304 (1.47); 7.5271 (0.83); 7.5002 (2.53); 7.4848 (1.79);

7.4811 (3.16); 7.4675 (0.61); 7.4635 (1.26); 7.4603 (0.77); 7.1058 (1.33); 7.0993 (1.33); 7.0916 (1.17); 7.0851 (1.27); 5.7586 (0.81); 5.3352

(6.89); 4.1135 (2.18); 4.0969 (4.56); 4.0803 (2.26); 3.3199 (123.98); 3.2974 (1.65); 3.2466 (0.43); 3.0700 (16.00); 2.5159 (16.11); 2.5115

(31.93); 2.5070 (43.10); 2.5025 (31.56); 2.4981 (16.17); 1.6332 (0.49); 1.6161 (1.46); 1.6098 (0.63); 1.5988 (1.89); 1.5793 (1.62); 1.5626 (0.70);

1.4204 (0.35); 1.4017 (1.17); 1.3826 (1.84); 1.3638 (1.87); 1.3457 (1.15); 1.3275 (0.38); 0.9319 (4.19); 0.9135 (8.44); 0.8951 (3.70)

›Example 19, Solvent: DMSO, Spectrometer: 400.13 MHz

12.5294 (1.59); 7.7395 (2.96); 7.7217 (3.52); 7.7180 (2.62); 7.5699 (0.52); 7.5585 (0.41); 7.5515 (1.73); 7.5460 (0.60); 7.5336 (1.56); 7.5075

(2.73); 7.4884 (3.34); 7.4749 (0.59); 7.4709 (1.23); 7.4677 (0.83); 7.3325 (4.63); 7.3036 (1.94); 7.2821 (3.54); 7.2636 (2.48); 6.9614 (1.16);

6.9430 (2.09); 6.9213 (3.45); 6.9193 (3.62); 6.8995 (3.04); 6.8745 (0.67); 6.8547 (0.61); 5.7576 (7.18); 5.3414 (6.67); 5.0710 (0.48); 5.0546

(1.66); 5.0380 (1.67); 5.0215 (0.47); 4.8193 (0.35); 4.8023 (0.36); 4.0438 (0.43); 4.0260 (0.43); 3.3243 (31.22); 3.2976 (0.51); 3.0193 (16.00);

2.5112 (16.98); 2.5068 (22.43); 2.5025 (16.19); 1.9934 (1.84); 1.5537 (6.33); 1.5372 (6.27); 1.5084 (1.60); 1.4914 (1.55); 1.1977 (0.50); 1.1799

(0.97); 1.1621 (0.48)

›Example 20, Solvent: DMSO, Spectrometer: 400.13 MHz

12.8184 (0.79); 7.9522 (1.39); 7.9328 (1.87); 7.9302 (2.03); 7.9232 (1.21); 7.9043 (0.92); 7.8986 (1.06); 7.8944 (0.81); 7.7505 (2.86); 7.7328

(3.50); 7.7291 (2.65); 7.6359 (0.58); 7.6213 (0.71); 7.6156 (1.16); 7.6010 (1.22); 7.5963 (0.95); 7.5813 (0.86); 7.5730 (0.69); 7.5698 (0.55);

7.5615 (0.51); 7.5545 (1.81); 7.5486 (0.75); 7.5399 (1.10); 7.5365 (1.69); 7.5332 (1.10); 7.5236 (0.96); 7.5124 (2.95); 7.4972 (2.81); 7.4935

(3.80); 7.4804 (1.23); 7.4759 (1.84); 7.4033 (4.13); 5.7585 (2.30); 5.3933 (6.38); 3.3207 (94.77); 3.0251 (16.00); 2.5159 (15.95); 2.5115 (31.24);

2.5070 (42.01); 2.5026 (31.01); 2.4983 (16.05); 1.9937 (1.08); 1.1804 (0.60); 1.1626 (0.32)

›Example 21, Solvent: DMSO, Spectrometer: 400.13 MHz

9.8506 (1.17); 7.7812 (0.84); 7.7650 (1.91); 7.7608 (1.24); 7.7441 (0.38); 7.7251 (1.21); 7.7072 (1.45); 7.7036 (1.09); 7.5480 (0.72); 7.5297

(0.63); 7.4996 (1.08); 7.4804 (1.33); 7.4627 (0.54); 7.0797 (0.62); 7.0756 (0.64); 7.0635 (0.56); 7.0592 (0.56); 5.3201 (2.79); 3.3634 (296.68);

3.3409 (5.56); 3.0665 (6.33); 2.5114 (20.72); 2.5070 (27.49); 2.5027 (20.59); 1.9926 (0.59); 1.4657 (16.00); 1.3519 (0.95); 1.3258 (0.32);

1.3018 (0.57); 1.2479 (1.59); 1.1776 (0.35); 0.8776 (0.50); 0.8610 (1.44); 0.8434 (0.62)

›Example 22, Solvent: DMSO, Spectrometer: 400.13 MHz

10.2809 (0.68); 7.9559 (2.45); 7.8012 (0.44); 7.7827 (0.45); 7.7542 (0.59); 7.5933 (0.62); 7.5763 (0.76); 7.5723 (0.62); 7.4749 (0.36); 7.4574

(0.44); 7.4426 (0.79); 7.4239 (0.71); 7.1464 (0.42); 7.1282 (0.38); 5.2591 (1.46); 4.1891 (0.53); 4.1724 (1.13); 4.1557 (0.53); 3.3545 (11.64);

2.9169 (0.49); 2.9104 (0.92); 2.9037 (0.73); 2.8939 (16.00); 2.7343 (13.95); 2.5721 (0.33); 2.5656 (0.35); 2.5554 (0.71); 2.5488 (0.69); 2.5386

(0.50); 2.5289 (0.66); 2.5107 (16.80); 2.5064 (22.26); 2.5022 (16.29)

›Example 23, Solvent: DMSO, Spectrometer: 400.13 MHz

7.9573 (0.37); 7.8215 (0.44); 7.8010 (0.38); 7.7687 (0.36); 7.7571 (0.37); 7.7329 (0.39); 7.6427 (6.99); 7.6251 (8.28); 7.6214 (5.86); 7.5318

(1.42); 7.5134 (4.14); 7.5075 (1.62); 7.4956 (4.03); 7.4750 (6.92); 7.4628 (5.13); 7.4600 (5.35); 7.4559 (7.63); 7.4433 (5.44); 7.4389 (3.11);

7.4245 (2.90); 6.5712 (4.72); 6.5530 (4.29); 6.4382 (4.75); 6.4174 (4.44); 6.2342 (1.45); 5.3354 (0.74); 5.2840 (0.39); 5.2036 (16.00); 2.8945

(1.61); 2.7352 (1.36); 2.6755 (0.58); 2.5106 (89.93); 2.5064 (117.56); 2.5022 (87.81); 2.3332 (0.77); 2.0801 (0.45); 1.4661 (0.44); 1.3663 (0.51)

›Example 25, Solvent: DMSO, Spectrometer: 499.93 MHz

7.6204 (1.43); 7.6161 (1.82); 7.6090 (2.12); 7.6011 (1.97); 7.5108 (4.24); 7.5065 (3.96); 7.4998 (2.44); 7.4899 (0.61); 7.3940 (1.02); 7.3787

(1.60); 7.3630 (1.08); 6.4882 (1.74); 6.4738 (1.68); 6.3819 (1.77); 6.3654 (1.72); 5.9978 (2.42); 5.9845 (0.70); 5.1329 (6.30); 3.3423 (16.00);

3.3187 (1.72); 3.2748 (12.78); 2.5150 (6.35); 2.5118 (8.32); 2.5085 (6.37); 1.9993 (0.40)

›Example 26, Solvent: DMSO, Spectrometer: 499.93 MHz

10.1670 (6.78); 7.8170 (0.80); 7.8000 (5.62); 7.7954 (6.11); 7.7896 (11.23); 7.7790 (1.06); 7.6251 (3.99); 7.6211 (5.06); 7.6141 (5.59); 7.6060

(5.42); 7.5141 (11.08); 7.5103 (10.73); 7.5035 (6.79); 7.5009 (5.93); 7.4926 (1.69); 7.4851 (0.50); 7.0871 (0.47); 7.0764 (2.89); 7.0703 (3.01);

7.0660 (2.72); 7.0600 (2.76); 7.0495 (0.35); 5.2849 (16.00); 4.1004 (4.60); 4.0870 (9.35); 4.0736 (4.60); 3.9135 (0.57); 3.4056 (0.54); 3.4000

(0.48); 3.3947 (0.60); 3.3823 (0.34); 3.3455 (28.74); 3.3219 (1.33); 3.2412 (32.31); 2.5150 (6.09); 2.5118 (7.70); 2.5086 (5.87); 1.6258 (2.65);

1.6122 (4.01); 1.5986 (2.87); 1.5854 (0.93); 1.3570 (0.76); 1.3299 (9.83); 1.3229 (7.95); 1.3156 (6.59); 1.2430 (0.60); 0.9010 (4.82); 0.8873

(11.07); 0.8734 (4.09); 0.8477 (0.32)

›Example 27, Solvent: DMSO, Spectrometer: 399.95 MHz

12.6614 (1.15); 7.7421 (2.97); 7.7381 (1.73); 7.7337 (1.65); 7.7297 (2.20); 7.7245 (3.73); 7.7208 (2.69); 7.7115 (0.81); 7.6590 (0.35); 7.6545

(0.35); 7.6457 (0.43); 7.6407 (0.79); 7.6381 (0.67); 7.6362 (0.65); 7.6339 (0.56); 7.6271 (0.63); 7.6227 (0.74); 7.6199 (0.81); 7.6151 (0.48);

7.6062 (0.45); 7.6018 (0.40); 7.5662 (0.49); 7.5630 (0.34); 7.5548 (0.38); 7.5479 (1.67); 7.5420 (0.55); 7.5332 (1.02); 7.5298 (1.56); 7.5263

(0.85); 7.5048 (2.60); 7.4896 (1.77); 7.4859 (3.17); 7.4725 (0.57); 7.4684 (1.28); 7.4649 (0.78); 7.3945 (5.01); 7.3703 (1.05); 7.3648 (1.42);

7.3624 (1.65); 7.3437 (2.87); 7.3248 (0.97); 7.3224 (0.86); 5.3703 (6.26); 3.3387 (88.38); 3.0367 (16.00); 2.8907 (2.15); 2.7323 (1.76); 2.7311

(1.75); 2.5253 (0.70); 2.5119 (12.90); 2.5076 (24.75); 2.5031 (32.03); 2.4985 (23.64); 2.4941 (11.72); −0.0002 (2.90)

›Example 28, Solvent: DMSO, Spectrometer: 399.95 MHz

12.4655 (1.14); 7.9527 (0.99); 7.7392 (2.77); 7.7267 (0.81); 7.7216 (3.44); 7.7179 (2.52); 7.5665 (0.48); 7.5633 (0.32); 7.5551 (0.34); 7.5481

(1.66); 7.5423 (0.52); 7.5334 (0.94); 7.5301 (1.53); 7.5266 (0.81); 7.5045 (2.56); 7.4893 (1.64); 7.4855 (3.14); 7.4721 (0.49); 7.4680 (1.21);

7.4645 (0.73); 7.3366 (4.68); 7.2656 (0.68); 7.2628 (0.73); 7.2439 (0.97); 7.2364 (0.75); 7.2327 (0.77); 7.2161 (0.80); 7.2127 (0.84); 7.1310

(0.32); 7.1101 (1.28); 7.1067 (1.34); 7.1005 (1.10); 7.0930 (2.68); 7.0805 (1.09); 7.0759 (1.12); 7.0601 (0.40); 6.9975 (0.48); 6.9899 (0.48);

6.9859 (0.60); 6.9816 (0.71); 6.9773 (0.56); 6.9751 (0.51); 6.9682 (0.78); 6.9657 (0.70); 6.9632 (0.87); 6.9547 (0.32); 6.9481 (0.34); 5.3405

(6.14); 4.9435 (7.87); 3.3318 (62.16); 3.0274 (16.00); 2.8903 (7.39); 2.7317 (6.11); 2.7307 (5.95); 2.5248 (0.67); 2.5114 (13.19); 2.5070 (26.28);

2.5024 (34.60); 2.4978 (25.54); 2.4934 (12.50); −0.0002 (3.67)

›Example 29, Solvent: DMSO, Spectrometer: 399.95 MHz

10.8476 (1.94); 8.0189 (0.92); 7.9981 (1.14); 7.9532 (1.08); 7.8446 (1.33); 7.8254 (1.80); 7.8051 (1.16); 7.7317 (2.58); 7.7278 (1.28); 7.7190

(0.82); 7.7139 (3.41); 7.7101 (2.40); 7.5687 (0.49); 7.5568 (0.36); 7.5504 (1.66); 7.5446 (0.51); 7.5354 (0.90); 7.5321 (1.43); 7.5287 (0.73);

7.5015 (2.41); 7.4981 (1.07); 7.4860 (1.69); 7.4823 (3.11); 7.4687 (0.51); 7.4646 (1.26); 7.4614 (0.75); 7.4499 (1.15); 7.4432 (0.66); 7.4381

(1.17); 7.4343 (0.98); 7.4269 (2.33); 7.4200 (0.92); 7.4165 (1.17); 7.4107 (0.71); 7.4044 (1.37); 7.3272 (0.45); 7.3154 (3.00); 7.3088 (1.57);

7.3044 (1.99); 7.3026 (1.89); 7.2984 (1.35); 7.2920 (2.28); 7.1682 (1.80); 7.1498 (1.74); 5.3814 (6.18); 3.9278 (6.08); 3.3309 (77.15); 3.0671

(16.00); 2.8905 (8.60); 2.7319 (7.04); 2.5250 (0.86); 2.5201 (1.35); 2.5116 (14.93); 2.5071 (29.35); 2.5025 (38.25); 2.4979 (27.55); 2.4934

(13.01); −0.0002 (7.72)

›Example 30, Solvent: DMSO, Spectrometer: 400.13 MHz

7.9623 (2.56); 7.5454 (4.64); 7.5077 (2.36); 7.4103 (1.46); 7.3904 (3.38); 7.3590 (6.53); 6.5101 (2.80); 6.4923 (2.68); 6.3971 (2.78); 6.3764

(2.66); 6.0256 (7.00); 5.1800 (9.75); 3.3528 (4.97); 3.0867 (16.00); 2.8990 (10.92); 2.7401 (10.31); 2.5122 (33.53); 2.3438 (15.48); 1.3684

(0.34)

›Example 31, Solvent: DMSO, Spectrometer: 399.95 MHz

10.4632 (2.02); 8.0550 (0.92); 8.0343 (1.16); 7.9530 (0.48); 7.8907 (1.24); 7.8714 (1.69); 7.8512 (1.08); 7.7316 (1.86); 7.7289 (2.49); 7.7250

(1.20); 7.7163 (0.73); 7.7111 (3.35); 7.7074 (2.31); 7.5666 (0.47); 7.5547 (0.35); 7.5483 (1.59); 7.5426 (0.46); 7.5334 (0.85); 7.5300 (1.40);

7.5266 (0.69); 7.4988 (2.28); 7.4953 (0.96); 7.4834 (1.56); 7.4796 (2.97); 7.4661 (0.46); 7.4620 (1.21); 7.4587 (0.68); 7.2092 (1.66); 7.1918

(1.59); 7.0301 (0.88); 7.0259 (0.69); 7.0100 (1.81); 7.0064 (1.26); 6.9842 (0.94); 6.9799 (2.12); 6.9755 (0.85); 6.9600 (3.36); 6.9556 (0.76);

6.9410 (0.94); 6.9369 (0.54); 6.8974 (1.18); 6.8932 (1.16); 6.8784 (0.97); 6.8741 (1.28); 6.8593 (0.54); 6.8552 (0.51); 5.3901 (5.77); 4.7685

(6.26); 3.8129 (15.55); 3.3339 (69.55); 3.0703 (16.00); 2.8906 (4.10); 2.7322 (3.23); 2.7310 (3.16); 2.5252 (0.57); 2.5204 (0.92); 2.5119 (11.58);

2.5074 (23.25); 2.5028 (30.71); 2.4981 (22.16); 2.4936 (10.43); −0.0002 (2.85)

›Example 32, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5046 (1.97); 8.0714 (1.21); 8.0507 (1.44); 7.8316 (1.26); 7.8123 (1.72); 7.7920 (1.17); 7.7263 (1.95); 7.7238 (2.53); 7.7199 (1.25); 7.7111

(0.79); 7.7060 (3.46); 7.7022 (2.34); 7.5642 (0.48); 7.5523 (0.36); 7.5459 (1.62); 7.5401 (0.48); 7.5309 (0.87); 7.5276 (1.41); 7.5242 (0.70);

7.4964 (2.38); 7.4930 (1.00); 7.4811 (1.63); 7.4773 (3.05); 7.4638 (0.48); 7.4596 (1.23); 7.4564 (0.67); 7.1398 (1.73); 7.1223 (1.69); 5.3535

(6.09); 3.3302 (50.68); 3.0535 (16.00); 2.5256 (0.54); 2.5207 (0.86); 2.5122 (10.08); 2.5077 (19.99); 2.5031 (26.30); 2.4985 (19.01); 2.4939

(8.99); 2.3905 (1.50); 2.3722 (2.83); 2.3536 (1.64); 1.5818 (0.77); 1.5641 (1.11); 1.5463 (0.74); 1.2705 (3.87); 1.2642 (4.45); 1.2541 (3.48);

1.2368 (1.95); 0.8754 (0.76); 0.8701 (1.75); 0.8624 (1.34); 0.8532 (5.74); 0.8356 (1.92); −0.0002 (6.01)

›Example 33, Solvent: DMSO, Spectrometer: 399.95 MHz

10.1847 (2.26); 7.8318 (0.33); 7.8107 (2.37); 7.8045 (2.45); 7.7972 (5.68); 7.7836 (0.38); 7.7228 (2.60); 7.7190 (1.28); 7.7102 (0.77); 7.7051

(3.36); 7.7013 (2.32); 7.5624 (0.48); 7.5505 (0.36); 7.5440 (1.64); 7.5383 (0.49); 7.5291 (0.89); 7.5258 (1.43); 7.5224 (0.73); 7.4955 (2.41);

7.4921 (1.03); 7.4802 (1.66); 7.4764 (3.07); 7.4629 (0.48); 7.4588 (1.21); 7.4555 (0.67); 7.1023 (1.29); 7.0950 (1.29); 7.0888 (1.06); 7.0815

(1.24); 5.3323 (6.65); 4.0624 (2.38); 4.0456 (5.06); 4.0289 (2.42); 3.3316 (57.81); 3.0663 (16.00); 2.8908 (2.35); 2.7322 (1.84); 2.7312 (1.85);

2.5254 (0.53); 2.5205 (0.81); 2.5120 (10.19); 2.5075 (20.50); 2.5029 (27.14); 2.4983 (19.73); 2.4938 (9.45); 1.6509 (1.17); 1.6337 (2.43);

1.6154 (2.49); 1.5982 (1.26); 0.9367 (4.25); 0.9183 (8.68); 0.8997 (3.83); −0.0002 (9.66)

›Example 34, Solvent: DMSO, Spectrometer: 399.95 MHz

10.6207 (1.46); 10.5100 (0.68); 8.0663 (0.64); 8.0593 (0.96); 8.0456 (0.78); 8.0385 (1.14); 7.9533 (0.80); 7.9271 (0.69); 7.9082 (0.92); 7.8871

(0.68); 7.8441 (1.02); 7.8340 (0.57); 7.8247 (1.43); 7.8147 (0.71); 7.8046 (0.91); 7.7944 (0.43); 7.7548 (2.52); 7.7369 (3.27); 7.7332 (2.45);

7.7232 (2.85); 7.7053 (3.56); 7.7016 (2.53); 7.5895 (0.51); 7.5865 (0.32); 7.5769 (0.39); 7.5711 (1.62); 7.5655 (0.94); 7.5528 (1.58); 7.5471

(1.90); 7.5414 (0.54); 7.5318 (1.02); 7.5287 (1.53); 7.5254 (0.83); 7.5132 (2.27); 7.4977 (4.11); 7.4940 (3.92); 7.4790 (3.78); 7.4652 (0.59);

7.4613 (1.28); 7.4582 (0.75); 7.1532 (1.37); 7.1348 (1.37); 7.1217 (0.59); 6.9698 (0.93); 6.9412 (1.41); 6.9229 (1.13); 5.3831 (5.27); 5.3573

(5.56); 4.2783 (1.44); 4.2607 (2.68); 4.2431 (1.49); 3.6906 (1.84); 3.6740 (3.88); 3.6576 (1.90); 3.4255 (3.69); 3.4089 (8.93); 3.3836 (60.04);

3.2564 (0.33); 3.2516 (0.35); 3.2395 (0.33); 3.2334 (0.32); 3.0626 (16.00); 3.0570 (15.53); 2.8913 (4.82); 2.7316 (3.93); 2.6729 (0.42); 2.5715

(1.35); 2.5534 (2.62); 2.5449 (1.30); 2.5349 (1.99); 2.5310 (2.66); 2.5261 (1.54); 2.5127 (25.60); 2.5084 (49.26); 2.5038 (63.69); 2.4993 (46.36);

2.4949 (22.25); 2.4447 (1.04); 2.4382 (0.67); 2.4249 (2.44); 2.4201 (1.20); 2.4040 (1.62); 2.3306 (0.42); 2.1795 (0.34); 2.1618 (0.91); 2.1590

(0.59); 2.1419 (1.07); 2.1230 (0.71); 2.0522 (0.43); 2.0353 (1.34); 2.0175 (1.87); 2.0002 (1.21); 1.9828 (0.35); 1.7324 (0.48); 1.7141 (0.67);

1.6965 (0.49); 1.2345 (0.33); −0.0002 (4.61)

›Example 35, Solvent: DMSO, Spectrometer: 399.95 MHz

10.8718 (2.00); 8.0528 (1.58); 8.0323 (1.90); 7.8250 (1.35); 7.8057 (1.88); 7.7855 (1.22); 7.7280 (2.71); 7.7243 (1.36); 7.7153 (0.85); 7.7102

(3.47); 7.7064 (2.56); 7.5663 (0.49); 7.5632 (0.32); 7.5545 (0.36); 7.5480 (1.68); 7.5424 (0.51); 7.5331 (0.91); 7.5298 (1.44); 7.5264 (0.75);

7.4999 (2.50); 7.4845 (1.70); 7.4808 (3.17); 7.4672 (0.49); 7.4631 (1.22); 7.4599 (0.70); 7.1412 (1.90); 7.1230 (1.83); 5.3661 (6.68); 3.3300

(61.03); 3.0561 (16.00); 2.8908 (2.33); 2.7318 (1.87); 2.5252 (0.58); 2.5119 (10.86); 2.5074 (21.30); 2.5029 (27.86); 2.4983 (20.28); 2.4938

(9.71); 2.0339 (0.48); 2.0293 (0.53); 2.0233 (0.42); 2.0162 (0.94); 2.0088 (0.39); 2.0030 (0.53); 1.9987 (0.53); 0.8757 (0.45); 0.8129 (4.44);

0.8057 (3.17); 0.7929 (2.42); 0.7862 (0.84); −0.0002 (4.96)

›Example 36, Solvent: DMSO, Spectrometer: 400.13 MHz

10.2460 (0.33); 7.8570 (0.58); 5.3910 (0.69); 4.1415 (0.46); 3.8432 (1.77); 3.4129 (16.00); 3.1113 (1.64); 2.5736 (1.01); 2.5693 (2.12); 2.5648

(2.89); 2.5604 (2.08); 2.5560 (0.97); 1.3848 (0.40); 0.9402 (0.53)

›Example 37, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5318 (2.14); 8.0721 (1.28); 8.0515 (1.53); 7.8370 (1.30); 7.8177 (1.81); 7.7975 (1.19); 7.7260 (2.07); 7.7237 (2.64); 7.7199 (1.29); 7.7110

(0.84); 7.7059 (3.46); 7.7021 (2.42); 7.5647 (0.49); 7.5615 (0.32); 7.5528 (0.37); 7.5464 (1.67); 7.5407 (0.51); 7.5314 (0.90); 7.5281 (1.44);

7.5248 (0.73); 7.4974 (2.45); 7.4940 (1.08); 7.4820 (1.70); 7.4783 (3.14); 7.4646 (0.50); 7.4606 (1.23); 7.4574 (0.70); 7.1450 (1.82); 7.1266

(1.78); 5.3564 (6.32); 3.3326 (72.03); 3.0560 (16.00); 2.8909 (0.99); 2.7639 (1.41); 2.7572 (3.09); 2.7506 (1.43); 2.7321 (0.80); 2.5253 (0.68);

2.5121 (11.45); 2.5076 (22.26); 2.5030 (29.03); 2.4984 (21.05); 2.4939 (10.05); 2.4166 (1.58); 2.3984 (3.10); 2.3798 (1.72); 2.1999 (1.12);

2.1932 (1.17); 2.1821 (2.56); 2.1755 (2.49); 2.1646 (1.31); 2.1580 (1.20); 1.6938 (0.36); 1.6755 (1.08); 1.6567 (1.47); 1.6505 (0.82); 1.6378

(1.18); 1.6189 (0.49); 1.4968 (0.52); 1.4789 (1.36); 1.4654 (0.87); 1.4592 (1.53); 1.4479 (0.46); 1.4409 (1.10); −0.0002 (5.85)

›Example 38, Solvent: DMSO, Spectrometer: 399.95 MHz

12.4201 (0.81); 7.9526 (1.01); 7.7385 (2.70); 7.7346 (1.31); 7.7261 (0.76); 7.7209 (3.49); 7.7171 (2.41); 7.5667 (0.47); 7.5553 (0.33); 7.5484

(1.67); 7.5425 (0.50); 7.5337 (0.91); 7.5303 (1.51); 7.5268 (0.77); 7.5047 (2.55); 7.5014 (1.08); 7.4896 (1.59); 7.4856 (3.10); 7.4724 (0.48);

7.4682 (1.22); 7.4647 (0.67); 7.3371 (4.84); 7.1550 (1.82); 7.1490 (0.60); 7.1378 (0.81); 7.1322 (3.25); 7.1280 (0.77); 7.1219 (0.34); 7.1168

(0.72); 7.1107 (2.55); 7.0018 (2.50); 6.9957 (0.79); 6.9909 (2.55); 6.9848 (1.20); 6.9788 (1.83); 6.9739 (0.69); 6.9678 (1.79); 5.3423 (5.97);

4.8284 (7.85); 3.3366 (94.01); 3.0211 (16.00); 2.8904 (8.13); 2.7319 (6.30); 2.7309 (6.69); 2.5252 (0.62); 2.5205 (0.97); 2.5119 (12.85); 2.5074

(25.82); 2.5028 (34.30); 2.4982 (24.98); 2.4937 (11.95); −0.0002 (1.87)

›Example 39, Solvent: DMSO, Spectrometer: 300.16 MHz

10.0097 (2.45); 7.8064 (1.40); 7.7537 (3.31); 7.7417 (3.41); 7.7253 (3.44); 7.5382 (1.67); 7.5166 (2.48); 7.4949 (2.76); 7.1091 (1.48); 7.0870

(1.40); 5.3399 (5.03); 3.3558 (7.80); 3.3512 (7.52); 3.0891 (8.18); 3.0850 (8.18); 2.9282 (2.25); 2.8184 (4.78); 2.5210 (9.14); 1.5191 (16.00);

1.3792 (0.78); 1.2615 (1.92); 0.8795 (0.98)

›Example 40, Solvent: DMSO, Spectrometer: 399.95 MHz

9.7892 (1.97); 8.0289 (1.61); 8.0091 (1.98); 7.8398 (1.33); 7.8207 (1.78); 7.8003 (1.20); 7.7243 (2.79); 7.7204 (1.43); 7.7115 (0.91); 7.7064

(3.71); 7.7027 (2.50); 7.5638 (0.52); 7.5606 (0.36); 7.5518 (0.40); 7.5455 (1.71); 7.5398 (0.55); 7.5305 (0.92); 7.5272 (1.47); 7.5239 (0.78);

7.4957 (2.58); 7.4923 (1.14); 7.4802 (1.80); 7.4765 (3.26); 7.4629 (0.52); 7.4588 (1.29); 7.4557 (0.73); 7.1532 (1.79); 7.1357 (1.71); 5.3794

(6.29); 3.3277 (50.30); 3.0878 (0.59); 3.0757 (16.00); 2.8908 (1.39); 2.7321 (1.09); 2.7312 (1.09); 2.5250 (0.66); 2.5117 (12.62); 2.5072 (24.96);

2.5026 (32.84); 2.4980 (23.92); 2.4935 (11.50); 2.1329 (0.75); 2.1212 (0.72); 2.1045 (0.76); 2.0921 (0.69); 1.5114 (0.71); 1.4957 (0.88); 1.4756

(1.03); 1.4525 (0.48); 1.4384 (0.46); 1.3871 (0.33); 1.3621 (0.73); 1.3517 (0.68); 1.3366 (0.97); 1.2984 (1.77); 1.2716 (1.59); 1.2531 (0.78);

1.2457 (0.85); 1.2378 (0.87); 1.1964 (11.91); 1.1791 (0.56); 1.0784 (1.14); 0.8758 (0.58); 0.8623 (0.36); 0.0080 (0.45); −0.0002 (12.32); −0.0085

(0.41)

›Example 41, Solvent: DMSO, Spectrometer: 400.13 MHz

11.7635 (1.63); 7.6175 (3.88); 7.5970 (4.40); 7.3056 (3.82); 7.2853 (3.30); 7.2404 (4.71); 5.2588 (7.03); 4.1594 (2.19); 4.1427 (4.54); 4.1260

(2.21); 3.4666 (0.54); 3.4647 (0.51); 3.4155 (8.00); 3.3657 (567.17); 3.3160 (5.69); 3.0145 (16.00); 2.6768 (0.48); 2.6722 (0.36); 2.5618 (0.82);

2.5576 (1.04); 2.5532 (0.80); 2.5120 (62.60); 2.5078 (80.97); 2.5037 (60.79); 2.4624 (0.90); 2.4583 (0.98); 2.3518 (11.48); 2.3347 (0.83);

1.9934 (0.53); 1.6405 (1.26); 1.6235 (1.99); 1.6063 (1.44); 1.5902 (0.51); 1.3285 (2.73); 1.3204 (4.35); 1.3110 (4.54); 1.3023 (3.00); 1.2702

(0.89); 1.2482 (2.14); 1.1781 (0.32); 0.8955 (2.32); 0.8782 (7.02); 0.8705 (2.97); 0.8613 (4.37); 0.8439 (1.25)

›Example 42, Solvent: DMSO, Spectrometer: 400.13 MHz

11.0254 (2.58); 8.1759 (1.76); 8.1554 (2.12); 7.9478 (1.32); 7.9283 (1.92); 7.9083 (1.24); 7.8924 (1.34); 7.8899 (1.11); 7.8729 (1.66); 7.8705

(1.45); 7.8610 (1.03); 7.8575 (0.71); 7.8421 (0.83); 7.8362 (0.96); 7.8320 (0.71); 7.6408 (0.66); 7.6367 (0.98); 7.6310 (0.91); 7.6199 (1.28);

7.6163 (1.45); 7.6113 (1.18); 7.6030 (2.24); 7.6008 (2.41); 7.5875 (0.76); 7.5819 (1.16); 7.5676 (1.38); 7.5624 (0.93); 7.5565 (0.92); 7.5501

(1.40); 7.5360 (1.28); 7.5309 (0.66); 7.5154 (0.61); 7.4861 (0.59); 7.4841 (0.64); 7.4795 (0.58); 7.4627 (1.00); 7.4573 (0.90); 7.4400 (0.81);

7.4371 (0.99); 7.4157 (0.94); 7.4120 (0.87); 7.3973 (0.43); 7.3948 (0.45); 7.3912 (0.42); 7.3887 (0.38); 7.2648 (1.94); 7.2466 (1.85); 5.4490

(6.50); 4.0438 (0.49); 4.0260 (0.50); 3.3947 (0.56); 3.3445 (30.39); 3.2944 (0.40); 3.0831 (16.00); 2.5647 (0.40); 2.5602 (0.50); 2.5323 (0.59);

2.5186 (12.69); 2.5143 (26.30); 2.5099 (35.79); 2.5054 (25.86); 2.5011 (12.23); 2.4644 (0.36); 2.4598 (0.39); 1.9965 (2.17); 1.2490 (0.82);

1.1987 (0.60); 1.1809 (1.16); 1.1631 (0.56); 0.8798 (0.37); 0.8631 (1.17); 0.8455 (0.46)

›Example 43, Solvent: DMSO, Spectrometer: 400.13 MHz

7.7323 (2.93); 7.7195 (0.96); 7.7145 (3.65); 7.7108 (2.62); 7.5658 (0.54); 7.5627 (0.37); 7.5542 (0.45); 7.5475 (1.78); 7.5418 (0.57); 7.5327

(1.08); 7.5294 (1.59); 7.5261 (0.85); 7.5023 (2.72); 7.4870 (1.88); 7.4832 (3.39); 7.4697 (0.57); 7.4657 (1.30); 7.4623 (0.78); 7.3826 (1.70);

7.3779 (1.99); 7.3746 (2.56); 7.3615 (3.01); 7.3567 (3.52); 7.3439 (1.57); 7.2839 (1.87); 7.2796 (0.72); 7.2656 (3.56); 7.2463 (1.91); 7.1900

(1.24); 7.1870 (0.76); 7.1765 (0.61); 7.1718 (1.68); 7.1668 (0.48); 7.1536 (0.59); 7.0849 (1.44); 7.0648 (1.49); 6.4965 (2.07); 6.4788 (1.99);

6.4067 (1.60); 6.3858 (1.55); 5.1787 (6.38); 5.0182 (0.49); 5.0001 (0.70); 4.9823 (0.48); 3.3856 (0.80); 3.3356 (42.56); 3.3119 (0.34); 3.2856

(0.63); 2.9802 (16.00); 2.5186 (4.40); 2.5142 (8.84); 2.5097 (11.86); 2.5053 (8.48); 2.5009 (3.99); 1.9177 (0.32); 1.4203 (5.64); 1.4031 (5.60)

›Example 44, Solvent: DMSO, Spectrometer: 399.95 MHz

10.8984 (2.13); 8.1729 (1.55); 8.1528 (1.85); 7.9531 (0.60); 7.9259 (1.20); 7.9065 (1.70); 7.8863 (1.11); 7.7360 (2.46); 7.7322 (1.21); 7.7235

(0.71); 7.7183 (3.19); 7.7146 (2.25); 7.6143 (1.14); 7.6119 (0.98); 7.5953 (3.17); 7.5888 (1.86); 7.5676 (0.46); 7.5558 (0.32); 7.5493 (1.55);

7.5436 (0.46); 7.5344 (0.84); 7.5311 (1.37); 7.5277 (0.69); 7.5013 (2.26); 7.4979 (0.98); 7.4859 (1.52); 7.4821 (2.90); 7.4685 (0.44); 7.4645

(1.15); 7.4612 (0.65); 7.4367 (1.07); 7.4165 (1.89); 7.3971 (1.13); 7.2329 (1.70); 7.2149 (1.65); 7.1635 (0.94); 7.1615 (1.01); 7.1571 (0.97);

7.1551 (0.93); 7.1430 (0.79); 7.1404 (0.80); 7.1370 (0.80); 7.1344 (0.73); 5.4218 (5.82); 3.8501 (16.00); 3.8030 (0.36); 3.3414 (75.06); 3.0860

(14.99); 2.8908 (4.68); 2.7323 (3.81); 2.7313 (3.75); 2.5257 (0.56); 2.5209 (0.89); 2.5124 (10.84); 2.5079 (21.59); 2.5034 (28.45); 2.4988

(20.65); 2.4943 (9.83); −0.0002 (2.50)

›Example 45, Solvent: DMSO, Spectrometer: 399.95 MHz

10.1700 (2.41); 7.9533 (0.33); 7.8296 (0.37); 7.8086 (2.07); 7.8002 (2.23); 7.7940 (5.01); 7.7793 (0.42); 7.7250 (1.89); 7.7224 (2.42); 7.7186

(1.20); 7.7099 (0.75); 7.7047 (3.18); 7.7010 (2.23); 7.5626 (0.46); 7.5508 (0.35); 7.5443 (1.53); 7.5385 (0.47); 7.5294 (0.83); 7.5260 (1.34);

7.5226 (0.69); 7.4957 (2.25); 7.4923 (0.99); 7.4803 (1.55); 7.4766 (2.88); 7.4630 (0.44); 7.4589 (1.14); 7.4557 (0.64); 7.1023 (1.23); 7.0959

(1.22); 7.0879 (1.05); 7.0815 (1.16); 5.3309 (6.06); 4.0886 (1.69); 4.0718 (3.60); 4.0549 (1.71); 3.3454 (102.18); 3.0662 (14.92); 2.8915 (2.58);

2.7329 (2.10); 2.7317 (2.05); 2.5263 (0.57); 2.5130 (9.66); 2.5086 (19.08); 2.5040 (25.08); 2.4994 (18.29); 2.4948 (8.80); 1.6430 (0.43); 1.6259

(1.03); 1.6119 (0.85); 1.6067 (1.14); 1.5995 (0.86); 1.5861 (1.36); 1.5686 (1.08); 1.5515 (0.95); 1.5348 (0.80); 1.5182 (0.43); 1.2581 (1.01);

1.2450 (0.92); 1.2408 (1.40); 1.2381 (1.35); 1.2324 (0.97); 1.2283 (0.83); 1.2188 (1.38); 1.2013 (0.73); 0.8893 (0.94); 0.8808 (16.00); 0.8731

(1.37); 0.8643 (15.22); −0.0002 (1.46)

›Example 46, Solvent: DMSO, Spectrometer: 399.95 MHz

11.0119 (1.84); 8.0896 (0.97); 8.0687 (1.17); 7.9529 (1.27); 7.8574 (1.18); 7.8381 (1.61); 7.8178 (1.08); 7.7108 (1.82); 7.7083 (2.40); 7.7045

(1.13); 7.6955 (0.72); 7.6905 (3.19); 7.6867 (2.22); 7.5581 (0.48); 7.5549 (0.32); 7.5459 (0.37); 7.5398 (1.54); 7.5342 (0.49); 7.5247 (0.81);

7.5214 (1.29); 7.5180 (0.65); 7.4867 (2.20); 7.4832 (0.91); 7.4712 (1.56); 7.4675 (2.88); 7.4538 (0.46); 7.4498 (1.17); 7.4467 (0.65); 7.3600

(0.94); 7.3575 (0.84); 7.3465 (16.00); 7.3391 (7.90); 7.3325 (7.19); 7.3258 (0.98); 7.3181 (1.80); 7.3142 (1.05); 7.3116 (1.13); 7.2767 (1.35);

7.2697 (1.65); 7.2631 (1.38); 7.2609 (1.35); 7.2550 (1.78); 7.2473 (0.99); 7.2413 (0.72); 7.2336 (0.47); 7.1685 (1.64); 7.1507 (1.59); 5.4111

(1.96); 5.3530 (5.42); 4.1499 (0.33); 4.1321 (0.33); 3.3723 (0.49); 3.3414 (160.75); 3.0220 (15.01); 2.8903 (10.82); 2.7319 (8.39); 2.7310 (8.34);

2.5255 (0.83); 2.5207 (1.35); 2.5122 (15.28); 2.5076 (30.21); 2.5030 (39.63); 2.4984 (28.45); 2.4939 (13.26); 1.1843 (0.35); 1.1666 (0.74);

1.1488 (0.36); −0.0002 (8.12)

›Example 47, Solvent: DMSO, Spectrometer: 399.95 MHz

11.7568 (1.08); 7.7382 (0.48); 7.7303 (2.52); 7.7174 (1.00); 7.7123 (3.26); 7.7085 (2.27); 7.5623 (0.53); 7.5590 (0.36); 7.5508 (0.41); 7.5440

(1.80); 7.5381 (0.56); 7.5293 (1.03); 7.5259 (1.61); 7.5224 (0.80); 7.4998 (2.66); 7.4965 (1.17); 7.4847 (1.78); 7.4808 (3.32); 7.4674 (0.54);

7.4633 (1.30); 7.4597 (0.76); 7.2522 (3.78); 5.2823 (5.46); 4.1986 (1.61); 4.1815 (3.38); 4.1644 (1.62); 4.0909 (0.42); 4.0374 (0.33); 4.0220

(0.34); 3.9781 (0.34); 3.9613 (0.33); 3.3283 (60.16); 3.0484 (0.43); 3.0294 (13.57); 2.9949 (0.45); 2.8908 (2.32); 2.7321 (1.85); 2.7310 (1.78);

2.5250 (0.60); 2.5202 (1.00); 2.5117 (13.08); 2.5071 (26.34); 2.5025 (34.91); 2.4979 (25.44); 2.4934 (12.20); 1.6951 (0.60); 1.6782 (0.78);

1.6614 (0.69); 1.6447 (0.43); 1.5447 (1.01); 1.5277 (2.84); 1.5106 (2.51); 1.4933 (0.84); 1.4862 (0.37); 1.2348 (0.38); 1.1205 (0.57); 1.1053

(0.57); 0.9225 (0.69); 0.9097 (16.00); 0.8931 (15.47); 0.8788 (2.11); 0.8725 (1.79); 0.8603 (1.01); 0.8137 (0.96); 0.8064 (0.35); 0.7971 (0.92);

0.7900 (0.36); 0.0080 (0.40); −0.0002 (12.62); −0.0085 (0.42)

›Example 48, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5510 (1.98); 8.0744 (1.17); 8.0536 (1.40); 7.8447 (1.34); 7.8253 (1.81); 7.8052 (1.17); 7.7233 (2.71); 7.7196 (1.30); 7.7104 (0.82); 7.7055

(3.48); 7.7017 (2.39); 7.5639 (0.49); 7.5520 (0.36); 7.5455 (1.69); 7.5399 (0.48); 7.5306 (0.89); 7.5273 (1.42); 7.5240 (0.73); 7.4964 (2.50);

7.4808 (1.71); 7.4772 (3.18); 7.4635 (0.49); 7.4595 (1.22); 7.4564 (0.70); 7.1539 (1.85); 7.1357 (1.74); 5.3768 (0.36); 5.3585 (6.41); 3.6536

(1.84); 3.6379 (4.14); 3.6223 (1.96); 3.4447 (1.40); 3.4272 (4.47); 3.4097 (4.54); 3.3922 (1.48); 3.3337 (93.21); 3.0551 (16.00); 2.8906 (1.56);

2.7311 (1.26); 2.6422 (1.75); 2.6266 (3.60); 2.6109 (1.65); 2.5252 (0.55); 2.5118 (11.81); 2.5074 (23.64); 2.5028 (31.28); 2.4982 (22.84);

2.4937 (10.97); 1.0934 (4.59); 1.0759 (9.31); 1.0584 (4.44); −0.0002 (5.00)

›Example 49, Solvent: DMSO, Spectrometer: 399.95 MHz

10.2863 (2.97); 7.9533 (0.95); 7.8241 (0.78); 7.8031 (1.97); 7.7856 (2.37); 7.7725 (2.64); 7.7537 (1.10); 7.7217 (3.16); 7.7037 (3.78); 7.7001

(2.94); 7.6773 (0.33); 7.5623 (0.72); 7.5593 (0.63); 7.5446 (4.04); 7.5258 (1.82); 7.4949 (2.93); 7.4756 (3.65); 7.4579 (1.56); 7.4307 (1.31);

7.4111 (1.55); 7.3381 (1.16); 7.3189 (2.10); 7.2857 (2.27); 7.2664 (2.76); 7.2613 (1.04); 7.2466 (1.27); 7.1057 (1.74); 7.1035 (1.80); 7.0884

(1.71); 7.0861 (1.70); 5.3324 (7.17); 5.3085 (0.52); 4.3076 (1.89); 4.2910 (4.10); 4.2744 (2.04); 3.3303 (65.47); 3.3068 (4.07); 3.0606 (16.00);

3.0371 (0.88); 3.0206 (0.32); 3.0046 (0.32); 2.9542 (1.75); 2.9377 (3.46); 2.9213 (1.76); 2.8906 (6.69); 2.8670 (0.33); 2.7316 (5.59); 2.5112

(17.01); 2.5072 (30.80); 2.5027 (39.61); 2.4983 (29.86); 2.4795 (3.61); 1.2347 (0.39); 0.0075 (0.44); −0.0002 (6.95); −0.0082 (0.42)

›Example 50, Solvent: DMSO, Spectrometer: 399.95 MHz

12.5452 (0.92); 7.9531 (0.69); 7.7390 (1.89); 7.7362 (2.54); 7.7323 (1.20); 7.7239 (0.75); 7.7187 (3.36); 7.7149 (2.29); 7.5664 (0.47); 7.5549

(0.33); 7.5481 (1.60); 7.5422 (0.48); 7.5334 (0.88); 7.5300 (1.44); 7.5264 (0.71); 7.5035 (2.35); 7.5001 (0.98); 7.4885 (1.53); 7.4845 (2.93);

7.4711 (0.46); 7.4670 (1.18); 7.4635 (0.64); 7.3334 (4.28); 7.1878 (0.92); 7.1675 (1.79); 7.1483 (0.76); 7.1463 (0.93); 6.5383 (0.76); 6.5358

(0.89); 6.5334 (0.98); 6.5309 (1.00); 6.5163 (0.79); 6.5118 (1.14); 6.5106 (1.09); 6.4930 (0.98); 6.4866 (2.77); 6.4834 (3.02); 6.4656 (1.11);

6.4598 (0.75); 5.3393 (5.31); 5.0533 (0.34); 5.0369 (1.31); 5.0204 (1.32); 5.0038 (0.34); 3.6961 (16.00); 3.3466 (81.44); 3.0198 (0.71); 3.0116

(15.09); 2.8909 (5.66); 2.7329 (4.46); 2.7317 (4.50); 2.5266 (0.40); 2.5217 (0.63); 2.5132 (8.04); 2.5087 (16.11); 2.5041 (21.24); 2.4994 (15.32);

2.4949 (7.20); 1.5351 (4.98); 1.5186 (4.92); −0.0002 (1.37)

›Example 51, Solvent: DMSO, Spectrometer: 399.95 MHz

10.6093 (1.98); 8.0360 (0.78); 8.0154 (0.99); 7.9529 (0.47); 7.8853 (1.19); 7.8660 (1.63); 7.8458 (1.02); 7.7312 (1.80); 7.7287 (2.34); 7.7248

(1.12); 7.7160 (0.68); 7.7109 (3.10); 7.7071 (2.15); 7.5671 (0.44); 7.5488 (1.49); 7.5431 (0.43); 7.5338 (0.79); 7.5305 (1.29); 7.5271 (0.63);

7.4993 (2.15); 7.4958 (0.89); 7.4838 (1.48); 7.4801 (2.78); 7.4665 (0.42); 7.4624 (1.13); 7.4592 (0.61); 7.2131 (1.01); 7.2054 (1.79); 7.1976

(0.51); 7.1935 (1.04); 7.1885 (1.85); 7.1714 (1.26); 6.5619 (0.61); 6.5590 (0.91); 6.5572 (0.94); 6.5543 (1.15); 6.5382 (4.39); 6.5340 (3.31);

6.5272 (0.69); 6.5232 (1.17); 6.5201 (0.90); 6.5153 (0.44); 5.3850 (5.51); 4.7744 (5.49); 3.7264 (16.00); 3.3359 (75.79); 3.0697 (14.58); 2.8905

(3.90); 2.7320 (3.10); 2.7309 (3.03); 2.5253 (0.55); 2.5205 (0.87); 2.5119 (10.89); 2.5074 (21.83); 2.5028 (28.72); 2.4982 (20.67); 2.4937

(9.70); −0.0002 (2.40)

›Example 52, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5643 (1.54); 8.0510 (0.88); 8.0302 (1.05); 7.9531 (0.40); 7.8350 (1.27); 7.8157 (1.73); 7.7955 (1.16); 7.7264 (1.89); 7.7239 (2.51); 7.7200

(1.26); 7.7113 (0.78); 7.7061 (3.47); 7.7024 (2.31); 7.5651 (0.48); 7.5533 (0.35); 7.5468 (1.58); 7.5411 (0.47); 7.5319 (0.85); 7.5286 (1.40);

7.5251 (0.70); 7.4982 (2.36); 7.4947 (1.02); 7.4829 (1.58); 7.4791 (2.98); 7.4655 (0.46); 7.4614 (1.19); 7.4582 (0.66); 7.1454 (1.72); 7.1281

(1.65); 5.3545 (6.40); 3.3372 (100.07); 3.0527 (16.00); 2.8909 (3.30); 2.7322 (2.56); 2.7312 (2.58); 2.5257 (0.58); 2.5208 (0.94); 2.5123 (10.62);

2.5078 (21.02); 2.5032 (27.63); 2.4986 (19.95); 2.4941 (9.41); 2.0857 (14.04); 2.0777 (0.59); 1.2832 (0.34); 0.8757 (0.59); 0.8624

(0.34); −0.0002 (5.06)

›Example 53, Solvent: DMSO, Spectrometer: 399.95 MHz

11.7519 (1.32); 7.7380 (0.41); 7.7325 (2.01); 7.7297 (2.63); 7.7258 (1.33); 7.7173 (0.93); 7.7121 (3.48); 7.7083 (2.41); 7.5624 (0.50); 7.5591

(0.34); 7.5509 (0.37); 7.5441 (1.71); 7.5382 (0.54); 7.5293 (0.98); 7.5259 (1.56); 7.5224 (0.79); 7.4998 (2.58); 7.4965 (1.15); 7.4848 (1.73);

7.4808 (3.20); 7.4674 (0.55); 7.4633 (1.31); 7.4598 (0.78); 7.2507 (4.08); 5.2821 (5.73); 4.1571 (1.77); 4.1404 (3.86); 4.1237 (1.81); 4.0502

(0.37); 3.3370 (86.57); 3.3043 (0.38); 3.0488 (0.33); 3.0295 (16.00); 3.0146 (0.37); 2.9877 (0.47); 2.8913 (0.81); 2.7326 (0.65); 2.7313 (0.62);

2.5257 (0.61); 2.5209 (1.02); 2.5124 (11.52); 2.5079 (22.88); 2.5033 (30.10); 2.4987 (21.78); 2.4942 (10.36); 1.6314 (1.02); 1.6143 (1.43);

1.5950 (1.25); 1.5781 (0.49); 1.3518 (0.70); 1.3353 (0.97); 1.3314 (0.95); 1.3223 (0.83); 1.3134 (1.16); 1.2903 (3.23); 1.2809 (2.75); 1.2740

(3.07); 1.2660 (1.70); 1.2563 (0.99); 1.2351 (0.45); 1.1207 (0.63); 1.1055 (0.61); 0.8872 (0.61); 0.8813 (1.73); 0.8643 (5.42); 0.8471 (1.72);

0.8205 (0.38); 0.0080 (0.34); −0.0002 (9.49)

›Example 54, Solvent: DMSO, Spectrometer: 399.95 MHz

10.8752 (2.27); 8.1766 (1.70); 8.1563 (2.02); 8.0342 (2.65); 8.0211 (0.79); 8.0164 (3.14); 8.0128 (2.29); 7.9532 (0.73); 7.9258 (1.33); 7.9064

(1.86); 7.8862 (1.22); 7.7463 (0.35); 7.7381 (2.65); 7.7343 (1.30); 7.7254 (0.83); 7.7203 (3.41); 7.7164 (2.36); 7.6198 (0.34); 7.6167 (0.58);

7.6136 (0.34); 7.6037 (0.42); 7.5984 (1.65); 7.5933 (0.49); 7.5831 (0.76); 7.5800 (1.27); 7.5768 (0.69); 7.5678 (0.51); 7.5646 (0.36); 7.5559

(0.37); 7.5493 (1.73); 7.5437 (0.58); 7.5343 (1.33); 7.5306 (3.22); 7.5102 (3.39); 7.5018 (2.63); 7.4981 (1.28); 7.4922 (1.57); 7.4897 (1.24);

7.4866 (1.85); 7.4825 (3.17); 7.4690 (0.49); 7.4649 (1.22); 7.4617 (0.68); 7.2313 (1.86); 7.2131 (1.77); 5.4203 (6.48); 3.3357 (90.19); 3.0861

(16.00); 3.0220 (0.36); 2.8906 (5.67); 2.7315 (4.54); 2.5254 (0.57); 2.5121 (11.61); 2.5076 (23.03); 2.5030 (30.30); 2.4984 (21.97); 2.4939

(10.47); 0.0079 (0.38); −0.0002 (10.47)

›Example 55, Solvent: DMSO, Spectrometer: 399.95 MHz

12.4362 (0.68); 7.9524 (1.44); 7.7380 (2.85); 7.7342 (1.42); 7.7203 (3.63); 7.7165 (2.58); 7.5670 (0.50); 7.5638 (0.34); 7.5556 (0.35); 7.5486

(1.84); 7.5428 (0.55); 7.5340 (0.99); 7.5306 (1.65); 7.5272 (0.85); 7.5050 (2.80); 7.4899 (1.79); 7.4858 (3.72); 7.4764 (4.26); 7.4708 (1.70);

7.4687 (1.70); 7.4650 (0.98); 7.4594 (1.36); 7.4538 (4.56); 7.4451 (0.42); 7.3375 (5.05); 6.9640 (0.40); 6.9553 (4.29); 6.9497 (1.30); 6.9382

(1.24); 6.9326 (4.04); 6.9239 (0.52); 5.3415 (6.44); 4.9711 (0.83); 4.8566 (7.26); 3.3437 (154.86); 3.0349 (2.07); 3.0231 (16.00); 3.0083 (0.42);

2.8908 (11.54); 2.7312 (9.32); 2.5257 (0.83); 2.5208 (1.37); 2.5123 (16.37); 2.5078 (32.60); 2.5033 (43.10); 2.4987 (31.36); 2.4942

(14.97); −0.0002 (1.53)

›Example 56, Solvent: DMSO, Spectrometer: 399.95 MHz

10.1719 (2.73); 7.9534 (0.38); 7.8298 (0.35); 7.8088 (2.32); 7.8018 (2.45); 7.7949 (5.68); 7.7808 (0.42); 7.7247 (1.99); 7.7222 (2.56); 7.7183

(1.24); 7.7095 (0.78); 7.7044 (3.43); 7.7006 (2.37); 7.5624 (0.48); 7.5506 (0.36); 7.5441 (1.64); 7.5384 (0.48); 7.5292 (0.88); 7.5259 (1.41);

7.5225 (0.71); 7.4954 (2.38); 7.4920 (1.00); 7.4801 (1.64); 7.4763 (3.06); 7.4627 (0.47); 7.4587 (1.22); 7.4554 (0.67); 7.1020 (1.29); 7.0950

(1.27); 7.0882 (1.09); 7.0812 (1.23); 5.3304 (6.47); 4.1488 (0.95); 4.1424 (1.15); 4.1333 (1.24); 4.1299 (1.20); 4.1248 (2.03); 4.1153 (1.01);

4.1079 (0.85); 3.3424 (114.20); 3.0653 (16.00); 2.8915 (3.12); 2.7327 (2.47); 2.7318 (2.36); 2.5263 (0.49); 2.5214 (0.79); 2.5130 (9.87); 2.5084

(19.71); 2.5038 (26.01); 2.4992 (18.86); 2.4947 (8.98); 1.6653 (0.35); 1.6526 (0.68); 1.6334 (0.71); 1.6208 (0.57); 1.4904 (0.49); 1.4735 (0.58);

1.4588 (0.69); 1.4426 (0.85); 1.4272 (0.79); 1.4101 (0.63); 1.3907 (0.44); 1.3838 (0.42); 1.3702 (0.43); 1.3652 (0.46); 1.3509 (0.73); 1.3373

(0.54); 1.3318 (0.64); 1.3186 (0.50); 1.1993 (0.56); 1.1809 (0.89); 1.1654 (0.63); 1.1628 (0.70); 1.1473 (0.72); 1.1291 (0.46); 0.8923 (7.35);

0.8761 (7.67); 0.8715 (4.41); 0.8529 (8.39); 0.8344 (3.20); −0.0002 (1.69)

›Example 57, Solvent: DMSO, Spectrometer: 399.95 MHz

12.7535 (1.68); 7.9525 (1.45); 7.7420 (2.08); 7.7392 (2.76); 7.7354 (1.45); 7.7267 (0.89); 7.7216 (3.48); 7.7179 (2.59); 7.6441 (1.18); 7.6411

(1.29); 7.6255 (1.55); 7.6220 (1.61); 7.5952 (0.64); 7.5922 (0.83); 7.5751 (2.18); 7.5722 (2.29); 7.5651 (1.69); 7.5610 (1.41); 7.5541 (0.53);

7.5472 (3.21); 7.5432 (1.86); 7.5324 (1.09); 7.5289 (1.86); 7.5231 (0.93); 7.5037 (2.59); 7.5005 (1.29); 7.4886 (1.81); 7.4846 (3.59); 7.4789

(1.79); 7.4713 (0.72); 7.4670 (1.75); 7.4640 (2.20); 7.4609 (1.68); 7.4461 (0.72); 7.4424 (0.68); 7.3992 (4.05); 5.3631 (6.03); 3.3442 (117.73);

3.0457 (16.00); 2.8909 (10.77); 2.7322 (9.09); 2.7308 (8.86); 2.5255 (0.68); 2.5121 (13.58); 2.5076 (26.45); 2.5031 (34.39); 2.4985 (25.53);

2.4941 (12.66); −0.0002 (1.25)

›Example 58, Solvent: DMSO, Spectrometer: 400.13 MHz

10.3551 (0.43); 10.3115 (7.26); 8.3851 (0.33); 7.8845 (0.33); 7.8375 (2.37); 7.8176 (5.07); 7.8004 (10.27); 7.7837 (14.27); 7.7641 (2.76);

7.7411 (0.59); 7.7194 (0.39); 7.6537 (0.36); 7.6311 (1.91); 7.5722 (1.56); 7.5538 (4.13); 7.5356 (3.52); 7.5062 (6.33); 7.4897 (9.13); 7.4868

(9.11); 7.4686 (2.99); 7.3490 (2.16); 7.0658 (4.27); 7.0485 (4.20); 5.4362 (0.72); 5.3459 (16.00); 4.1885 (4.96); 4.1719 (10.50); 4.1553 (5.32);

4.0587 (0.57); 4.0402 (1.80); 4.0225 (1.70); 4.0046 (0.59); 3.4983 (1.04); 3.4907 (1.16); 3.3563 (2317.28); 3.3345 (45.91); 3.2320 (2.12);

3.1656 (0.62); 3.1409 (0.47); 2.9133 (3.25); 2.9069 (6.58); 2.9004 (3.36); 2.8852 (0.35); 2.6755 (1.96); 2.5706 (4.74); 2.5644 (5.28); 2.5541

(9.00); 2.5474 (9.66); 2.5371 (8.98); 2.5099 (258.76); 2.5063 (322.76); 2.3327 (2.37); 2.2491 (0.34); 2.2060 (0.33); 2.0761 (0.56); 1.9924 (7.15);

1.2839 (0.38); 1.2486 (1.45); 1.1947 (1.94); 1.1771 (3.72); 1.1597 (1.92); 0.8735 (0.54); 0.8609 (1.48); 0.8452 (0.66)

›Example 59, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5388 (0.75); 8.0594 (0.45); 8.0386 (0.54); 7.8303 (0.47); 7.8109 (0.66); 7.7907 (0.43); 7.7245 (0.97); 7.7208 (0.48); 7.7068 (1.25); 7.7030

(0.88); 7.5464 (0.61); 7.5315 (0.33); 7.5282 (0.52); 7.4973 (0.90); 7.4940 (0.39); 7.4818 (0.62); 7.4781 (1.15); 7.4605 (0.45); 7.1379 (0.67);

7.1202 (0.64); 5.3552 (2.34); 3.3292 (18.57); 3.0546 (5.87); 2.8908 (1.64); 2.7320 (1.30); 2.7312 (1.29); 2.5118 (4.25); 2.5073 (8.32); 2.5027

(10.90); 2.4981 (7.96); 2.4937 (3.84); 2.3834 (0.64); 2.3680 (0.42); 2.3632 (0.67); 2.3574 (0.40); 2.3426 (0.70); 1.5193 (0.79); 1.5043 (0.43);

1.4985 (0.70); 1.4938 (0.45); 1.4784 (0.71); 0.8796 (16.00); −0.0002 (2.86)

›Example 60, Solvent: DMSO, Spectrometer: 399.95 MHz

10.1438 (2.72); 7.9531 (0.74); 7.8047 (0.76); 7.7837 (1.74); 7.7659 (1.99); 7.7503 (2.03); 7.7479 (2.29); 7.7295 (1.23); 7.7256 (2.45); 7.7228

(2.81); 7.7190 (1.38); 7.7101 (0.84); 7.7050 (3.53); 7.7012 (2.48); 7.5639 (0.49); 7.5608 (0.33); 7.5521 (0.36); 7.5456 (1.65); 7.5399 (0.53);

7.5307 (0.89); 7.5274 (1.45); 7.5240 (0.77); 7.4969 (2.52); 7.4936 (1.11); 7.4815 (1.70); 7.4777 (3.18); 7.4642 (0.52); 7.4601 (1.26); 7.4569

(0.73); 7.3101 (0.46); 7.3038 (0.33); 7.2930 (9.21); 7.2820 (8.50); 7.2638 (0.72); 7.2601 (0.83); 7.2449 (0.55); 7.2422 (0.72); 7.2205 (0.95);

7.2094 (1.08); 7.1984 (1.23); 7.1881 (0.72); 7.1849 (0.76); 7.1770 (0.36); 7.0919 (1.53); 7.0894 (1.59); 7.0743 (1.51); 7.0717 (1.48); 5.3278

(6.23); 5.0059 (0.52); 4.9908 (0.98); 4.9752 (0.97); 4.9584 (0.54); 3.3899 (0.38); 3.3485 (165.03); 3.0645 (16.00); 2.9281 (0.69); 2.9105 (0.55);

2.8909 (6.45); 2.8830 (0.37); 2.8765 (1.32); 2.8570 (1.29); 2.8427 (1.37); 2.8229 (0.57); 2.8087 (0.50); 2.7317 (4.89); 2.5263 (0.65); 2.5130

(12.58); 2.5085 (25.04); 2.5039 (32.97); 2.4993 (24.03); 2.4948 (11.56); 1.3012 (0.99); 1.2855 (0.98); 1.2321 (6.28); 1.2165 (6.11); −0.0002

(3.72)

›Example 61, Solvent: DMSO, Spectrometer: 400.13 MHz

10.0934 (6.86); 7.8319 (1.42); 7.8110 (4.22); 7.7939 (6.37); 7.7908 (5.85); 7.7869 (5.91); 7.7696 (1.74); 7.7660 (1.14); 7.7264 (6.39); 7.7086

(7.84); 7.7049 (5.67); 7.5741 (1.13); 7.5711 (0.81); 7.5623 (1.04); 7.5558 (3.81); 7.5501 (1.31); 7.5409 (2.36); 7.5377 (3.40); 7.5345 (1.89);

7.5102 (5.90); 7.4947 (4.24); 7.4911 (7.16); 7.4775 (1.33); 7.4735 (2.74); 7.4703 (1.67); 7.0919 (3.36); 7.0884 (3.37); 7.0751 (3.21); 7.0716

(3.13); 5.7665 (4.63); 5.3415 (14.80); 4.6794 (1.01); 4.6671 (1.18); 4.6570 (1.86); 4.6476 (1.36); 4.6348 (0.92); 4.6254 (0.51); 3.5308 (1.95);

3.5127 (6.35); 3.4945 (6.46); 3.4764 (2.02); 3.3905 (1.14); 3.3406 (77.67); 3.3170 (0.72); 3.2904 (0.93); 2.5603 (0.43); 2.5558 (0.33); 2.5189

(12.38); 2.5147 (23.99); 2.5103 (31.66); 2.5059 (22.93); 2.5018 (11.08); 2.4647 (0.37); 2.4603 (0.42); 1.8689 (1.91); 1.8563 (2.21); 1.8423

(2.28); 1.7304 (1.91); 1.7221 (2.06); 1.7079 (2.22); 1.5236 (1.00); 1.5147 (1.06); 1.4936 (1.18); 1.4677 (1.05); 1.4594 (0.94); 1.4351 (2.23);

1.4106 (2.82); 1.3851 (2.90); 1.3719 (1.69); 1.3584 (2.54); 1.3327 (2.03); 1.3265 (2.22); 1.3007 (1.22); 1.2813 (1.02); 1.2507 (1.38); 1.2405

(1.27); 1.2271 (1.08); 1.2097 (0.64); 1.0652 (7.47); 1.0471 (16.00); 1.0289 (6.94)

›Example 62, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5328 (2.07); 8.0693 (1.32); 8.0486 (1.57); 7.8330 (1.31); 7.8136 (1.87); 7.7934 (1.20); 7.7231 (2.73); 7.7103 (0.86); 7.7053 (3.48); 7.7016

(2.44); 7.5649 (0.51); 7.5618 (0.33); 7.5530 (0.39); 7.5466 (1.69); 7.5410 (0.50); 7.5316 (0.93); 7.5284 (1.45); 7.5251 (0.74); 7.4975 (2.52);

7.4820 (1.78); 7.4783 (3.18); 7.4646 (0.51); 7.4606 (1.23); 7.4575 (0.70); 7.1408 (1.90); 7.1228 (1.81); 5.3557 (6.62); 3.3433 (112.40); 3.3109

(0.36); 3.0531 (16.00); 2.8912 (2.26); 2.7317 (1.85); 2.5260 (0.67); 2.5127 (11.48); 2.5083 (22.15); 2.5038 (28.70); 2.4992 (20.81); 2.4947

(9.94); 2.4795 (1.96); 2.4612 (2.90); 2.4422 (1.93); 1.5070 (0.98); 1.4890 (2.25); 1.4702 (2.27); 1.4523 (0.95); 0.7231 (0.43); 0.7173 (0.39);

0.7133 (0.34); 0.7054 (0.72); 0.6975 (0.35); 0.6929 (0.41); 0.6858 (0.47); 0.3938 (0.77); 0.3836 (2.14); 0.3794 (2.21); 0.3738 (0.95); 0.3696

(1.05); 0.3635 (2.15); 0.3593 (1.96); 0.3496 (0.76); 0.0611 (0.78); 0.0509 (2.30); 0.0475 (2.45); 0.0388 (2.25); 0.0353 (2.26); 0.0247

(0.62); −0.0002 (7.48)

›Example 63, Solvent: DMSO, Spectrometer: 399.95 MHz

10.7229 (1.56); 8.3829 (0.46); 8.3620 (0.86); 8.3425 (0.72); 8.1789 (0.32); 8.1410 (0.89); 8.1381 (1.02); 8.1203 (1.17); 8.1168 (1.00); 8.0789

(0.75); 8.0583 (0.93); 7.9526 (0.74); 7.8660 (1.20); 7.8468 (1.58); 7.8266 (1.03); 7.8158 (0.33); 7.7972 (0.67); 7.7787 (0.45); 7.7418 (1.63);

7.7238 (4.26); 7.7048 (3.39); 7.7011 (2.36); 7.6486 (1.05); 7.6443 (0.96); 7.6280 (1.50); 7.6139 (0.47); 7.6095 (0.91); 7.6029 (0.45); 7.5997

(0.60); 7.5965 (0.48); 7.5870 (0.60); 7.5815 (1.82); 7.5763 (1.12); 7.5628 (2.00); 7.5524 (0.57); 7.5461 (1.90); 7.5403 (0.71); 7.5310 (1.15);

7.5276 (2.01); 7.5236 (2.14); 7.5025 (2.77); 7.4967 (2.92); 7.4886 (0.89); 7.4811 (3.37); 7.4774 (3.94); 7.4616 (3.04); 7.4481 (1.05); 7.4448

(1.04); 7.4401 (0.98); 7.4317 (0.53); 7.1885 (0.53); 7.1743 (1.79); 7.1567 (1.68); 7.0494 (0.33); 7.0316 (0.33); 6.4903 (0.70); 6.4782 (0.32);

6.4718 (0.72); 5.7781 (2.99); 5.3760 (1.33); 5.3658 (5.60); 4.7148 (0.79); 4.6973 (1.38); 4.6802 (0.92); 4.6669 (0.42); 4.6478 (0.39); 3.8819

(1.66); 3.8662 (3.52); 3.8506 (1.79); 3.3707 (8.60); 3.3284 (192.98); 3.0960 (10.49); 3.0593 (7.61); 3.0555 (16.00); 3.0523 (4.74); 3.0422 (1.91);

2.9579 (1.08); 2.9400 (1.91); 2.9263 (2.53); 2.9109 (3.38); 2.8950 (1.87); 2.8905 (6.69); 2.7503 (0.46); 2.7312 (5.05); 2.6802 (0.34); 2.6756

(0.73); 2.6710 (1.00); 2.6665 (0.70); 2.5244 (2.72); 2.5196 (4.18); 2.5111 (55.95); 2.5065 (113.37); 2.5019 (151.00); 2.4973 (109.61); 2.4928

(52.06); 2.3377 (0.37); 2.3333 (0.75); 2.3287 (1.02); 2.3241 (0.74); 2.3196 (0.35); 1.9090 (0.74); 1.2358 (1.11); 0.8539 (0.35); 0.0080

(1.83); −0.0002 (57.04); −0.0085 (1.68)

›Example 64, Solvent: DMSO, Spectrometer: 399.95 MHz

10.8680 (2.25); 8.0124 (1.32); 7.9918 (1.74); 7.9532 (0.79); 7.8730 (1.39); 7.8537 (1.92); 7.8335 (1.16); 7.7274 (2.81); 7.7144 (0.88); 7.7095

(3.56); 7.7058 (2.55); 7.5678 (0.51); 7.5647 (0.33); 7.5557 (0.40); 7.5494 (1.73); 7.5439 (0.53); 7.5344 (0.94); 7.5312 (1.46); 7.5279 (0.77);

7.4985 (2.55); 7.4828 (1.85); 7.4793 (3.28); 7.4654 (0.55); 7.4616 (1.30); 7.4586 (0.76); 7.3313 (1.15); 7.3257 (0.32); 7.3101 (2.59); 7.2891

(1.61); 7.2088 (1.93); 7.1907 (1.86); 7.0128 (3.47); 7.0073 (2.68); 7.0021 (1.71); 6.9968 (1.43); 6.9952 (1.47); 6.9123 (1.06); 6.9101 (1.12);

6.9068 (1.02); 6.9047 (0.96); 6.8912 (1.04); 6.8897 (1.03); 6.8854 (0.99); 5.3897 (6.43); 5.1387 (0.34); 5.1226 (1.13); 5.1062 (1.14); 5.0899

(0.34); 3.3374 (98.89); 3.0642 (16.00); 2.8910 (6.17); 2.7317 (4.95); 2.5259 (0.74); 2.5124 (14.35); 2.5080 (27.93); 2.5035 (36.37); 2.4989

(26.54); 2.4945 (12.86); 1.5377 (5.80); 1.5213 (5.72); −0.0002 (2.08)

›Example 65, Solvent: DMSO, Spectrometer: 399.95 MHz

10.6872 (2.25); 8.0182 (0.71); 7.9976 (0.92); 7.9527 (0.83); 7.8811 (1.33); 7.8619 (1.81); 7.8416 (1.11); 7.7279 (2.61); 7.7241 (1.26); 7.7152

(0.78); 7.7101 (3.42); 7.7064 (2.37); 7.5683 (0.49); 7.5564 (0.36); 7.5500 (1.64); 7.5443 (0.48); 7.5350 (0.87); 7.5317 (1.42); 7.5283 (0.71);

7.5005 (2.41); 7.4971 (1.04); 7.4849 (1.95); 7.4814 (3.29); 7.4756 (4.59); 7.4700 (1.42); 7.4637 (1.43); 7.4587 (1.65); 7.4530 (4.56); 7.4442

(0.39); 7.2039 (1.77); 7.1861 (1.68); 6.9528 (0.42); 6.9441 (4.29); 6.9385 (1.26); 6.9270 (1.22); 6.9215 (3.97); 6.9127 (0.33); 5.3821 (6.15);

4.8083 (5.61); 3.3429 (143.71); 3.3076 (0.38); 3.0661 (16.00); 2.8908 (6.80); 2.7319 (5.24); 2.7312 (5.34); 2.5258 (0.71); 2.5209 (1.16); 2.5124

(14.14); 2.5079 (28.18); 2.5033 (37.11); 2.4987 (26.84); 2.4942 (12.72); −0.0002 (0.63)

›Example 66, Solvent: DMSO, Spectrometer: 399.95 MHz

10.6366 (2.23); 8.0298 (0.83); 8.0093 (1.06); 7.8832 (1.35); 7.8638 (1.84); 7.8436 (1.15); 7.7281 (2.63); 7.7243 (1.26); 7.7154 (0.76); 7.7103

(3.43); 7.7065 (2.38); 7.5681 (0.48); 7.5562 (0.35); 7.5497 (1.65); 7.5442 (0.47); 7.5348 (0.86); 7.5315 (1.41); 7.5282 (0.72); 7.5004 (2.42);

7.4970 (1.02); 7.4849 (1.63); 7.4812 (3.10); 7.4676 (0.47); 7.4635 (1.22); 7.4603 (0.69); 7.2047 (1.81); 7.1865 (1.72); 7.1554 (1.85); 7.1495

(0.60); 7.1383 (0.81); 7.1328 (3.23); 7.1285 (0.74); 7.1224 (0.33); 7.1173 (0.71); 7.1112 (2.49); 6.9915 (2.48); 6.9854 (0.79); 6.9805 (2.52);

6.9745 (1.19); 6.9685 (1.83); 6.9635 (0.69); 6.9576 (1.78); 5.3827 (6.30); 4.7789 (6.47); 3.3427 (116.03); 3.0663 (16.00); 2.8908 (0.57); 2.7314

(0.44); 2.5259 (0.59); 2.5211 (0.94); 2.5125 (12.03); 2.5080 (24.07); 2.5035 (31.81); 2.4988 (23.05); 2.4943 (10.95); −0.0002 (0.76)

›Example 67, Solvent: DMSO, Spectrometer: 400.13 MHz

10.5993 (1.82); 9.1108 (1.66); 9.0962 (1.84); 8.6341 (0.47); 8.6147 (1.06); 8.5952 (0.64); 8.4425 (2.28); 8.1891 (1.06); 8.1707 (1.63); 8.1543

(1.14); 8.0594 (0.95); 8.0392 (1.18); 7.8476 (0.94); 7.8278 (1.38); 7.8079 (0.92); 7.7257 (2.11); 7.7078 (2.67); 7.7041 (2.13); 7.5766 (0.37);

7.5581 (1.35); 7.5399 (1.16); 7.5070 (1.93); 7.4877 (2.53); 7.4700 (1.04); 7.1633 (1.46); 7.1449 (1.45); 5.3555 (4.71); 4.6487 (0.94); 4.6306

(1.84); 4.6126 (1.04); 3.5220 (0.60); 3.4965 (1.34); 3.4471 (16.00); 3.3968 (911.69); 3.3470 (19.34); 3.2969 (2.10); 3.2676 (0.98); 3.2281 (0.66);

3.1869 (0.44); 3.1680 (0.34); 3.1020 (0.37); 3.0512 (11.93); 2.6848 (0.88); 2.6802 (1.19); 2.6756 (0.99); 2.6109 (0.34); 2.5660 (2.35); 2.5616

(3.07); 2.5571 (2.61); 2.5525 (2.00); 2.5333 (5.11); 2.5199 (65.47); 2.5156 (134.39); 2.5112 (183.81); 2.5067 (138.75); 2.5025 (71.95); 2.4707

(4.11); 2.4658 (3.82); 2.4611 (4.02); 2.4562 (3.69); 2.4530 (3.49); 2.4352 (1.51); 2.3425 (0.79); 2.3381 (1.09); 2.3336 (0.84); 1.9767 (0.71);

1.9569 (1.03); 1.9392 (0.80); 1.6144 (0.35); 1.5965 (0.84); 1.5778 (1.03); 1.5580 (0.75)

›Example 68, Solvent: DMSO, Spectrometer: 400.13 MHz

10.3171 (2.77); 7.8219 (0.76); 7.8011 (1.72); 7.7834 (1.99); 7.7697 (2.19); 7.7672 (2.40); 7.7490 (1.03); 7.7275 (2.73); 7.7097 (3.44); 7.7060

(2.42); 7.5683 (0.53); 7.5567 (0.45); 7.5500 (1.72); 7.5444 (0.53); 7.5351 (0.97); 7.5318 (1.45); 7.5007 (2.52); 7.4852 (1.82); 7.4815 (3.19);

7.4638 (1.29); 7.4451 (1.37); 7.4413 (1.84); 7.4236 (3.52); 7.3981 (2.13); 7.3932 (0.69); 7.3801 (3.38); 7.3607 (1.53); 7.3220 (0.78); 7.3184

(1.21); 7.3148 (0.66); 7.3062 (0.56); 7.3005 (1.46); 7.2953 (0.39); 7.2827 (0.50); 7.1078 (1.57); 7.1054 (1.50); 7.0903 (1.50); 7.0877 (1.42);

5.8544 (0.42); 5.8383 (1.42); 5.8218 (1.40); 5.8054 (0.40); 5.3399 (6.46); 3.3747 (0.40); 3.3249 (36.38); 3.3011 (1.86); 3.0722 (16.00); 2.6831

(0.66); 2.6786 (0.87); 2.6741 (0.64); 2.5638 (1.28); 2.5594 (1.69); 2.5547 (1.30); 2.5496 (0.86); 2.5184 (55.80); 2.5140 (109.68); 2.5095

(145.64); 2.5050 (103.32); 2.5006 (48.57); 2.4642 (1.44); 2.4597 (1.70); 2.4554 (1.26); 2.3409 (0.71); 2.3363 (0.91); 2.3319 (0.70); 1.5370

(6.04); 1.5206 (6.03)

›Example 69, Solvent: DMSO, Spectrometer: 399.95 MHz

10.7919 (2.10); 8.0189 (1.20); 7.9983 (1.56); 7.9528 (0.58); 7.8679 (1.28); 7.8488 (1.77); 7.8284 (1.12); 7.7294 (2.04); 7.7268 (2.58); 7.7231

(1.28); 7.7142 (0.80); 7.7091 (3.40); 7.7054 (2.43); 7.5685 (0.48); 7.5565 (0.36); 7.5502 (1.60); 7.5445 (0.48); 7.5351 (0.87); 7.5318 (1.41);

7.5285 (0.71); 7.4997 (2.31); 7.4963 (1.02); 7.4841 (1.67); 7.4805 (3.03); 7.4669 (0.49); 7.4628 (1.21); 7.4596 (0.73); 7.2021 (1.76); 7.1880

(1.10); 7.1831 (2.00); 7.1680 (1.52); 7.1600 (0.34); 7.1457 (1.28); 6.5295 (0.71); 6.5259 (1.12); 6.5220 (1.10); 6.5005 (4.44); 6.4956 (2.89);

6.4894 (0.91); 6.4827 (1.25); 6.4772 (0.71); 5.3853 (5.82); 5.0648 (1.00); 5.0483 (1.01); 3.6978 (16.00); 3.3541 (114.20); 3.3508 (148.75);

3.0722 (0.65); 3.0627 (15.32); 2.8911 (4.53); 2.7326 (3.78); 2.7314 (3.60); 2.5265 (0.69); 2.5217 (1.11); 2.5131 (13.04); 2.5086 (25.87); 2.5040

(33.86); 2.4994 (24.65); 2.4950 (11.81); 1.5207 (5.12); 1.5043 (5.05); −0.0002 (0.57)

›Example 70, Solvent: DMSO, Spectrometer: 400.13 MHz

10.2616 (6.41); 7.8384 (1.50); 7.8176 (3.85); 7.8000 (4.59); 7.7878 (5.39); 7.7694 (2.18); 7.7665 (2.07); 7.7568 (6.17); 7.7388 (7.21); 7.7352

(5.36); 7.5659 (1.06); 7.5538 (0.91); 7.5475 (3.51); 7.5421 (1.20); 7.5294 (3.02); 7.4987 (5.30); 7.4794 (6.77); 7.4617 (2.53); 7.1330 (3.40);

7.1179 (3.22); 5.3776 (13.62); 4.9879 (16.00); 4.1989 (4.31); 4.1823 (9.34); 4.1657 (4.39); 3.3284 (39.57); 2.9114 (2.84); 2.9049 (6.17); 2.8984

(3.00); 2.6755 (0.37); 2.5801 (2.62); 2.5735 (2.75); 2.5635 (5.52); 2.5569 (5.41); 2.5469 (3.10); 2.5403 (3.08); 2.5109 (49.01); 2.5066 (64.28);

2.5023 (46.96); 2.3333 (0.41); 2.3292 (0.32); 2.0798 (9.91)

›Example 71, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5020 (1.86); 8.0726 (1.33); 8.0519 (1.58); 7.8358 (1.32); 7.8165 (1.83); 7.7963 (1.21); 7.7264 (2.09); 7.7240 (2.64); 7.7202 (1.33); 7.7113

(0.82); 7.7062 (3.56); 7.7024 (2.42); 7.5648 (0.49); 7.5530 (0.36); 7.5465 (1.65); 7.5408 (0.50); 7.5315 (0.89); 7.5282 (1.42); 7.5249 (0.73);

7.4977 (2.44); 7.4944 (1.07); 7.4823 (1.68); 7.4786 (3.11); 7.4650 (0.48); 7.4609 (1.22); 7.4577 (0.69); 7.1399 (1.83); 7.1215 (1.78); 5.3540

(6.65); 3.3299 (59.74); 3.0539 (16.00); 2.8909 (2.02); 2.7321 (1.63); 2.5253 (0.57); 2.5120 (10.69); 2.5075 (21.11); 2.5029 (27.62); 2.4983

(20.03); 2.4939 (9.54); 2.4190 (1.06); 2.4001 (3.52); 2.3812 (3.61); 2.3624 (1.15); 1.2828 (0.35); 1.0758 (3.97); 1.0570 (8.37); 1.0381 (3.78);

0.8759 (0.59); 0.8625 (0.34); −0.0002 (5.22)

›Example 72, Solvent: DMSO, Spectrometer: 399.95 MHz

11.7791 (0.48); 7.9532 (0.41); 7.7367 (0.88); 7.7340 (1.19); 7.7300 (0.60); 7.7216 (0.39); 7.7163 (1.56); 7.7125 (1.10); 7.5449 (0.78); 7.5303

(0.43); 7.5269 (0.70); 7.5234 (0.36); 7.5014 (1.14); 7.4980 (0.51); 7.4864 (0.74); 7.4824 (1.40); 7.4649 (0.56); 7.4613 (0.33); 7.2579 (1.81);

5.2897 (2.57); 3.8663 (3.73); 3.3298 (35.01); 3.0324 (7.32); 2.8910 (3.43); 2.7322 (2.69); 2.7313 (2.64); 2.5204 (0.41); 2.5118 (5.50); 2.5073

(11.12); 2.5027 (14.79); 2.4981 (10.79); 2.4936 (5.19); 0.9301 (16.00); 0.9054 (0.41); 0.7329 (1.03); −0.0002 (5.07)

›Example 73, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5533 (1.12); 10.5076 (0.32); 8.0711 (0.88); 8.0504 (1.04); 7.9531 (0.43); 7.9406 (0.34); 7.9208 (0.49); 7.9007 (0.37); 7.8411 (0.76); 7.8217

(1.10); 7.8016 (0.70); 7.7470 (1.25); 7.7287 (2.00); 7.7252 (2.79); 7.7053 (2.50); 7.7016 (1.79); 7.5750 (0.77); 7.5690 (0.40); 7.5653 (0.45);

7.5596 (0.52); 7.5564 (0.72); 7.5533 (0.61); 7.5470 (1.25); 7.5414 (0.39); 7.5318 (0.75); 7.5287 (1.08); 7.5253 (0.64); 7.5168 (1.12); 7.4977

(3.16); 7.4789 (2.78); 7.4650 (0.42); 7.4610 (0.88); 7.4579 (0.51); 7.1491 (1.03); 7.1312 (0.99); 7.1239 (0.37); 6.9620 (0.80); 6.9433 (1.07);

5.3809 (2.55); 5.3567 (4.46); 3.5688 (1.27); 3.5524 (2.55); 3.5358 (1.37); 3.5214 (0.33); 3.3933 (30.62); 3.0690 (0.47); 3.0549 (16.00); 2.8914

(2.58); 2.7321 (2.19); 2.5635 (1.27); 2.5496 (2.64); 2.5357 (1.55); 2.5260 (1.26); 2.5123 (18.66); 2.5081 (35.20); 2.5036 (45.00); 2.4991 (32.97);

2.4949 (16.23); 2.4520 (0.45); 2.4425 (0.90); 2.4348 (0.42); 2.4240 (1.82); 2.4062 (1.01); 2.3822 (0.49); 2.2189 (0.32); 2.2010 (0.56); 2.1823

(0.33); 1.8432 (0.54); 1.8265 (0.75); 1.8060 (0.75); 1.7894 (0.38); 1.7292 (0.35); 1.7109 (0.76); 1.6927 (0.80); 1.6741 (0.49); 1.5973 (0.42);

1.4284 (0.46); 1.4082 (0.44); 1.2374 (0.33); −0.0002 (2.87)

›Example 74, Solvent: DMSO, Spectrometer: 400.13 MHz

7.7393 (2.83); 7.7213 (3.50); 7.7177 (2.51); 7.5588 (0.53); 7.5468 (0.45); 7.5405 (1.70); 7.5350 (0.56); 7.5253 (0.98); 7.5222 (1.45); 7.4896

(2.51); 7.4703 (3.27); 7.4526 (1.26); 7.4107 (1.21); 7.3925 (1.60); 7.3901 (1.55); 7.3719 (1.34); 7.2932 (0.91); 7.2749 (2.76); 7.2574 (3.45);

7.2413 (4.27); 7.2248 (1.60); 7.2087 (0.81); 7.2049 (0.96); 7.2001 (0.55); 7.1874 (1.45); 7.1810 (0.34); 7.1702 (0.48); 6.6962 (0.65); 6.6824

(1.29); 6.6685 (0.64); 6.5234 (2.00); 6.5057 (1.92); 6.4393 (1.98); 6.4185 (1.92); 5.7637 (2.15); 5.2300 (6.75); 3.4554 (0.83); 3.4394 (1.58);

3.4232 (1.48); 3.4193 (1.57); 3.4044 (0.93); 3.3765 (0.60); 3.3438 (155.57); 3.3200 (0.57); 3.0562 (16.00); 2.8373 (1.71); 2.8181 (2.42); 2.8003

(1.51); 2.5153 (15.94); 2.5113 (31.31); 2.5069 (41.19); 2.5025 (29.46)

›Example 75, Solvent: DMSO, Spectrometer: 399.95 MHz

12.3671 (0.65); 9.3200 (0.57); 7.9528 (1.31); 7.7467 (2.02); 7.7441 (2.74); 7.7400 (1.43); 7.7346 (0.98); 7.7316 (1.14); 7.7265 (3.57); 7.7227

(2.60); 7.7173 (1.04); 7.7134 (0.72); 7.5699 (0.48); 7.5665 (0.33); 7.5586 (0.40); 7.5515 (1.69); 7.5455 (0.65); 7.5419 (0.57); 7.5369 (1.03);

7.5334 (1.56); 7.5299 (0.88); 7.5238 (0.51); 7.5087 (2.57); 7.5050 (1.31); 7.4938 (1.68); 7.4897 (3.18); 7.4855 (1.48); 7.4819 (1.48); 7.4765

(0.77); 7.4722 (1.44); 7.4683 (1.26); 7.4651 (2.00); 7.4603 (0.88); 7.4465 (2.69); 7.4303 (0.88); 7.4258 (2.30); 7.4199 (0.33); 7.3952 (0.42);

7.3921 (0.59); 7.3732 (0.35); 7.3355 (4.18); 7.3157 (1.19); 7.3131 (0.78); 7.2972 (1.69); 7.2813 (0.46); 7.2787 (0.76); 7.2759 (0.53); 7.2665

(2.44); 7.2636 (3.00); 7.2584 (0.82); 7.2448 (2.40); 7.2427 (1.94); 7.1751 (0.44); 7.1561 (0.46); 7.1534 (0.60); 7.1354 (0.48); 6.9953 (0.75);

6.7583 (0.99); 6.7556 (0.91); 6.7367 (0.95); 6.6282 (0.77); 5.3233 (5.58); 5.1160 (1.48); 3.3335 (41.99); 3.3310 (55.90); 3.0577 (16.00); 3.0481

(4.23); 3.0354 (0.50); 3.0175 (0.44); 2.8901 (10.70); 2.7317 (8.74); 2.7306 (8.34); 2.5247 (0.78); 2.5199 (1.27); 2.5113 (15.49); 2.5068 (30.92);

2.5022 (40.65); 2.4976 (29.35); 2.4931 (13.84); 0.0080 (0.36); −0.0002 (10.76)

›Example 76, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5782 (2.22); 8.0435 (0.84); 8.0229 (1.07); 7.8826 (1.33); 7.8633 (1.84); 7.8431 (1.13); 7.7276 (2.63); 7.7239 (1.28); 7.7149 (0.81); 7.7099

(3.44); 7.7061 (2.40); 7.5676 (0.49); 7.5557 (0.36); 7.5493 (1.65); 7.5436 (0.48); 7.5344 (0.88); 7.5310 (1.42); 7.5277 (0.72); 7.4998 (2.42);

7.4964 (1.03); 7.4843 (1.69); 7.4806 (3.11); 7.4670 (0.49); 7.4629 (1.23); 7.4597 (0.70); 7.2035 (1.81); 7.1853 (1.77); 7.1717 (1.12); 7.1525

(1.64); 7.1320 (1.18); 7.1120 (0.71); 7.1090 (0.60); 6.8792 (0.97); 6.8608 (1.70); 6.8450 (2.09); 6.8260 (1.47); 5.3814 (6.24); 4.8169 (6.31);

3.3473 (125.30); 3.0626 (16.00); 2.8906 (0.86); 2.7322 (0.69); 2.7312 (0.68); 2.5260 (0.56); 2.5126 (11.38); 2.5081 (22.51); 2.5035 (29.43);

2.4989 (21.30); 2.4944 (10.12); 2.2248 (10.54); −0.0002 (0.43)

›Example 77, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5111 (2.02); 8.0678 (1.23); 8.0471 (1.47); 7.8297 (1.26); 7.8105 (1.73); 7.7902 (1.19); 7.7235 (2.59); 7.7197 (1.29); 7.7108 (0.83); 7.7058

(3.52); 7.7020 (2.35); 7.5641 (0.49); 7.5522 (0.37); 7.5458 (1.63); 7.5401 (0.49); 7.5308 (0.87); 7.5275 (1.41); 7.5241 (0.71); 7.4963 (2.41);

7.4928 (1.02); 7.4809 (1.69); 7.4771 (3.07); 7.4635 (0.49); 7.4594 (1.23); 7.4562 (0.68); 7.1387 (1.76); 7.1211 (1.70); 5.3535 (6.08); 3.3290

(52.17); 3.0676 (0.35); 3.0535 (16.00); 2.8908 (2.53); 2.7322 (1.96); 2.7312 (1.99); 2.5252 (0.56); 2.5204 (0.95); 2.5119 (11.27); 2.5074 (22.37);

2.5028 (29.46); 2.4982 (21.31); 2.4937 (10.07); 2.4097 (1.50); 2.3910 (2.25); 2.3714 (1.63); 1.7077 (0.95); 1.6732 (1.93); 1.6378 (1.20); 1.6145

(0.63); 1.6107 (0.63); 1.5899 (0.46); 1.4985 (0.80); 1.4809 (1.64); 1.4611 (1.74); 1.4434 (0.86); 1.2341 (0.51); 1.2233 (0.48); 1.2146 (0.45);

1.1968 (0.93); 1.1923 (0.95); 1.1863 (1.02); 1.1685 (1.50); 1.1621 (1.26); 1.1507 (0.86); 1.1400 (1.27); 1.1205 (0.60); 1.1137 (0.38); 0.9076

(0.44); 0.8938 (0.47); 0.8760 (1.38); 0.8621 (0.67); 0.8563 (0.94); 0.8498 (0.93); −0.0002 (5.59)

›Example 78, Solvent: DMSO, Spectrometer: 399.95 MHz

10.4942 (2.05); 8.0673 (1.38); 8.0466 (1.63); 7.9534 (0.69); 7.8251 (1.26); 7.8060 (1.85); 7.7856 (1.16); 7.7236 (2.98); 7.7108 (0.93); 7.7058

(3.91); 7.7021 (2.73); 7.5641 (0.55); 7.5610 (0.37); 7.5522 (0.41); 7.5458 (1.87); 7.5401 (0.57); 7.5308 (1.00); 7.5276 (1.62); 7.5243 (0.85);

7.4963 (2.80); 7.4808 (1.93); 7.4772 (3.56); 7.4635 (0.56); 7.4595 (1.39); 7.4563 (0.81); 7.1383 (1.91); 7.1198 (1.86); 5.3545 (7.06); 4.0446

(0.41); 4.0268 (0.42); 3.3291 (63.21); 3.0565 (16.00); 2.8909 (5.44); 2.7321 (4.37); 2.5252 (0.65); 2.5118 (13.63); 2.5074 (27.22); 2.5028

(36.02); 2.4982 (26.50); 2.4938 (12.92); 2.4656 (0.42); 2.4441 (0.48); 2.4299 (1.12); 2.4083 (1.54); 2.4021 (1.39); 2.3846 (1.43); 2.3664 (0.40);

2.3489 (0.50); 2.2552 (0.38); 2.2358 (0.52); 2.2202 (0.49); 2.2126 (0.37); 2.2012 (0.37); 2.1318 (1.14); 2.1213 (0.74); 2.0934 (1.22); 1.7405

(0.35); 1.7367 (0.33); 1.7184 (0.45); 1.7107 (0.59); 1.7000 (0.47); 1.5393 (0.53); 1.5318 (0.37); 1.5098 (0.52); 1.4804 (0.38); 1.4703 (0.61);

1.4617 (0.61); 1.4507 (0.55); 1.4409 (0.62); 1.4326 (0.49); 1.4228 (0.38); 1.3350 (0.96); 1.3115 (1.45); 1.2982 (0.81); 1.2832 (0.78); 1.2688

(0.42); 1.2440 (1.23); 1.2395 (1.35); 1.2213 (0.71); 1.2164 (0.71); 1.1836 (0.54); 1.1658 (1.05); 1.1552 (0.39); 1.1481 (0.89); 1.1393 (0.39);

1.1327 (0.48); 1.1279 (0.63); 1.1221 (0.62); 1.1165 (0.62); 1.1108 (0.44); 1.1052 (0.40); 1.0928 (0.35); 0.8757 (0.62); 0.8625 (0.38); 0.8570

(0.33); 0.7119 (0.48); 0.7064 (0.52); 0.6989 (0.51); 0.6930 (0.49); 0.6817 (0.47); 0.6762 (0.49); 0.6686 (0.50); 0.6632 (0.46); −0.0002 (7.35)

›Example 79, Solvent: DMSO, Spectrometer: 399.95 MHz

10.2078 (2.01); 7.9530 (0.61); 7.8012 (0.70); 7.7805 (1.26); 7.7618 (1.18); 7.7227 (1.62); 7.7201 (2.12); 7.7163 (1.14); 7.7078 (1.92); 7.7024

(2.89); 7.6987 (2.01); 7.6880 (0.87); 7.5628 (0.39); 7.5445 (1.30); 7.5388 (0.40); 7.5295 (0.70); 7.5262 (1.13); 7.5228 (0.59); 7.4948 (1.93);

7.4914 (0.85); 7.4794 (1.37); 7.4756 (2.55); 7.4687 (1.72); 7.4653 (2.07); 7.4581 (1.24); 7.4546 (0.83); 7.4472 (2.45); 7.4445 (2.34); 7.4222

(0.36); 7.4195 (0.34); 7.3465 (0.38); 7.3371 (1.38); 7.3322 (0.53); 7.3186 (2.37); 7.3025 (0.63); 7.2985 (1.45); 7.2396 (0.46); 7.2227 (0.96);

7.2199 (1.41); 7.2101 (0.50); 7.2062 (0.54); 7.2018 (1.33); 7.1865 (0.34); 7.1836 (0.50); 7.0898 (1.35); 7.0730 (1.30); 5.3272 (4.75); 4.2948

(1.05); 4.1307 (5.89); 3.3440 (106.63); 3.0502 (12.46); 2.8907 (4.85); 2.7324 (3.83); 2.7313 (3.90); 2.5259 (0.53); 2.5211 (0.86); 2.5125 (9.60);

2.5080 (19.06); 2.5034 (25.11); 2.4988 (18.33); 2.4943 (8.79); 1.3430 (16.00); −0.0002 (1.31)

›Example 80, Solvent: DMSO, Spectrometer: 399.95 MHz

12.5113 (0.77); 7.9531 (0.80); 7.7377 (2.09); 7.7352 (2.72); 7.7312 (1.30); 7.7226 (0.85); 7.7175 (3.57); 7.7137 (2.43); 7.5656 (0.50); 7.5624

(0.32); 7.5541 (0.35); 7.5473 (1.72); 7.5414 (0.51); 7.5325 (0.95); 7.5291 (1.52); 7.5257 (0.76); 7.5024 (2.53); 7.4990 (1.07); 7.4873 (1.70);

7.4834 (3.18); 7.4699 (0.50); 7.4658 (1.27); 7.4624 (0.71); 7.3294 (4.53); 7.1646 (1.08); 7.1446 (2.02); 7.1241 (1.01); 6.7642 (1.30); 6.7463

(3.02); 6.6956 (1.00); 6.6895 (0.82); 6.6756 (0.78); 6.6719 (0.87); 5.3366 (5.85); 5.0461 (0.39); 5.0297 (1.47); 5.0131 (1.48); 4.9966 (0.40);

3.3407 (71.31); 3.0279 (0.40); 3.0092 (16.00); 2.8906 (6.59); 2.7323 (5.26); 2.7314 (5.08); 2.5259 (0.50); 2.5211 (0.81); 2.5125 (9.65); 2.5080

(19.21); 2.5034 (25.24); 2.4988 (18.23); 2.4943 (8.61); 2.2409 (9.78); 1.5310 (5.59); 1.5145 (5.54); −0.0002 (2.73)

›Example 81, Solvent: DMSO, Spectrometer: 399.95 MHz

12.7334 (2.08); 7.9525 (1.68); 7.7397 (4.10); 7.7214 (5.10); 7.7179 (2.82); 7.6092 (1.18); 7.6045 (1.36); 7.5907 (1.65); 7.5860 (1.81); 7.5651

(0.49); 7.5620 (0.33); 7.5537 (0.36); 7.5467 (1.75); 7.5410 (0.52); 7.5320 (1.00); 7.5287 (1.59); 7.5251 (0.93); 7.5225 (0.87); 7.5192 (0.87);

7.5036 (4.33); 7.5007 (2.84); 7.4847 (4.20); 7.4756 (1.50); 7.4706 (1.79); 7.4669 (1.44); 7.4634 (0.85); 7.4563 (1.45); 7.4515 (1.42); 7.4373

(0.58); 7.4327 (0.51); 7.3982 (4.18); 5.3621 (6.32); 3.3383 (108.95); 3.0483 (16.00); 2.8905 (13.02); 2.7314 (10.70); 2.5250 (0.66); 2.5116

(14.14); 2.5072 (28.01); 2.5026 (36.80); 2.4981 (26.89); 2.4937 (13.03); −0.0002 (4.70)

›Example 82, Solvent: DMSO, Spectrometer: 399.95 MHz

12.5092 (1.00); 7.9529 (0.89); 7.7422 (0.32); 7.7365 (2.08); 7.7339 (2.67); 7.7299 (1.25); 7.7213 (0.83); 7.7162 (3.53); 7.7124 (2.38); 7.5655

(0.50); 7.5539 (0.35); 7.5472 (1.71); 7.5413 (0.49); 7.5324 (0.93); 7.5290 (1.52); 7.5255 (0.75); 7.5022 (2.50); 7.4988 (1.04); 7.4870 (1.67);

7.4831 (3.13); 7.4697 (0.49); 7.4656 (1.25); 7.4622 (0.77); 7.3383 (0.36); 7.3292 (4.54); 7.1636 (1.03); 7.1470 (1.10); 7.1452 (1.14); 7.1101

(0.49); 7.1069 (0.46); 7.0909 (1.05); 7.0711 (0.65); 7.0679 (0.57); 6.8576 (0.91); 6.8392 (1.54); 6.8224 (0.69); 6.8206 (0.68); 6.7567 (1.53);

6.7365 (1.38); 5.3340 (5.73); 5.0373 (0.38); 5.0208 (1.39); 5.0042 (1.40); 4.9877 (0.38); 3.3396 (95.93); 3.0194 (1.06); 3.0102 (16.00); 2.8904

(7.42); 2.7321 (5.68); 2.7311 (5.88); 2.5256 (0.51); 2.5208 (0.80); 2.5123 (10.61); 2.5077 (21.37); 2.5031 (28.27); 2.4985 (20.41); 2.4940 (9.65);

2.2170 (9.94); 1.5659 (5.54); 1.5494 (5.60); 1.5299 (0.37); −0.0002 (3.61)

›Example 83, Solvent: DMSO, Spectrometer: 400.13 MHz

8.0123 (2.60); 7.6632 (3.98); 7.6419 (5.53); 7.6155 (0.94); 7.5975 (1.97); 7.5808 (1.80); 7.5641 (0.72); 7.4461 (3.86); 7.4264 (2.24); 6.5748

(2.81); 6.5571 (2.64); 6.4532 (2.79); 6.4325 (2.61); 6.0832 (6.83); 5.2576 (9.84); 3.4172 (4.30); 3.1433 (16.00); 2.9496 (10.68); 2.7900 (10.04);

2.7305 (0.36); 2.5619 (55.79); 2.3883 (0.36); 1.4182 (0.70); −0.0002 (1.16)

›Example 84, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5205 (1.96); 8.0698 (1.18); 8.0491 (1.40); 7.8298 (1.23); 7.8106 (1.67); 7.7903 (1.16); 7.7320 (0.32); 7.7265 (1.94); 7.7237 (2.55); 7.7198

(1.30); 7.7111 (0.83); 7.7060 (3.53); 7.7022 (2.37); 7.5641 (0.48); 7.5522 (0.36); 7.5458 (1.59); 7.5401 (0.50); 7.5309 (0.86); 7.5275 (1.41);

7.5241 (0.73); 7.4964 (2.39); 7.4930 (1.04); 7.4811 (1.64); 7.4773 (3.02); 7.4637 (0.50); 7.4596 (1.23); 7.4564 (0.69); 7.1387 (1.71); 7.1215

(1.64); 7.1201 (1.60); 5.3539 (5.96); 3.3295 (63.55); 3.0540 (16.00); 2.8911 (1.73); 2.7326 (1.37); 2.7313 (1.38); 2.5254 (0.58); 2.5206 (1.00);

2.5121 (11.09); 2.5076 (21.82); 2.5030 (28.61); 2.4984 (20.72); 2.4938 (9.82); 2.4106 (1.56); 2.3920 (2.27); 2.3727 (1.71); 1.7602 (0.38);

1.7429 (1.06); 1.7268 (1.48); 1.7123 (0.94); 1.6995 (0.67); 1.6087 (0.84); 1.5897 (1.60); 1.5716 (1.96); 1.5552 (1.24); 1.5403 (0.52); 1.5373

(0.49); 1.5268 (0.32); 1.5126 (0.39); 1.5082 (0.35); 1.4948 (0.49); 1.4855 (0.79); 1.4752 (0.81); 1.4693 (0.89); 1.4563 (0.79); 1.1065 (0.55);

1.0957 (0.72); 1.0904 (0.83); 1.0802 (0.69); 1.0756 (0.62); 1.0715 (0.62); 1.0645 (0.46); 1.0601 (0.44); 0.8759 (0.52); −0.0002 (5.65)

›Example 85, Solvent: DMSO, Spectrometer: 399.95 MHz

10.0121 (2.29); 8.0825 (1.39); 8.0623 (1.78); 7.9530 (0.86); 7.9149 (1.28); 7.8955 (1.81); 7.8754 (1.10); 7.7325 (1.98); 7.7299 (2.61); 7.7260

(1.30); 7.7173 (0.84); 7.7121 (3.46); 7.7084 (2.42); 7.5666 (0.49); 7.5548 (0.37); 7.5483 (1.62); 7.5426 (0.50); 7.5334 (0.90); 7.5301 (1.44);

7.5267 (0.74); 7.4995 (2.40); 7.4961 (1.07); 7.4841 (1.68); 7.4804 (3.07); 7.4668 (0.51); 7.4627 (1.24); 7.4595 (0.71); 7.2181 (2.13); 7.2133

(1.27); 7.2066 (5.37); 7.1988 (5.01); 7.1838 (0.85); 7.1134 (0.82); 7.1057 (1.05); 7.0976 (0.61); 5.3889 (6.09); 4.9691 (0.85); 4.9313 (2.12);

4.8885 (1.60); 4.8510 (0.61); 4.4782 (0.93); 4.4658 (0.97); 4.4538 (1.23); 4.4414 (0.98); 3.3302 (71.52); 3.0854 (16.00); 3.0122 (1.27); 3.0018

(1.83); 2.9796 (0.89); 2.8902 (6.85); 2.7318 (5.35); 2.7306 (5.48); 2.5247 (0.62); 2.5114 (12.73); 2.5069 (24.95); 2.5023 (32.61); 2.4977 (23.73);

2.4931 (11.41); −0.0002 (7.97)

›Example 86, Solvent: DMSO, Spectrometer: 400.13 MHz

10.2690 (7.09); 7.8414 (1.60); 7.8205 (4.46); 7.8032 (6.02); 7.7948 (6.83); 7.7768 (2.26); 7.6902 (7.09); 7.6722 (8.47); 7.6689 (6.85); 7.5582

(1.32); 7.5397 (4.13); 7.5218 (3.81); 7.4939 (6.61); 7.4746 (8.02); 7.4570 (3.23); 7.1412 (3.95); 7.1262 (3.78); 5.7626 (3.63); 5.3377 (16.00);

4.5315 (10.49); 4.5254 (10.88); 4.1988 (4.94); 4.1822 (10.57); 4.1655 (5.47); 4.1490 (0.77); 4.1330 (0.45); 4.0599 (0.34); 4.0422 (0.91); 4.0245

(0.91); 4.0068 (0.35); 3.3316 (33.70); 3.3251 (9.43); 3.3189 (4.52); 3.3080 (2.35); 2.9128 (3.20); 2.9063 (6.74); 2.8998 (3.70); 2.5808 (3.27);

2.5743 (3.63); 2.5643 (6.78); 2.5577 (6.87); 2.5476 (4.16); 2.5412 (3.91); 2.5106 (37.18); 2.5066 (48.53); 2.5026 (37.67); 2.3334 (0.40); 2.0789

(0.68); 1.9937 (3.66); 1.2820 (0.55); 1.2484 (2.52); 1.1966 (1.09); 1.1788 (1.97); 1.1610 (1.03); 0.8782 (1.00); 0.8620 (2.64); 0.8443 (1.22)

›Example 87, Solvent: DMSO, Spectrometer: 300.16 MHz

7.9539 (0.50); 7.5448 (0.60); 7.4309 (0.48); 7.4056 (0.47); 7.3921 (0.55); 7.3742 (0.93); 7.3647 (0.87); 5.4238 (1.47); 3.3516 (3.48); 3.0694

(2.92); 2.5216 (16.27); 2.3428 (2.48); 1.3706 (16.00)

›Example 88, Solvent: DMSO, Spectrometer: 400.13 MHz

10.7366 (1.91); 8.0323 (1.09); 8.0117 (1.32); 7.8379 (1.13); 7.8187 (1.56); 7.7984 (0.97); 7.7256 (2.28); 7.7127 (0.82); 7.7078 (2.91); 7.7040

(2.01); 7.5763 (0.43); 7.5645 (0.38); 7.5580 (1.42); 7.5524 (0.46); 7.5431 (0.83); 7.5399 (1.24); 7.5365 (0.65); 7.5103 (2.11); 7.4948 (1.51);

7.4911 (2.61); 7.4775 (0.45); 7.4735 (1.03); 7.4703 (0.58); 7.2722 (2.79); 7.2506 (3.04); 7.2434 (0.33); 7.1816 (0.54); 7.1599 (0.69); 7.1503

(1.63); 7.1319 (1.52); 6.8979 (0.52); 6.8908 (3.59); 6.8850 (1.46); 6.8740 (1.17); 6.8690 (3.18); 6.8620 (0.83); 5.3765 (5.28); 3.7503 (0.42);

3.7340 (3.41); 3.7251 (16.00); 3.6786 (0.33); 3.6353 (4.80); 3.4953 (0.76); 3.4848 (1.42); 3.4773 (2.39); 3.4591 (2.36); 3.4409 (0.74); 3.3414

(19.01); 2.6785 (0.33); 2.5640 (0.56); 2.5595 (0.75); 2.5551 (0.58); 2.5318 (1.59); 2.5183 (20.91); 2.5140 (41.52); 2.5095 (55.24); 2.5051

(39.23); 2.5007 (18.19); 2.4641 (0.47); 2.4597 (0.60); 2.4554 (0.44); 2.3364 (0.33); 1.9968 (0.89); 1.2524 (0.59); 1.1813 (0.48); 1.0367 (2.67);

1.0186 (5.93); 1.0004 (2.55); 0.8649 (0.80); 0.8473 (0.32)

›Example 89, Solvent: DMSO, Spectrometer: 399.95 MHz

10.2546 (2.49); 8.1091 (0.37); 7.9531 (1.07); 7.8233 (0.70); 7.8024 (1.78); 7.7852 (2.22); 7.7778 (2.06); 7.7747 (2.28); 7.7570 (0.76); 7.7538

(0.54); 7.7225 (2.91); 7.7046 (3.72); 7.7009 (2.61); 7.6824 (0.43); 7.6644 (0.50); 7.6610 (0.39); 7.5692 (0.33); 7.5667 (0.35); 7.5633 (0.53);

7.5603 (0.37); 7.5514 (0.45); 7.5451 (1.74); 7.5395 (0.75); 7.5302 (1.15); 7.5268 (1.59); 7.5234 (0.89); 7.4961 (2.82); 7.4807 (1.96); 7.4770

(3.62); 7.4632 (0.87); 7.4593 (1.49); 7.4562 (0.94); 7.4517 (0.47); 7.4450 (0.50); 7.4401 (0.61); 7.4284 (0.62); 7.4243 (0.52); 7.3657 (1.64);

7.3607 (0.72); 7.3516 (1.85); 7.3441 (2.09); 7.3380 (0.87); 7.3357 (0.89); 7.3301 (1.87); 7.3219 (0.33); 7.3171 (0.61); 7.2944 (0.33); 7.2244

(1.73); 7.2224 (1.71); 7.2072 (3.30); 7.1431 (2.14); 7.1378 (0.69); 7.1266 (0.83); 7.1207 (3.52); 7.1149 (0.82); 7.1044 (1.90); 7.1019 (2.00);

7.0987 (2.07); 7.0881 (1.49); 7.0848 (1.40); 6.9748 (0.38); 6.0034 (0.44); 5.5348 (0.89); 5.3320 (6.39); 5.1790 (1.02); 4.2843 (1.67); 4.2674

(3.78); 4.2505 (1.72); 3.6701 (0.33); 3.3415 (169.96); 3.0881 (2.44); 3.0723 (0.52); 3.0617 (16.00); 3.0364 (2.41); 2.9409 (1.41); 2.9240 (2.85);

2.9071 (1.38); 2.8909 (8.40); 2.7322 (6.73); 2.7317 (6.68); 2.5258 (1.02); 2.5124 (18.10); 2.5080 (35.40); 2.5034 (46.36); 2.4988 (33.81);

2.4944 (16.26); −0.0002 (2.58)

›Example 90, Solvent: DMSO, Spectrometer: 400.13 MHz

7.6966 (2.41); 7.6942 (4.34); 7.6916 (2.60); 7.6774 (3.33); 7.6761 (3.88); 7.6741 (3.72); 7.6224 (0.97); 7.6127 (8.36); 7.6101 (8.68); 7.6038

(6.46); 7.6025 (6.04); 7.5997 (5.69); 7.5960 (4.19); 7.5795 (0.81); 7.5759 (0.77); 7.5413 (0.58); 7.5300 (2.94); 7.5213 (2.60); 7.5168 (2.10);

7.5108 (2.69); 7.5082 (2.22); 7.5032 (2.14); 7.4968 (1.80); 7.4891 (1.58); 7.0336 (8.70); 6.6786 (8.90); 5.1662 (16.00); 4.0604 (0.42); 4.0426

(1.32); 4.0248 (1.35); 4.0070 (0.45); 3.4210 (0.35); 3.4000 (3.06); 3.3501 (236.52); 3.3278 (0.65); 3.3185 (0.35); 3.3154 (0.41); 3.3003 (2.76);

3.2516 (40.94); 3.2018 (0.44); 2.5626 (0.41); 2.5580 (0.56); 2.5535 (0.41); 2.5307 (0.71); 2.5172 (16.79); 2.5128 (34.61); 2.5082 (46.67);

2.5037 (32.85); 2.4993 (15.06); 2.4629 (0.40); 2.4584 (0.51); 2.4538 (0.37); 1.9946 (5.99); 1.2471 (0.47); 1.1970 (1.65); 1.1792 (3.31); 1.1614

(1.60); 0.8625 (0.70)

›Example 91, Solvent: DMSO, Spectrometer: 399.95 MHz

11.9263 (2.25); 7.9528 (0.84); 7.7470 (1.98); 7.7442 (2.67); 7.7402 (1.31); 7.7318 (0.82); 7.7266 (3.45); 7.7228 (2.38); 7.6999 (1.37); 7.6955

(1.49); 7.6808 (1.52); 7.6764 (1.52); 7.5858 (0.78); 7.5813 (0.74); 7.5669 (1.36); 7.5647 (1.39); 7.5631 (1.41); 7.5604 (1.04); 7.5551 (0.42);

7.5472 (2.01); 7.5419 (1.33); 7.5334 (0.95); 7.5300 (1.53); 7.5264 (0.77); 7.5053 (2.50); 7.5019 (1.09); 7.4904 (1.59); 7.4864 (3.01); 7.4730

(0.50); 7.4689 (1.21); 7.4653 (0.70); 7.3504 (3.93); 7.2191 (1.82); 7.1988 (1.59); 7.1073 (1.02); 7.1053 (1.01); 7.0885 (1.78); 7.0866 (1.75);

7.0699 (0.91); 7.0678 (0.86); 5.3579 (5.97); 3.9100 (14.72); 3.3360 (72.19); 3.0555 (16.00); 2.8905 (6.69); 2.7320 (5.33); 2.7309 (5.35); 2.5251

(0.65); 2.5118 (11.62); 2.5073 (22.88); 2.5027 (29.89); 2.4981 (21.65); 2.4936 (10.27); −0.0002 (9.23)

›Example 92, Solvent: DMSO, Spectrometer: 400.13 MHz

10.3314 (3.16); 7.8494 (0.63); 7.8284 (1.98); 7.8112 (3.98); 7.8062 (2.83); 7.7892 (0.73); 7.7853 (0.41); 7.6247 (0.70); 7.6206 (1.05); 7.6150

(0.98); 7.6063 (1.23); 7.6030 (0.98); 7.5999 (1.03); 7.5953 (1.27); 7.5893 (2.51); 7.5869 (2.39); 7.5637 (0.78); 7.5496 (0.87); 7.5435 (1.19);

7.5292 (1.23); 7.5240 (0.64); 7.5086 (0.55); 7.4328 (0.54); 7.4301 (0.60); 7.4266 (0.54); 7.4238 (0.52); 7.4090 (0.99); 7.4052 (0.87); 7.3905

(0.44); 7.3880 (0.46); 7.3847 (0.42); 7.3820 (0.37); 7.1326 (1.47); 7.1288 (1.52); 7.1160 (1.40); 7.1122 (1.42); 5.7683 (0.62); 5.3615 (6.85);

4.1962 (2.13); 4.1796 (4.68); 4.1629 (2.17); 4.0438 (0.65); 4.0260 (0.66); 3.3444 (20.58); 3.0699 (16.00); 2.9229 (1.35); 2.9163 (3.03); 2.9097

(1.45); 2.5802 (1.26); 2.5736 (1.32); 2.5636 (2.87); 2.5569 (2.77); 2.5469 (1.34); 2.5403 (1.23); 2.5324 (0.51); 2.5186 (9.20); 2.5144 (18.80);

2.5100 (25.43); 2.5056 (18.47); 2.5015 (8.79); 1.9966 (2.83); 1.2490 (0.63); 1.1986 (0.76); 1.1808 (1.48); 1.1630 (0.73); 0.8634 (0.82); 0.8457

(0.34)

›Example 93, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5108 (2.23); 10.0297 (1.39); 8.0760 (1.54); 8.0726 (1.57); 8.0555 (1.80); 8.0520 (1.84); 7.8852 (0.85); 7.8659 (1.30); 7.8457 (0.79); 7.8327

(1.32); 7.8133 (1.96); 7.7931 (1.20); 7.7256 (4.21); 7.7061 (4.91); 7.5645 (0.80); 7.5525 (0.63); 7.5462 (2.74); 7.5407 (0.82); 7.5309 (1.63);

7.5279 (2.33); 7.4966 (4.18); 7.4774 (5.31); 7.4597 (2.05); 7.4569 (1.23); 7.1990 (1.27); 7.1804 (1.23); 7.1416 (1.99); 7.1231 (1.92); 5.8216

(0.60); 5.8128 (0.33); 5.8049 (0.32); 5.7959 (0.91); 5.7789 (0.95); 5.7699 (0.37); 5.7621 (0.36); 5.7532 (0.70); 5.7366 (0.34); 5.3750 (4.48);

5.3540 (6.90); 5.0233 (0.51); 5.0195 (1.08); 5.0144 (1.14); 5.0105 (0.53); 4.9804 (0.45); 4.9766 (0.98); 4.9715 (1.03); 4.9677 (0.47); 4.9429

(1.15); 4.9402 (1.08); 4.9375 (1.00); 4.9175 (1.09); 4.9148 (1.01); 4.9121 (0.92); 4.1059 (1.06); 4.0893 (1.08); 3.4632 (0.38); 3.4566 (0.62);

3.4405 (1.75); 3.4246 (1.73); 3.4086 (0.64); 3.4019 (0.38); 3.3284 (64.05); 3.0753 (10.22); 3.0534 (16.00); 2.5253 (0.98); 2.5074 (35.87);

2.5029 (46.20); 2.4984 (34.05); 2.4942 (16.81); 2.3945 (1.65); 2.3761 (3.21); 2.3576 (1.79); 2.3297 (0.32); 2.0393 (0.63); 2.0222 (1.78); 2.0045

(1.81); 1.9867 (0.75); 1.6131 (0.41); 1.5945 (1.23); 1.5762 (1.75); 1.5577 (1.35); 1.5335 (0.84); 1.5166 (1.10); 1.5129 (1.05); 1.4956 (1.16);

1.4793 (0.48); 1.3849 (0.99); 1.3664 (2.14); 1.3477 (2.36); 1.3283 (1.70); 1.3168 (0.85); 1.3087 (1.55); 1.3014 (5.27); 1.2847 (5.18); 1.2697

(0.68); 1.2604 (0.72); 1.2347 (0.38); 0.8946 (2.74); 0.8763 (5.43); 0.8578 (2.34); 0.0078 (0.42); −0.0002 (11.40); −0.0085 (0.43)

›Example 94, Solvent: DMSO, Spectrometer: 399.95 MHz

9.7653 (1.93); 8.0534 (1.29); 8.0329 (1.62); 7.8853 (1.31); 7.8659 (1.82); 7.8458 (1.13); 7.7271 (1.94); 7.7246 (2.52); 7.7207 (1.20); 7.7119

(0.79); 7.7068 (3.39); 7.7031 (2.32); 7.5641 (0.48); 7.5522 (0.35); 7.5458 (1.61); 7.5401 (0.46); 7.5308 (0.87); 7.5275 (1.39); 7.5241 (0.69);

7.4959 (2.35); 7.4925 (0.98); 7.4805 (1.64); 7.4767 (3.03); 7.4631 (0.48); 7.4591 (1.22); 7.4559 (0.66); 7.1944 (1.76); 7.1768 (1.65); 5.3740

(6.25); 4.0556 (8.70); 4.0391 (0.58); 4.0319 (0.73); 4.0266 (0.75); 4.0184 (0.75); 4.0140 (0.39); 3.3331 (71.93); 3.0795 (16.00); 3.0692 (0.50);

2.8909 (1.03); 2.7322 (0.81); 2.7313 (0.79); 2.5254 (0.57); 2.5206 (0.88); 2.5120 (11.07); 2.5075 (22.26); 2.5029 (29.43); 2.4983 (21.27);

2.4938 (10.06); 1.7085 (0.41); 1.7041 (0.47); 1.6908 (0.93); 1.6879 (0.97); 1.6729 (2.08); 1.6681 (2.39); 1.6626 (2.83); 1.6573 (2.42); 1.6548

(2.60); 1.6476 (1.03); 1.6424 (1.58); 1.6392 (1.47); 1.6234 (0.49); 1.6189 (0.46); 1.6146 (0.51); 1.5263 (0.33); 1.5183 (0.46); 1.5141 (0.64);

1.5071 (0.69); 1.5025 (0.98); 1.4995 (0.95); 1.4963 (1.01); 1.4922 (0.82); 1.4862 (0.71); 1.4767 (0.39); −0.0002 (2.96)

›Example 95, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5088 (2.07); 8.0749 (1.25); 8.0542 (1.48); 7.8323 (1.25); 7.8130 (1.74); 7.7928 (1.14); 7.7239 (2.57); 7.7201 (1.24); 7.7112 (0.85); 7.7061

(3.36); 7.7023 (2.31); 7.5642 (0.48); 7.5522 (0.37); 7.5458 (1.62); 7.5402 (0.47); 7.5309 (0.88); 7.5276 (1.39); 7.5243 (0.71); 7.4965 (2.37);

7.4811 (1.66); 7.4773 (3.03); 7.4637 (0.48); 7.4597 (1.19); 7.4565 (0.67); 7.1409 (1.78); 7.1231 (1.70); 5.3541 (6.16); 3.3284 (55.96); 3.0536

(15.38); 2.8909 (1.12); 2.7321 (0.88); 2.5252 (0.53); 2.5119 (10.97); 2.5074 (21.54); 2.5028 (28.23); 2.4982 (20.56); 2.4937 (9.88); 2.3775

(1.53); 2.3590 (3.07); 2.3404 (1.72); 1.6080 (0.40); 1.5890 (1.07); 1.5805 (0.58); 1.5758 (0.80); 1.5697 (1.41); 1.5627 (1.07); 1.5483 (1.36);

1.5302 (1.36); 1.5133 (0.85); 1.4966 (0.45); 1.1911 (1.03); 1.1740 (1.43); 1.1651 (0.81); 1.1615 (0.76); 1.1516 (1.48); 1.1344 (0.79); 0.8644

(16.00); 0.8478 (15.28); −0.0002 (7.59)

›Example 96, Solvent: DMSO, Spectrometer: 400.13 MHz

7.6611 (6.58); 7.6574 (3.58); 7.6487 (2.26); 7.6436 (8.50); 7.6397 (6.42); 7.5529 (0.65); 7.5497 (1.18); 7.5465 (0.85); 7.5386 (0.99); 7.5314

(4.08); 7.5255 (1.43); 7.5169 (2.49); 7.5134 (3.82); 7.5100 (2.13); 7.4900 (8.69); 7.4701 (11.84); 7.4567 (1.82); 7.4520 (5.86); 6.5825 (4.46);

6.5648 (4.35); 6.4667 (4.64); 6.4462 (4.56); 6.4157 (0.33); 6.3951 (0.36); 6.3121 (0.68); 6.2256 (0.38); 5.7692 (0.38); 5.6971 (0.37); 5.6829

(0.39); 5.6382 (0.40); 5.6223 (0.40); 5.6026 (0.40); 5.2839 (0.36); 5.2331 (16.00); 5.1823 (0.33); 2.5661 (0.42); 2.5616 (0.63); 2.5571 (0.53);

2.5329 (0.85); 2.5193 (16.27); 2.5150 (34.12); 2.5105 (47.07); 2.5061 (35.41); 2.5019 (18.34); 2.4691 (0.91); 2.4642 (0.97); 2.4597 (1.00);

2.4553 (0.80)

›Example 97, Solvent: DMSO, Spectrometer: 300.16 MHz

9.8567 (1.13); 7.7858 (0.94); 7.7766 (1.05); 7.7674 (2.28); 7.7308 (0.34); 7.7111 (0.55); 7.7051 (0.65); 7.6844 (0.35); 7.6792 (0.36); 7.6382

(0.36); 7.6187 (0.34); 7.6103 (0.41); 7.4006 (0.41); 7.3713 (0.80); 7.3655 (0.59); 7.3479 (0.81); 7.3454 (0.75); 7.3377 (0.45); 7.3230 (0.42);

7.3195 (0.34); 7.0981 (0.54); 7.0887 (0.56); 7.0799 (0.48); 7.0706 (0.54); 5.3503 (2.73); 3.3348 (10.70); 3.3146 (0.49); 3.1887 (6.24); 2.5158

(0.74); 2.5099 (1.54); 2.5039 (2.08); 2.4978 (1.52); 2.4920 (0.74); 1.9905 (1.26); 1.4664 (16.00); 1.1988 (0.34); 1.1751 (0.68); 1.1514

(0.33); −0.0002 (0.54)

›Example 98, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5038 (2.10); 8.0709 (1.23); 8.0503 (1.45); 7.8312 (1.27); 7.8120 (1.74); 7.7917 (1.18); 7.7261 (2.01); 7.7234 (2.66); 7.7196 (1.34); 7.7108

(0.89); 7.7057 (3.61); 7.7020 (2.40); 7.5639 (0.50); 7.5607 (0.33); 7.5520 (0.39); 7.5456 (1.63); 7.5399 (0.52); 7.5307 (0.91); 7.5273 (1.45);

7.5239 (0.75); 7.4961 (2.47); 7.4927 (1.08); 7.4807 (1.74); 7.4770 (3.12); 7.4634 (0.53); 7.4593 (1.25); 7.4561 (0.71); 7.1393 (1.77); 7.1219

(1.68); 5.3532 (6.11); 3.3286 (57.15); 3.0536 (16.00); 2.5253 (0.63); 2.5120 (11.46); 2.5075 (22.17); 2.5029 (28.83); 2.4983 (20.85); 2.4938

(9.87); 2.3890 (1.45); 2.3706 (2.77); 2.3521 (1.59); 1.5794 (0.74); 1.5621 (1.09); 1.5449 (0.76); 1.2650 (4.90); 1.2575 (5.11); 1.2428 (4.42);

0.8756 (0.62); 0.8637 (1.94); 0.8472 (5.84); 0.8296 (2.02); −0.0002 (6.05)

›Example 99, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5108 (1.12); 10.0299 (2.22); 8.0771 (1.86); 8.0568 (2.26); 7.8852 (1.36); 7.8659 (2.03); 7.8457 (1.21); 7.8326 (0.68); 7.8133 (0.98); 7.7931

(0.61); 7.7259 (3.97); 7.7077 (4.53); 7.5647 (0.75); 7.5617 (0.49); 7.5526 (0.59); 7.5464 (2.53); 7.5409 (0.76); 7.5311 (1.47); 7.5281 (2.12);

7.5250 (1.11); 7.4966 (3.81); 7.4773 (4.87); 7.4634 (0.84); 7.4596 (1.86); 7.4566 (1.09); 7.1990 (1.99); 7.1805 (1.92); 7.1416 (1.01); 7.1230

(0.96); 5.7960 (0.46); 5.7790 (0.48); 5.7532 (0.35); 5.3750 (6.93); 5.3540 (3.50); 5.0195 (0.55); 5.0144 (0.57); 4.9767 (0.49); 4.9714 (0.51);

4.9429 (0.57); 4.9402 (0.53); 4.9376 (0.48); 4.9175 (0.55); 4.9148 (0.50); 4.9120 (0.45); 4.1225 (0.47); 4.1059 (1.68); 4.0893 (1.70); 4.0727

(0.47); 3.4633 (0.61); 3.4566 (0.98); 3.4405 (2.76); 3.4247 (2.72); 3.4087 (1.00); 3.4019 (0.63); 3.3280 (60.97); 3.0752 (16.00); 3.0533 (8.12);

2.5117 (17.95); 2.5074 (33.96); 2.5029 (43.62); 2.4984 (31.88); 2.4941 (15.63); 2.3945 (0.83); 2.3761 (1.61); 2.3576 (0.90); 2.0223 (0.88);

2.0045 (0.88); 1.9868 (0.37); 1.5946 (0.62); 1.5761 (0.87); 1.5578 (0.68); 1.5512 (0.53); 1.5476 (0.45); 1.5331 (1.19); 1.5167 (1.69); 1.5130

(1.60); 1.4957 (1.79); 1.4793 (0.75); 1.3845 (0.73); 1.3661 (1.90); 1.3472 (2.48); 1.3281 (2.14); 1.3094 (1.74); 1.3014 (7.15); 1.2848 (7.02);

1.2602 (0.41); 1.2347 (0.37); 0.8947 (4.30); 0.8854 (0.52); 0.8764 (8.53); 0.8579 (3.66); 0.0079 (0.44); −0.0002 (11.06); −0.0085 (0.42)

›Example 100, Solvent: DMSO, Spectrometer: 399.95 MHz

12.4363 (1.13); 7.9530 (1.03); 7.7422 (2.09); 7.7397 (2.67); 7.7358 (1.27); 7.7272 (0.79); 7.7220 (3.47); 7.7182 (2.41); 7.5667 (0.47); 7.5553

(0.34); 7.5484 (1.69); 7.5425 (0.50); 7.5337 (0.94); 7.5303 (1.52); 7.5268 (0.74); 7.5048 (2.52); 7.5014 (1.07); 7.4897 (1.64); 7.4858 (3.14);

7.4723 (0.49); 7.4682 (1.23); 7.4647 (0.67); 7.3591 (0.68); 7.3419 (5.34); 7.3206 (1.46); 7.3179 (0.94); 7.3000 (0.72); 6.8902 (0.60); 6.8842

(1.30); 6.8782 (0.83); 6.8620 (0.56); 6.8561 (1.28); 6.8503 (0.87); 6.8344 (1.42); 6.8287 (1.55); 6.8230 (0.64); 6.8136 (1.21); 6.8077 (1.97);

6.8019 (0.97); 6.7866 (0.57); 6.7806 (0.47); 5.3455 (6.00); 4.8795 (7.70); 3.3316 (60.64); 3.0226 (16.00); 2.8905 (8.25); 2.7318 (6.79); 2.5249

(0.61); 2.5199 (1.00); 2.5115 (12.85); 2.5071 (25.50); 2.5025 (33.42); 2.4979 (24.14); 2.4934 (11.42); −0.0002 (3.58)

›Example 101, Solvent: DMSO, Spectrometer: 300.16 MHz

10.7469 (2.01); 8.0501 (1.22); 8.0225 (1.59); 7.8555 (1.13); 7.8297 (1.58); 7.8028 (0.98); 7.4420 (0.86); 7.4156 (2.00); 7.3889 (1.62); 7.2982

(1.74); 7.2878 (2.96); 7.2721 (1.43); 7.2673 (1.58); 7.2585 (4.15); 7.2491 (2.27); 7.2438 (1.36); 7.1721 (1.72); 7.1601 (1.18); 7.1493 (1.96);

7.1348 (0.90); 7.1268 (0.84); 6.9187 (0.43); 6.9090 (3.60); 6.9024 (1.25); 6.8868 (1.07); 6.8802 (3.15); 5.7792 (10.93); 5.3829 (5.06); 3.8221

(0.32); 3.8006 (14.08); 3.7764 (0.65); 3.7715 (0.47); 3.7393 (16.00); 3.6481 (5.03); 3.3457 (19.77); 3.0509 (12.47); 2.5332 (4.56); 2.5275 (9.68);

2.5215 (13.43); 2.5155 (9.90); 2.5097 (4.84); 2.0090 (0.55); 1.3760 (1.22); 1.2529 (0.35); 1.1941 (0.33)

›Example 102, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5242 (2.13); 8.0679 (1.37); 8.0472 (1.63); 7.8307 (1.34); 7.8114 (1.94); 7.7912 (1.22); 7.7241 (2.75); 7.7111 (0.90); 7.7062 (3.50); 7.7025

(2.47); 7.5645 (0.49); 7.5614 (0.32); 7.5526 (0.38); 7.5462 (1.71); 7.5406 (0.51); 7.5312 (0.95); 7.5280 (1.45); 7.5247 (0.76); 7.4971 (2.53);

7.4815 (1.78); 7.4779 (3.24); 7.4642 (0.51); 7.4602 (1.26); 7.4571 (0.76); 7.1399 (1.95); 7.1217 (1.87); 5.3548 (6.82); 3.3292 (42.97); 3.0730

(0.32); 3.0546 (16.00); 2.8909 (1.93); 2.7319 (1.57); 2.5252 (0.57); 2.5118 (11.07); 2.5074 (21.63); 2.5029 (28.29); 2.4983 (20.72); 2.4939

(10.11); 2.4089 (1.88); 2.3900 (2.51); 2.3714 (1.87); 1.5491 (0.55); 1.5323 (0.76); 1.5164 (0.78); 1.4985 (1.41); 1.4795 (2.01); 1.4614 (1.88);

1.4455 (0.59); 0.8855 (15.29); 0.8696 (14.75); −0.0002 (6.94)

›Example 103, Solvent: DMSO, Spectrometer: 399.95 MHz

11.6620 (1.02); 7.9532 (1.10); 7.7277 (2.89); 7.7100 (3.52); 7.7063 (2.55); 7.5612 (0.50); 7.5582 (0.33); 7.5497 (0.38); 7.5430 (1.74); 7.5371

(0.53); 7.5280 (1.04); 7.5248 (1.55); 7.5216 (0.82); 7.4989 (2.68); 7.4798 (3.33); 7.4622 (1.26); 7.4588 (0.79); 7.2416 (4.49); 5.2743 (6.55);

5.1458 (0.56); 5.1370 (0.72); 5.1313 (1.01); 5.1252 (0.71); 5.1167 (0.57); 3.3296 (47.71); 3.0365 (16.00); 2.8909 (7.86); 2.7321 (6.63); 2.5113

(13.57); 2.5071 (25.86); 2.5026 (33.34); 2.4981 (24.40); 2.4939 (11.91); 1.8996 (0.48); 1.8832 (1.00); 1.8717 (1.05); 1.8505 (0.60); 1.8449

(0.54); 1.7182 (0.46); 1.7032 (1.18); 1.6959 (1.56); 1.6925 (1.61); 1.6833 (2.22); 1.6735 (2.37); 1.6562 (1.08); 1.6320 (0.42); 1.6069 (0.36);

1.5959 (0.69); 1.5853 (0.68); 1.5704 (1.26); 1.5457 (0.35); 0.0080 (0.35); −0.0002 (9.28)

›Example 104, Solvent: DMSO, Spectrometer: 400.13 MHz

10.2939 (6.31); 7.8558 (0.51); 7.8440 (1.72); 7.8357 (0.89); 7.8230 (4.05); 7.8168 (0.98); 7.8054 (4.73); 7.7926 (4.97); 7.7902 (5.55); 7.7720

(2.13); 7.7215 (6.33); 7.7090 (2.34); 7.7038 (7.73); 7.7000 (5.45); 7.6175 (0.64); 7.5968 (0.54); 7.5713 (1.20); 7.5596 (1.05); 7.5530 (4.07);

7.5472 (1.42); 7.5380 (2.43); 7.5349 (3.51); 7.5073 (6.06); 7.4915 (4.68); 7.4882 (7.26); 7.4705 (2.77); 7.4674 (1.61); 7.2332 (0.54); 7.2143

(0.52); 7.1100 (3.45); 7.1076 (3.49); 7.0925 (3.45); 7.0899 (3.28); 5.7602 (11.54); 5.4179 (1.98); 5.3443 (14.61); 5.2751 (0.43); 4.2022 (0.88);

4.1917 (4.86); 4.1865 (2.38); 4.1750 (10.43); 4.1584 (4.82); 3.9159 (0.66); 3.8980 (0.66); 3.5263 (1.92); 3.5082 (6.28); 3.4900 (6.44); 3.4775

(1.40); 3.4719 (2.08); 3.4596 (0.99); 3.4413 (0.36); 3.3443 (713.81); 3.3210 (3.83); 3.3024 (0.58); 2.9067 (3.20); 2.9001 (6.96); 2.8935 (3.66);

2.8869 (1.01); 2.8805 (0.47); 2.6802 (0.44); 2.6757 (0.64); 2.6713 (0.41); 2.5730 (2.91); 2.5665 (3.13); 2.5564 (6.33); 2.5498 (6.37); 2.5397

(3.91); 2.5331 (4.11); 2.5154 (39.34); 2.5111 (78.78); 2.5067 (105.05); 2.5023 (74.78); 2.4980 (35.14); 2.3377 (0.50); 2.3334 (0.65); 2.3289

(0.47); 2.0901 (2.66); 2.0782 (0.62); 1.9929 (1.19); 1.4235 (0.61); 1.2382 (0.57); 1.1961 (0.35); 1.1784 (0.67); 1.1606 (0.37); 1.1448 (0.84);

1.1275 (1.87); 1.1100 (0.80); 1.0675 (1.39); 1.0599 (7.31); 1.0495 (3.20); 1.0418 (16.00); 1.0314 (1.91); 1.0237 (6.94)

›Example 105, Solvent: DMSO, Spectrometer: 399.95 MHz

10.6888 (2.29); 8.0230 (0.81); 8.0023 (1.05); 7.8853 (1.37); 7.8660 (1.90); 7.8458 (1.14); 7.7286 (2.72); 7.7157 (0.85); 7.7107 (3.53); 7.7070

(2.50); 7.5677 (0.49); 7.5558 (0.38); 7.5494 (1.72); 7.5437 (0.50); 7.5344 (0.92); 7.5311 (1.45); 7.5278 (0.74); 7.5000 (2.48); 7.4845 (1.77);

7.4808 (3.23); 7.4671 (0.52); 7.4631 (1.26); 7.4599 (0.72); 7.3445 (1.36); 7.3241 (2.63); 7.3037 (1.70); 7.2095 (1.86); 7.1910 (1.80); 7.0664

(1.30); 7.0612 (2.44); 7.0556 (1.80); 7.0393 (1.31); 7.0376 (1.44); 7.0347 (1.04); 7.0329 (0.93); 7.0196 (1.14); 7.0178 (1.14); 7.0149 (1.00);

7.0131 (0.84); 6.9594 (1.17); 6.9577 (1.14); 6.9533 (1.08); 6.9384 (1.06); 6.9323 (0.99); 5.3865 (6.45); 4.8441 (6.17); 3.3480 (144.23); 3.2984

(0.34); 3.0694 (16.00); 2.8911 (0.45); 2.7324 (0.35); 2.5262 (0.72); 2.5128 (13.63); 2.5084 (26.69); 2.5038 (34.77); 2.4993 (25.25); 2.4948

(12.15); −0.0002 (0.43)

›Example 106, Solvent: DMSO, Spectrometer: 399.95 MHz

10.2417 (2.97); 7.9536 (0.95); 7.8241 (0.68); 7.8032 (1.80); 7.7858 (2.31); 7.7775 (2.45); 7.7751 (2.42); 7.7569 (0.88); 7.7227 (2.89); 7.7047

(3.55); 7.7012 (2.48); 7.5630 (0.52); 7.5447 (1.70); 7.5394 (0.58); 7.5294 (1.13); 7.5267 (1.45); 7.4963 (2.60); 7.4769 (3.29); 7.4588 (1.64);

7.4539 (2.05); 7.4494 (2.24); 7.4435 (1.60); 7.4357 (2.21); 7.4307 (2.78); 7.4263 (1.72); 7.3234 (0.47); 7.3192 (0.61); 7.3050 (1.71); 7.3008

(1.58); 7.2944 (1.78); 7.2881 (2.65); 7.2825 (1.34); 7.2758 (1.44); 7.2708 (1.16); 7.2576 (0.62); 7.2524 (0.35); 7.2423 (0.38); 7.1068 (1.69);

7.1043 (1.56); 7.0896 (1.64); 7.0872 (1.47); 5.3307 (6.73); 4.3338 (1.79); 4.3167 (3.86); 4.2997 (1.85); 3.3359 (83.87); 3.0961 (1.82); 3.0791

(3.82); 3.0628 (16.00); 2.8910 (6.51); 2.7320 (5.63); 2.5076 (32.88); 2.5032 (39.64); 2.4988 (28.69); 2.4947 (14.33); 1.2352 (0.39); 0.0003

(5.61); −0.0002 (5.65)

›Example 107, Solvent: DMSO, Spectrometer: 399.95 MHz

10.1721 (2.46); 7.8286 (0.36); 7.8075 (2.24); 7.8003 (2.37); 7.7935 (5.60); 7.7793 (0.43); 7.7306 (0.33); 7.7250 (2.01); 7.7223 (2.61); 7.7185

(1.27); 7.7098 (0.80); 7.7046 (3.45); 7.7009 (2.39); 7.5616 (0.49); 7.5497 (0.38); 7.5433 (1.63); 7.5376 (0.49); 7.5284 (0.91); 7.5250 (1.44);

7.5216 (0.73); 7.4945 (2.40); 7.4911 (1.03); 7.4792 (1.69); 7.4754 (3.08); 7.4619 (0.50); 7.4578 (1.26); 7.4546 (0.69); 7.1006 (1.28); 7.0937

(1.26); 7.0866 (1.07); 7.0798 (1.21); 5.3301 (6.35); 4.0971 (1.77); 4.0804 (3.85); 4.0637 (1.82); 3.3283 (53.91); 3.0652 (16.00); 3.0545 (0.62);

2.5253 (0.57); 2.5205 (0.90); 2.5119 (11.11); 2.5074 (22.32); 2.5028 (29.56); 2.4982 (21.54); 2.4937 (10.36); 1.6184 (1.00); 1.6011 (1.41);

1.5818 (1.25); 1.5650 (0.47); 1.3629 (0.66); 1.3457 (0.90); 1.3334 (0.74); 1.3245 (0.96); 1.3098 (0.94); 1.2964 (2.73); 1.2872 (2.45); 1.2798

(2.81); 1.2710 (1.46); 1.2618 (0.93); 1.2345 (0.37); 0.8922 (0.61); 0.8869 (1.63); 0.8698 (5.16); 0.8595 (0.97); 0.8526 (1.69); −0.0002 (9.40)

›Example 108, Solvent: DMSO, Spectrometer: 400.13 MHz

7.9621 (1.63); 7.4051 (3.60); 7.3952 (3.49); 7.3888 (3.48); 7.2892 (2.92); 7.2696 (2.25); 7.2481 (4.22); 7.1363 (2.57); 7.1160 (2.18); 6.5182

(2.73); 6.5005 (2.58); 6.4004 (2.72); 6.3798 (2.56); 6.0273 (6.83); 5.9367 (0.32); 5.2248 (0.33); 5.1887 (9.33); 5.0260 (0.42); 3.7964 (16.00);

3.7671 (1.28); 3.3492 (7.06); 3.0848 (15.07); 2.8992 (6.82); 2.7403 (6.47); 2.5119 (33.94); 1.9999 (0.81); 1.3674 (2.15); 1.2435 (0.54); 1.2014

(0.33); 1.1841 (0.55)

›Example 109, Solvent: DMSO, Spectrometer: 399.95 MHz

10.3271 (3.10); 7.8427 (0.59); 7.8217 (2.51); 7.8111 (3.15); 7.8063 (5.43); 7.7907 (0.61); 7.7233 (3.28); 7.7050 (3.80); 7.7016 (2.83); 7.5629

(0.61); 7.5446 (1.89); 7.5391 (0.74); 7.5264 (1.63); 7.4964 (3.03); 7.4770 (3.60); 7.4594 (1.33); 7.1163 (1.58); 7.1106 (1.55); 7.1013 (1.43);

7.0957 (1.45); 6.0095 (0.33); 5.9963 (0.68); 5.9833 (0.68); 5.9700 (0.83); 5.9533 (0.85); 5.9402 (0.77); 5.9270 (0.81); 5.9139 (0.39); 5.3939

(1.55); 5.3897 (1.55); 5.3507 (2.00); 5.3495 (1.97); 5.3397 (8.04); 5.2409 (1.51); 5.2371 (1.45); 5.2146 (1.37); 5.2109 (1.32); 4.6268 (3.53);

4.6137 (3.35); 3.3417 (129.08); 3.0661 (16.00); 2.8909 (1.92); 2.7314 (1.69); 2.5077 (26.43); 2.5035 (32.92); 2.4992 (25.05)

›Example 110, Solvent: DMSO, Spectrometer: 399.95 MHz

10.0548 (2.57); 7.9532 (0.61); 7.8197 (0.51); 7.8038 (0.33); 7.7987 (1.99); 7.7830 (3.68); 7.7808 (3.18); 7.7646 (0.58); 7.7302 (0.33); 7.7247

(1.94); 7.7220 (2.61); 7.7182 (1.27); 7.7094 (0.79); 7.7043 (3.41); 7.7005 (2.35); 7.5617 (0.48); 7.5499 (0.36); 7.5434 (1.61); 7.5377 (0.48);

7.5285 (0.87); 7.5252 (1.43); 7.5217 (0.72); 7.4949 (2.40); 7.4915 (1.04); 7.4796 (1.62); 7.4758 (3.05); 7.4622 (0.47); 7.4581 (1.20); 7.4549

(0.67); 7.0923 (1.33); 7.0873 (1.33); 7.0766 (1.19); 7.0715 (1.26); 5.3225 (6.45); 5.0982 (0.54); 5.0902 (0.65); 5.0831 (0.91); 5.0762 (0.62);

5.0681 (0.50); 3.3296 (49.98); 3.0659 (16.00); 2.8907 (4.97); 2.7320 (3.82); 2.7311 (3.98); 2.5252 (0.63); 2.5203 (0.96); 2.5118 (10.77); 2.5073

(21.36); 2.5027 (28.12); 2.4981 (20.42); 2.4936 (9.73); 1.8855 (0.35); 1.8780 (0.43); 1.8663 (0.87); 1.8495 (0.80); 1.8362 (0.63); 1.8309 (0.55);

1.8225 (0.52); 1.7047 (0.59); 1.6833 (2.80); 1.6742 (1.66); 1.6689 (1.26); 1.6630 (1.06); 1.6539 (0.96); 1.6440 (0.57); 1.6363 (0.54); 1.5916

(0.45); 1.5826 (0.56); 1.5764 (0.64); 1.5611 (1.08); 1.5571 (0.89); 1.5509 (1.03); −0.0002 (7.45)

›Example 111, Solvent: DMSO, Spectrometer: 400.13 MHz

10.5173 (3.55); 8.0818 (2.07); 8.0610 (2.40); 7.8400 (1.49); 7.8204 (2.59); 7.8006 (1.35); 7.7321 (4.08); 7.7130 (4.68); 7.5713 (0.69); 7.5537

(2.02); 7.5358 (1.92); 7.5048 (3.39); 7.4858 (4.32); 7.4672 (1.60); 7.1487 (2.67); 7.1301 (2.55); 5.3622 (9.11); 4.0634 (0.77); 4.0458 (2.29);

4.0280 (2.34); 4.0104 (0.78); 3.5757 (1.57); 3.3373 (54.92); 3.0616 (16.00); 2.5108 (37.34); 2.3989 (2.30); 2.3805 (4.60); 2.3622 (2.55); 1.9970

(9.33); 1.6150 (0.58); 1.5967 (1.91); 1.5789 (2.76); 1.5616 (1.95); 1.5447 (0.63); 1.3107 (1.68); 1.2872 (4.54); 1.2794 (4.48); 1.2001 (2.47);

1.1823 (4.81); 1.1646 (2.43); 0.8870 (3.49); 0.8708 (7.31); 0.8535 (3.47)

›Example 112, Solvent: DMSO, Spectrometer: 400.13 MHz

10.1208 (2.89); 7.8322 (0.46); 7.8112 (1.96); 7.7990 (2.44); 7.7954 (3.87); 7.7783 (0.52); 7.4212 (1.03); 7.4012 (2.17); 7.3812 (1.57); 7.2836

(1.41); 7.2802 (1.23); 7.2667 (0.77); 7.2630 (1.17); 7.2609 (0.94); 7.2455 (1.55); 7.2396 (1.91); 7.2354 (1.30); 7.1432 (1.08); 7.1414 (1.11);

7.1368 (0.98); 7.1351 (0.95); 7.1226 (0.95); 7.1207 (0.92); 7.1163 (0.93); 7.0998 (1.28); 7.0945 (1.26); 7.0843 (1.15); 7.0791 (1.19); 5.7679

(0.34); 5.3315 (5.87); 4.6766 (0.39); 4.6635 (0.43); 4.6541 (0.70); 4.6446 (0.51); 4.6316 (0.34); 3.7886 (16.00); 3.4026 (2.53); 3.3527 (178.70);

3.3291 (0.82); 3.3028 (1.97); 3.0577 (14.67); 2.5595 (0.42); 2.5185 (11.43); 2.5141 (23.24); 2.5096 (31.23); 2.5051 (22.06); 2.5007 (10.07);

2.4597 (0.33); 1.8754 (0.69); 1.8619 (0.81); 1.8498 (0.83); 1.7325 (0.70); 1.7239 (0.75); 1.7097 (0.81); 1.7018 (0.74); 1.5284 (0.36); 1.5177

(0.38); 1.4971 (0.42); 1.4340 (0.80); 1.4088 (1.05); 1.3845 (1.17); 1.3585 (0.94); 1.3330 (0.71); 1.3263 (0.79); 1.3005 (0.41); 1.2779 (0.34);

1.2490 (0.53); 1.2223 (0.32)

›Example 113, Solvent: DMSO, Spectrometer: 399.95 MHz

12.5540 (0.80); 7.9538 (0.81); 7.7433 (1.98); 7.7404 (2.71); 7.7364 (1.31); 7.7280 (0.79); 7.7228 (3.57); 7.7190 (2.45); 7.6150 (1.60); 7.6111

(1.69); 7.5955 (1.74); 7.5915 (1.73); 7.5675 (0.49); 7.5561 (0.35); 7.5492 (1.69); 7.5433 (0.50); 7.5345 (0.94); 7.5311 (1.55); 7.5276 (0.77);

7.5052 (2.53); 7.5018 (1.07); 7.4902 (1.59); 7.4862 (3.09); 7.4729 (0.48); 7.4687 (1.26); 7.4652 (0.69); 7.3483 (4.70); 7.3229 (0.76); 7.3189

(0.76); 7.3043 (1.04); 7.3020 (1.20); 7.3006 (1.18); 7.2983 (1.03); 7.2837 (0.98); 7.2796 (0.92); 6.9421 (1.20); 6.9394 (1.71); 6.9307 (1.25);

6.9274 (0.83); 6.9212 (1.20); 6.9184 (1.52); 6.9117 (1.75); 6.9084 (1.26); 6.8926 (0.93); 6.8893 (0.75); 5.3443 (5.56); 5.1249 (0.37); 5.1085

(1.38); 5.0919 (1.38); 5.0754 (0.37); 3.3375 (33.52); 3.0312 (16.00); 2.8906 (6.70); 2.7329 (5.32); 2.7316 (5.38); 2.5217 (0.49); 2.5131 (6.08);

2.5086 (12.24); 2.5040 (16.21); 2.4994 (11.72); 2.4948 (5.51); 1.5957 (5.55); 1.5792 (5.51); −0.0002 (3.65)

›Example 114, Solvent: DMSO, Spectrometer: 399.95 MHz

10.8702 (1.70); 8.1751 (1.42); 8.1545 (1.70); 7.9528 (0.63); 7.9350 (1.32); 7.9154 (1.92); 7.8954 (1.21); 7.7304 (2.73); 7.7267 (1.39); 7.7174

(0.88); 7.7126 (3.87); 7.7090 (3.07); 7.6955 (1.19); 7.6910 (1.34); 7.6763 (0.74); 7.6721 (0.75); 7.6099 (0.35); 7.6053 (0.36); 7.5965 (0.39);

7.5916 (0.77); 7.5889 (0.59); 7.5872 (0.60); 7.5847 (0.51); 7.5767 (0.64); 7.5736 (0.64); 7.5707 (0.85); 7.5652 (0.83); 7.5616 (0.43); 7.5571

(0.53); 7.5528 (0.75); 7.5464 (1.70); 7.5408 (0.51); 7.5315 (0.93); 7.5282 (1.48); 7.5249 (0.76); 7.4981 (2.54); 7.4827 (1.70); 7.4790 (3.20);

7.4654 (0.50); 7.4614 (1.27); 7.4582 (0.74); 7.3500 (0.97); 7.3305 (1.97); 7.3254 (1.16); 7.3230 (1.02); 7.3137 (1.91); 7.3117 (1.78); 7.3044

(0.84); 7.3022 (0.81); 7.2951 (1.00); 7.2927 (0.81); 7.2431 (1.90); 7.2246 (1.80); 5.3929 (6.33); 3.3399 (89.26); 3.0941 (16.00); 3.0812 (0.41);

2.8906 (4.90); 2.7311 (3.99); 2.5255 (0.57); 2.5206 (0.91); 2.5121 (11.45); 2.5077 (22.91); 2.5031 (30.33); 2.4985 (22.07); 2.4940

(10.54); −0.0002 (1.99)

›Example 115, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5535 (2.14); 8.0453 (1.37); 8.0248 (1.75); 7.9533 (0.58); 7.8791 (1.33); 7.8597 (1.83); 7.8396 (1.15); 7.7277 (2.65); 7.7239 (1.28); 7.7149

(0.79); 7.7098 (3.48); 7.7061 (2.42); 7.5674 (0.50); 7.5554 (0.37); 7.5490 (1.69); 7.5434 (0.49); 7.5341 (0.87); 7.5308 (1.43); 7.5274 (0.72);

7.4986 (2.43); 7.4952 (1.03); 7.4831 (1.67); 7.4794 (3.16); 7.4657 (0.48); 7.4617 (1.25); 7.4585 (0.70); 7.2046 (1.82); 7.1866 (1.74); 7.0277

(0.86); 7.0235 (0.93); 7.0075 (1.89); 7.0037 (1.74); 6.9928 (1.10); 6.9892 (1.35); 6.9793 (1.11); 6.9733 (1.45); 6.9696 (1.93); 6.9605 (1.74);

6.9565 (1.00); 6.9409 (0.80); 6.9370 (0.55); 6.8791 (1.07); 6.8750 (1.06); 6.8600 (1.42); 6.8559 (1.24); 6.8409 (0.58); 6.8369 (0.54); 5.3912

(6.09); 4.9657 (0.34); 4.9492 (1.22); 4.9325 (1.22); 4.9160 (0.35); 3.8202 (15.07); 3.3287 (41.87); 3.0620 (16.00); 2.8905 (4.85); 2.7313 (3.79);

2.5251 (0.62); 2.5202 (1.01); 2.5117 (12.12); 2.5072 (24.14); 2.5026 (31.85); 2.4980 (23.10); 2.4935 (10.99); 1.5534 (5.69); 1.5368 (5.65);

0.0080 (0.39); −0.0002 (11.88); −0.0086 (0.37)

›Example 116, Solvent: DMSO, Spectrometer: 400.13 MHz

7.7403 (2.64); 7.7225 (3.27); 7.7188 (2.39); 7.5620 (0.53); 7.5503 (0.45); 7.5436 (1.64); 7.5379 (0.62); 7.5288 (1.03); 7.5256 (1.49); 7.4993

(2.51); 7.4803 (3.04); 7.4627 (1.21); 7.4594 (0.75); 7.3734 (1.12); 7.3554 (1.47); 7.3527 (1.43); 7.3347 (1.25); 6.5737 (0.68); 6.5594 (1.25);

6.5454 (0.68); 6.4757 (1.88); 6.4583 (1.83); 6.4262 (1.83); 6.4052 (1.78); 5.7631 (6.38); 5.1946 (6.31); 3.3269 (28.63); 3.3037 (0.54); 3.2732

(0.40); 3.0709 (16.00); 3.0541 (2.95); 3.0380 (1.79); 2.6757 (0.35); 2.5154 (22.73); 2.5112 (44.61); 2.5068 (59.64); 2.5024 (44.34); 2.3336

(0.48); 2.3289 (0.37); 1.7372 (1.18); 1.7049 (1.27); 1.6654 (1.03); 1.6368 (1.42); 1.6109 (0.90); 1.5936 (0.69); 1.5153 (0.46); 1.5035 (0.48);

1.4961 (0.57); 1.4872 (0.68); 1.4780 (0.58); 1.4693 (0.50); 1.4594 (0.43); 1.1809 (0.82); 1.1503 (1.56); 1.1275 (1.24); 1.0996 (0.36); 1.0938

(0.43); 0.9326 (0.53); 0.9028 (1.13); 0.8731 (1.01); 0.8453 (0.49)

›Example 117, Solvent: DMSO, Spectrometer: 400.13 MHz

10.3747 (3.00); 7.8516 (0.37); 7.8305 (2.52); 7.8245 (2.72); 7.8171 (5.74); 7.8036 (0.56); 7.5368 (2.33); 7.5220 (0.84); 7.5175 (0.74); 7.5125

(1.13); 7.5092 (1.16); 7.4998 (1.07); 7.4953 (0.82); 7.4443 (1.06); 7.4399 (1.48); 7.4232 (3.85); 7.4197 (3.53); 7.4154 (3.05); 7.4132 (2.99);

7.4078 (1.06); 7.3959 (3.95); 7.3913 (1.75); 7.3807 (1.43); 7.3767 (1.95); 7.3698 (2.93); 7.3685 (2.95); 7.3564 (4.77); 7.3457 (1.15); 7.3386

(1.55); 7.3308 (0.60); 7.3252 (0.51); 7.3212 (0.61); 7.3172 (0.41); 7.1149 (1.34); 7.1074 (1.36); 7.1015 (1.21); 7.0941 (1.31); 5.7646 (0.50);

5.3358 (6.92); 5.2055 (0.43); 5.1880 (7.58); 3.3664 (0.62); 3.3287 (11.77); 3.0586 (16.00); 2.5611 (0.48); 2.5569 (0.47); 2.5187 (10.61); 2.5143

(20.78); 2.5099 (27.63); 2.5054 (20.12); 2.5011 (10.23); 2.4685 (0.75); 2.4639 (0.79); 2.4593 (0.79); 2.3378 (11.35)

›Example 118, Solvent: DMSO, Spectrometer: 399.95 MHz

10.3719 (1.81); 8.0936 (0.97); 8.0729 (1.16); 7.9533 (0.46); 7.8377 (1.27); 7.8184 (1.73); 7.7982 (1.18); 7.7229 (2.03); 7.7203 (2.60); 7.7164

(1.24); 7.7074 (0.96); 7.7025 (3.46); 7.6987 (2.34); 7.5633 (0.50); 7.5514 (0.37); 7.5450 (1.66); 7.5393 (0.50); 7.5300 (0.89); 7.5267 (1.42);

7.5233 (0.71); 7.4956 (2.45); 7.4922 (1.03); 7.4803 (1.68); 7.4765 (3.14); 7.4629 (0.48); 7.4588 (1.25); 7.4556 (0.68); 7.1366 (1.73); 7.1356

(1.73); 7.1181 (1.67); 5.3482 (6.18); 3.3881 (0.63); 3.3675 (0.98); 3.3450 (1.22); 3.3310 (66.49); 3.0506 (16.00); 2.8910 (3.83); 2.7323 (3.00);

2.7314 (2.94); 2.5255 (0.56); 2.5207 (0.90); 2.5122 (10.83); 2.5076 (21.65); 2.5030 (28.64); 2.4984 (20.76); 2.4939 (9.81); 2.2280 (0.76);

2.2225 (0.64); 2.2043 (1.00); 2.1990 (1.29); 2.1826 (0.80); 2.1775 (1.17); 2.1550 (0.38); 2.1276 (0.33); 2.1207 (0.40); 2.1183 (0.41); 2.1060

(0.79); 2.0975 (1.04); 2.0908 (0.64); 2.0847 (0.68); 2.0758 (0.97); 2.0684 (0.57); 1.9514 (0.37); 1.9467 (0.32); 1.9286 (0.60); 1.9248 (0.61);

1.9076 (0.35); 1.9021 (0.83); 1.8808 (0.44); 1.7988 (0.53); 1.7880 (0.34); 1.7850 (0.33); 1.7746 (0.41); 0.8759 (0.50); 0.8627 (0.36); −0.0002

(5.96)

›Example 119, Solvent: DMSO, Spectrometer: 400.13 MHz

10.5103 (2.58); 7.8458 (0.89); 7.8253 (1.65); 7.8065 (1.51); 7.7503 (2.13); 7.7316 (3.58); 7.7193 (0.88); 7.7142 (3.30); 7.7105 (2.35); 7.5702

(0.47); 7.5583 (0.38); 7.5519 (1.61); 7.5462 (0.50); 7.5369 (0.91); 7.5337 (1.41); 7.5303 (0.74); 7.5036 (2.38); 7.4882 (1.66); 7.4845 (3.00);

7.4709 (0.49); 7.4669 (1.16); 7.4637 (0.68); 7.1399 (1.70); 7.1225 (1.65); 5.7646 (5.66); 5.3509 (6.05); 5.0796 (0.47); 5.0621 (1.86); 5.0444

(1.88); 5.0268 (0.48); 3.6946 (16.00); 3.3260 (15.16); 3.0829 (15.38); 2.5596 (0.41); 2.5319 (0.63); 2.5186 (12.09); 2.5142 (24.34); 2.5097

(32.66); 2.5052 (23.20); 2.5008 (10.83); 2.4598 (0.39); 1.9969 (0.93); 1.4619 (6.33); 1.4443 (6.26); 1.2544 (0.44); 1.1828 (0.51); 0.8664 (0.63)

›Example 120, Solvent: DMSO, Spectrometer: 400.13 MHz

9.8770 (1.66); 7.8031 (0.40); 7.7821 (1.16); 7.7651 (1.72); 7.7622 (1.52); 7.7582 (1.65); 7.7411 (0.55); 7.7369 (0.47); 7.7305 (1.28); 7.7277

(1.67); 7.7238 (0.88); 7.7152 (0.59); 7.7100 (2.21); 7.7063 (1.58); 7.5501 (1.04); 7.5444 (0.34); 7.5352 (0.60); 7.5318 (0.95); 7.5284 (0.52);

7.5012 (1.52); 7.4978 (0.72); 7.4859 (1.07); 7.4821 (1.97); 7.4686 (0.35); 7.4645 (0.83); 7.4613 (0.47); 7.0799 (0.87); 7.0761 (0.90); 7.0631

(0.85); 7.0593 (0.85); 5.3253 (3.92); 3.4053 (5.47); 3.3907 (0.44); 3.3555 (386.71); 3.3239 (2.18); 3.3057 (4.68); 3.0672 (10.54); 2.5628 (0.42);

2.5584 (0.60); 2.5538 (0.45); 2.5309 (1.03); 2.5262 (1.65); 2.5175 (16.50); 2.5131 (34.24); 2.5085 (47.05); 2.5040 (34.35); 2.4995 (17.21);

2.4634 (0.82); 2.4588 (0.82); 2.4543 (0.62); 1.7964 (0.40); 1.7779 (1.36); 1.7591 (1.45); 1.7407 (0.49); 1.4327 (16.00); 1.2515 (0.87); 0.9126

(1.76); 0.8941 (4.06); 0.8753 (1.92); 0.8632 (1.53); 0.8455 (0.60)

›Example 121, Solvent: DMSO, Spectrometer: 400.13 MHz

7.4804 (1.87); 7.4654 (5.40); 7.4431 (3.13); 7.4300 (2.24); 7.3773 (0.81); 7.3582 (3.18); 7.3431 (5.61); 6.5698 (2.81); 6.5518 (2.73); 6.4592

(2.87); 6.4384 (2.79); 6.2730 (0.68); 5.2206 (9.93); 4.6025 (1.13); 2.8986 (0.33); 2.5108 (35.19); 2.3426 (16.00); 1.3680 (0.35)

›Example 122, Solvent: DMSO, Spectrometer: 400.13 MHz

10.2685 (2.98); 7.8412 (0.42); 7.8202 (2.15); 7.8110 (2.41); 7.8053 (5.21); 7.7901 (0.50); 7.7290 (2.66); 7.7163 (0.88); 7.7113 (3.45); 7.7076

(2.43); 7.5675 (0.49); 7.5643 (0.33); 7.5556 (0.42); 7.5492 (1.67); 7.5435 (0.51); 7.5342 (0.92); 7.5309 (1.45); 7.5276 (0.75); 7.5000 (2.45);

7.4845 (1.76); 7.4808 (3.12); 7.4672 (0.53); 7.4632 (1.24); 7.4600 (0.73); 7.1118 (1.30); 7.1057 (1.29); 7.0972 (1.15); 7.0911 (1.24); 5.7661

(6.09); 5.3394 (6.38); 4.1390 (1.65); 4.1236 (3.56); 4.1078 (1.74); 3.3408 (21.83); 3.0678 (16.00); 2.5575 (0.36); 2.5300 (0.64); 2.5252 (1.07);

2.5165 (11.30); 2.5121 (22.87); 2.5076 (30.60); 2.5031 (21.66); 2.4987 (10.00); 2.4578 (0.36); 2.3548 (0.75); 2.3437 (0.49); 2.3348 (0.89);

2.3299 (0.74); 2.3257 (0.93); 2.3152 (0.88); 2.3061 (0.73); 2.2969 (0.41); 2.2862 (0.77); 1.9944 (0.92); 1.7148 (0.82); 1.6975 (1.24); 1.6794

(1.22); 1.6638 (0.52); 1.6264 (0.57); 1.6072 (1.12); 1.5987 (0.69); 1.5893 (1.26); 1.5748 (0.59); 1.5673 (0.74); 1.1788 (0.50); 0.8619 (0.38)

›Example 123, Solvent: DMSO, Spectrometer: 399.95 MHz

12.4657 (0.52); 7.7435 (1.98); 7.7407 (2.78); 7.7368 (1.34); 7.7284 (0.81); 7.7231 (3.56); 7.7193 (2.46); 7.6096 (3.22); 7.6031 (3.36); 7.5674

(0.49); 7.5642 (0.32); 7.5560 (0.35); 7.5491 (1.71); 7.5432 (0.52); 7.5344 (0.94); 7.5310 (1.58); 7.5275 (0.80); 7.5055 (2.62); 7.5022 (1.13);

7.4906 (1.60); 7.4865 (3.12); 7.4732 (0.49); 7.4691 (1.27); 7.4655 (0.71); 7.3681 (1.67); 7.3616 (1.59); 7.3458 (2.41); 7.3415 (5.22); 7.1019

(2.86); 7.0795 (2.44); 5.3418 (5.76); 5.0032 (6.64); 3.3373 (39.41); 3.0341 (16.00); 2.8904 (0.58); 2.7325 (0.45); 2.7313 (0.48); 2.5260 (0.37);

2.5213 (0.58); 2.5126 (7.10); 2.5081 (14.27); 2.5035 (18.89); 2.4989 (13.65); 2.4944 (6.45); −0.0002 (4.18)

›Example 124, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5358 (1.87); 8.1245 (1.44); 8.1040 (1.68); 7.9540 (0.34); 7.8403 (1.29); 7.8211 (1.78); 7.8008 (1.23); 7.7331 (0.32); 7.7251 (2.68); 7.7212

(1.36); 7.7124 (0.83); 7.7072 (3.64); 7.7035 (2.46); 7.5646 (0.49); 7.5614 (0.32); 7.5526 (0.37); 7.5463 (1.68); 7.5406 (0.53); 7.5313 (0.89);

7.5280 (1.43); 7.5246 (0.75); 7.4964 (2.51); 7.4930 (1.08); 7.4810 (1.73); 7.4773 (3.21); 7.4636 (0.50); 7.4596 (1.28); 7.4564 (0.71); 7.1509

(1.79); 7.1326 (1.76); 5.3651 (6.25); 3.3307 (55.19); 3.0885 (0.43); 3.0570 (16.00); 2.8913 (2.78); 2.7326 (2.23); 2.5257 (0.55); 2.5209 (0.89);

2.5124 (10.97); 2.5079 (21.87); 2.5033 (28.84); 2.4987 (20.95); 2.4942 (10.00); 2.4785 (0.51); 2.4675 (0.56); 2.4557 (0.78); 2.4435 (0.53);

2.4331 (0.42); 1.5830 (0.57); 1.5644 (0.75); 1.5604 (0.65); 1.5494 (1.04); 1.5419 (0.73); 1.5308 (1.10); 1.5270 (1.06); 1.5083 (0.92); 1.4565

(0.86); 1.4435 (1.04); 1.4380 (1.00); 1.4248 (1.29); 1.4101 (0.65); 1.4049 (0.78); 1.3916 (0.57); 1.2831 (0.40); 0.8761 (0.72); 0.8625 (0.55);

0.8497 (6.16); 0.8312 (13.00); 0.8126 (5.44); −0.0002 (6.14)

›Example 125, Solvent: DMSO, Spectrometer: 399.95 MHz

10.6838 (2.13); 8.0275 (0.70); 8.0071 (0.89); 7.9529 (0.51); 7.8836 (1.34); 7.8643 (1.83); 7.8441 (1.13); 7.7280 (2.62); 7.7242 (1.26); 7.7153

(0.76); 7.7103 (3.39); 7.7065 (2.35); 7.5672 (0.47); 7.5553 (0.35); 7.5488 (1.63); 7.5432 (0.47); 7.5339 (0.86); 7.5306 (1.41); 7.5273 (0.71);

7.4996 (2.39); 7.4962 (1.02); 7.4842 (1.62); 7.4804 (3.08); 7.4668 (0.47); 7.4628 (1.21); 7.4596 (0.68); 7.2637 (0.65); 7.2605 (0.68); 7.2418

(0.90); 7.2344 (0.71); 7.2306 (0.73); 7.2140 (0.86); 7.2070 (1.85); 7.1882 (1.71); 7.1166 (1.23); 7.1131 (1.25); 7.1062 (1.07); 7.0992 (2.47);

7.0861 (1.08); 7.0815 (1.08); 7.0656 (0.40); 6.9913 (0.47); 6.9839 (0.46); 6.9797 (0.57); 6.9753 (0.74); 6.9710 (0.51); 6.9688 (0.47); 6.9620

(0.72); 6.9595 (0.61); 6.9568 (0.81); 6.9417 (0.34); 5.3838 (6.25); 4.8919 (5.88); 3.3422 (120.00); 3.0701 (16.00); 2.8908 (4.16); 2.7314 (3.25);

2.5258 (0.59); 2.5209 (0.96); 2.5125 (12.14); 2.5080 (24.22); 2.5034 (32.04); 2.4988 (23.30); 2.4943 (11.11); −0.0002 (0.47)

›Example 126, Solvent: DMSO, Spectrometer: 399.95 MHz

12.2345 (1.79); 7.9531 (0.65); 7.7473 (0.32); 7.7416 (2.17); 7.7390 (2.79); 7.7350 (1.36); 7.7265 (0.85); 7.7213 (3.63); 7.7175 (2.55); 7.5658

(0.50); 7.5626 (0.34); 7.5544 (0.37); 7.5475 (1.77); 7.5416 (0.54); 7.5328 (0.99); 7.5294 (1.57); 7.5259 (0.79); 7.5039 (2.61); 7.5005 (1.12);

7.4889 (1.73); 7.4849 (3.27); 7.4715 (0.51); 7.4674 (1.27); 7.4638 (0.72); 7.3688 (0.58); 7.3548 (8.10); 7.3484 (3.98); 7.3392 (5.49); 7.3374

(5.17); 7.3256 (0.54); 7.3220 (0.68); 7.3198 (0.76); 7.3011 (0.72); 7.2948 (0.86); 7.2880 (0.73); 7.2835 (0.57); 7.2793 (0.84); 7.2704 (0.45);

7.2651 (0.33); 5.3402 (6.12); 4.8146 (0.33); 4.5665 (1.64); 4.5370 (2.66); 4.4470 (2.69); 4.4175 (1.75); 4.2618 (0.44); 4.2452 (1.72); 4.2284

(1.75); 4.2118 (0.45); 3.3318 (62.61); 3.0271 (16.00); 2.8906 (5.33); 2.7319 (4.34); 2.5251 (0.72); 2.5201 (1.16); 2.5117 (13.47); 2.5072 (26.54);

2.5026 (34.66); 2.4980 (25.07); 2.4935 (11.92); 2.2691 (0.44); 1.3627 (6.04); 1.3460 (5.97); −0.0002 (4.02)

›Example 127, Solvent: DMSO, Spectrometer: 400.13 MHz

10.2000 (6.98); 7.8389 (1.87); 7.8181 (4.15); 7.8002 (4.53); 7.7817 (5.60); 7.7629 (2.39); 7.7251 (6.61); 7.7073 (7.91); 7.7036 (5.68); 7.5740

(1.19); 7.5708 (0.90); 7.5621 (1.14); 7.5556 (3.97); 7.5500 (1.39); 7.5406 (2.48); 7.5376 (3.46); 7.5099 (6.02); 7.4907 (7.25); 7.4731 (2.66);

7.4700 (1.61); 7.1049 (3.87); 7.1031 (3.86); 7.0873 (3.71); 5.4189 (0.40); 5.3416 (14.90); 4.9351 (0.33); 4.9193 (1.53); 4.9040 (3.12); 4.8886

(3.12); 4.8733 (1.46); 3.5367 (2.01); 3.5187 (6.44); 3.5005 (6.54); 3.4824 (2.14); 3.4615 (0.52); 3.4113 (5.44); 3.3608 (562.41); 3.3260 (0.72);

3.3101 (8.40); 3.2614 (0.35); 2.9312 (3.09); 2.9247 (6.61); 2.9182 (3.06); 2.6840 (0.50); 2.6792 (0.64); 2.6749 (0.47); 2.5607 (1.30); 2.5565

(1.25); 2.5340 (7.87); 2.5278 (11.07); 2.5189 (47.05); 2.5147 (84.48); 2.5104 (107.33); 2.5060 (77.67); 2.4686 (0.81); 2.4641 (1.25); 2.4596

(1.62); 2.4551 (1.28); 2.3416 (0.54); 2.3373 (0.67); 2.3327 (0.48); 1.9964 (1.24); 1.3706 (1.15); 1.3167 (15.46); 1.3010 (15.61); 1.2836 (1.00);

1.2656 (0.90); 1.2502 (1.98); 1.1986 (0.44); 1.1808 (0.70); 1.1630 (0.37); 1.1258 (0.38); 1.0638 (7.30); 1.0458 (16.00); 1.0276 (7.04); 0.8805

(0.81); 0.8640 (2.18); 0.8463 (0.88)

›Example 128, Solvent: DMSO, Spectrometer: 399.95 MHz

10.7155 (2.03); 8.0201 (1.22); 7.9995 (1.58); 7.9531 (0.49); 7.8666 (1.32); 7.8474 (1.76); 7.8271 (1.13); 7.7281 (1.97); 7.7256 (2.53); 7.7217

(1.20); 7.7129 (0.76); 7.7078 (3.40); 7.7040 (2.35); 7.5673 (0.49); 7.5553 (0.35); 7.5490 (1.63); 7.5433 (0.47); 7.5340 (0.85); 7.5306 (1.40);

7.5272 (0.69); 7.4980 (2.33); 7.4946 (0.96); 7.4825 (1.64); 7.4788 (3.05); 7.4652 (0.47); 7.4611 (1.23); 7.4580 (0.68); 7.1982 (1.73); 7.1806

(1.68); 7.1660 (0.97); 7.1456 (2.10); 7.1255 (1.31); 6.7582 (2.69); 6.7413 (1.17); 6.7141 (0.88); 6.6937 (0.85); 6.6877 (0.71); 5.3827 (5.91);

5.0545 (1.06); 5.0380 (1.07); 3.3429 (107.22); 3.0573 (16.00); 2.8908 (4.15); 2.7323 (3.24); 2.7313 (3.21); 2.5260 (0.57); 2.5212 (0.93); 2.5126

(12.24); 2.5081 (24.48); 2.5035 (32.21); 2.4989 (23.19); 2.4944 (10.92); 2.2430 (9.37); 1.5184 (5.42); 1.5019 (5.40); −0.0002 (1.29)

›Example 129, Solvent: DMSO, Spectrometer: 400.13 MHz

7.6045 (0.61); 7.5849 (2.48); 7.5672 (8.15); 7.5630 (8.02); 7.5548 (9.54); 7.5335 (4.79); 7.5141 (2.65); 7.4570 (1.82); 7.4342 (2.49); 7.4185

(1.32); 6.6476 (4.56); 6.6296 (4.37); 6.5329 (4.74); 6.5120 (4.57); 6.3970 (0.74); 6.3109 (0.40); 5.3044 (16.00); 5.1127 (0.42); 5.0351 (0.34);

4.7538 (1.76); 4.5189 (0.41); 4.4872 (0.34); 2.9502 (0.66); 2.7909 (0.62); 2.5626 (54.18); 2.3891 (0.36); 1.4191 (0.50); −0.0002 (2.62)

›Example 130, Solvent: DMSO, Spectrometer: 400.13 MHz

10.6899 (5.67); 8.0245 (2.42); 8.0039 (3.35); 7.9045 (3.07); 7.8853 (4.11); 7.8650 (2.50); 7.7289 (5.97); 7.7252 (2.97); 7.7162 (1.84); 7.7112

(7.77); 7.7074 (5.51); 7.5829 (0.57); 7.5800 (1.08); 7.5768 (0.71); 7.5682 (0.82); 7.5616 (3.73); 7.5559 (1.15); 7.5467 (2.06); 7.5434 (3.29);

7.5400 (1.72); 7.5145 (5.55); 7.4992 (3.66); 7.4954 (6.95); 7.4819 (1.09); 7.4778 (2.68); 7.4746 (1.56); 7.2215 (4.06); 7.2037 (3.89); 7.0153

(2.78); 7.0110 (2.28); 7.0073 (1.43); 6.9983 (1.32); 6.9944 (5.05); 6.9904 (2.48); 6.9860 (0.80); 6.9096 (1.34); 6.9030 (1.64); 6.8933 (2.64);

6.8871 (4.18); 6.8820 (2.67); 6.8693 (9.15); 6.8657 (6.94); 6.8610 (4.65); 6.8495 (3.54); 6.8455 (0.95); 6.8371 (0.71); 6.8295 (0.67); 6.8255

(0.57); 5.3987 (13.52); 5.0934 (1.73); 5.0857 (2.23); 5.0819 (2.46); 5.0744 (1.78); 4.4509 (0.98); 4.4434 (1.16); 4.4215 (3.90); 4.4141 (3.74);

4.4071 (3.72); 4.3949 (3.44); 4.3776 (1.05); 4.3656 (1.10); 4.0433 (0.55); 4.0255 (0.55); 3.5160 (1.76); 3.4979 (5.98); 3.4797 (6.13); 3.4622

(2.17); 3.4131 (7.23); 3.3948 (0.59); 3.3824 (1.27); 3.3630 (703.91); 3.3279 (1.21); 3.3203 (1.10); 3.3134 (6.00); 2.6835 (0.40); 2.6789 (0.57);

2.6745 (0.41); 2.5645 (0.76); 2.5600 (0.98); 2.5555 (0.64); 2.5323 (1.32); 2.5276 (2.19); 2.5188 (33.47); 2.5144 (71.25); 2.5099 (97.99); 2.5054

(70.26); 2.5010 (32.73); 2.4647 (0.92); 2.4603 (1.04); 2.4559 (0.75); 2.3413 (0.47); 2.3367 (0.65); 2.3323 (0.46); 1.9958 (2.57); 1.3751 (0.35);

1.2514 (0.98); 1.1981 (0.72); 1.1803 (1.39); 1.1624 (0.67); 1.0707 (6.92); 1.0527 (16.00); 1.0344 (6.79); 0.8803 (0.46); 0.8635 (1.48); 0.8459

(0.57)

›Example 131, Solvent: DMSO, Spectrometer: 400.13 MHz

9.8705 (1.10); 7.7857 (0.75); 7.7701 (1.59); 7.7666 (1.14); 7.4220 (0.40); 7.4020 (0.87); 7.3820 (0.66); 7.2838 (0.56); 7.2814 (0.50); 7.2642

(0.47); 7.2621 (0.38); 7.2465 (0.61); 7.2407 (0.78); 7.2365 (0.54); 7.1422 (0.46); 7.1374 (0.47); 7.1234 (0.39); 7.1214 (0.41); 7.1170 (0.43);

7.0818 (0.53); 7.0772 (0.54); 7.0659 (0.49); 7.0612 (0.51); 5.3238 (2.45); 3.7901 (6.40); 3.7597 (0.86); 3.3412 (4.16); 3.0542 (5.92); 2.5596

(0.38); 2.5318 (0.39); 2.5182 (9.59); 2.5139 (19.99); 2.5094 (27.16); 2.5050 (19.46); 2.5006 (9.11); 2.4638 (0.36); 2.4592 (0.49); 2.4546 (0.36);

1.4692 (16.00); 1.3642 (2.08)

›Example 132, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5084 (1.89); 8.0977 (1.47); 8.0771 (1.73); 7.9534 (0.51); 7.8376 (1.28); 7.8183 (1.78); 7.7981 (1.20); 7.7242 (2.60); 7.7204 (1.26); 7.7115

(0.79); 7.7064 (3.42); 7.7027 (2.37); 7.5651 (0.48); 7.5532 (0.36); 7.5468 (1.63); 7.5411 (0.48); 7.5318 (0.87); 7.5285 (1.41); 7.5251 (0.72);

7.4974 (2.42); 7.4941 (1.04); 7.4820 (1.66); 7.4783 (3.08); 7.4647 (0.48); 7.4606 (1.22); 7.4575 (0.68); 7.1466 (1.79); 7.1289 (1.74); 5.3609

(6.34); 3.3353 (90.78); 3.0575 (16.00); 2.8911 (4.14); 2.7323 (3.28); 2.6169 (0.38); 2.6002 (0.62); 2.5815 (0.65); 2.5645 (0.43); 2.5258 (0.58);

2.5124 (11.50); 2.5079 (22.88); 2.5033 (30.06); 2.4987 (21.84); 2.4942 (10.42); 1.6265 (0.39); 1.6076 (0.56); 1.5929 (0.60); 1.5879 (0.49);

1.5739 (0.72); 1.5543 (0.52); 1.4098 (0.44); 1.3949 (0.61); 1.3914 (0.54); 1.3764 (0.84); 1.3614 (0.42); 1.3579 (0.55); 1.3430 (0.35); 1.0670

(6.48); 1.0500 (6.37); 0.8591 (3.34); 0.8406 (7.10); 0.8221 (2.95); −0.0002 (3.50)

›Example 133, Solvent: DMSO, Spectrometer: 399.95 MHz

10.2555 (2.88); 7.9531 (0.76); 7.8280 (0.44); 7.8069 (2.11); 7.7965 (2.37); 7.7915 (4.71); 7.7756 (0.51); 7.7315 (0.33); 7.7259 (2.06); 7.7234

(2.70); 7.7195 (1.31); 7.7107 (0.85); 7.7056 (3.55); 7.7019 (2.45); 7.5632 (0.50); 7.5600 (0.32); 7.5513 (0.38); 7.5448 (1.69); 7.5392 (0.51);

7.5300 (0.91); 7.5266 (1.46); 7.5232 (0.75); 7.4961 (2.48); 7.4928 (1.06); 7.4807 (1.71); 7.4770 (3.17); 7.4634 (0.50); 7.4593 (1.26); 7.4561

(0.71); 7.2626 (0.99); 7.2462 (1.42); 7.2345 (0.83); 7.2249 (1.11); 7.2124 (1.27); 7.1728 (0.56); 7.1672 (0.56); 7.1604 (1.25); 7.1500 (1.89);

7.1427 (0.74); 7.1365 (2.59); 7.1339 (2.60); 7.1288 (1.07); 7.1246 (2.62); 7.1186 (0.97); 7.1123 (1.83); 7.1086 (1.48); 7.1028 (1.38); 7.0936

(1.21); 7.0878 (1.28); 5.3338 (6.42); 4.3817 (0.48); 4.2754 (1.63); 4.2574 (3.43); 4.2394 (1.67); 3.3352 (98.43); 3.0632 (16.00); 3.0034 (0.39);

2.9546 (1.54); 2.9366 (3.11); 2.9187 (1.46); 2.8904 (6.13); 2.7320 (4.83); 2.7312 (4.79); 2.5252 (0.65); 2.5119 (12.06); 2.5074 (23.69); 2.5028

(30.99); 2.4982 (22.39); 2.4937 (10.61); 2.3295 (0.32); 2.3147 (12.20); 2.3068 (1.71); −0.0002 (3.96)

›Example 134, Solvent: DMSO, Spectrometer: 399.95 MHz

10.6679 (2.32); 8.1176 (1.76); 8.0970 (2.18); 7.9559 (2.46); 7.9543 (2.55); 7.9518 (2.58); 7.9093 (1.35); 7.8900 (1.98); 7.8698 (1.21); 7.7338

(2.71); 7.7208 (0.88); 7.7158 (3.43); 7.7121 (2.48); 7.6437 (2.27); 7.6348 (2.35); 7.5669 (0.49); 7.5550 (0.38); 7.5486 (1.70); 7.5430 (0.50);

7.5336 (0.94); 7.5304 (1.44); 7.5272 (0.76); 7.5003 (2.49); 7.4846 (1.77); 7.4810 (3.22); 7.4673 (0.52); 7.4633 (1.23); 7.4602 (0.73); 7.2176

(1.98); 7.1991 (1.92); 6.7062 (1.85); 6.7020 (1.84); 6.6974 (1.83); 6.6931 (1.77); 5.4100 (6.80); 3.3312 (65.24); 3.0741 (16.00); 2.8911 (0.91);

2.7321 (0.72); 2.5253 (0.67); 2.5119 (13.07); 2.5076 (25.52); 2.5030 (33.26); 2.4985 (24.41); 2.4941 (11.98); −0.0002 (5.84)

›Example 135, Solvent: DMSO, Spectrometer: 400.13 MHz

9.7994 (1.17); 7.9562 (0.46); 7.7879 (0.36); 7.7672 (0.81); 7.7492 (0.90); 7.7326 (1.08); 7.7138 (0.48); 7.6212 (1.23); 7.6039 (1.49); 7.6000

(1.17); 7.4966 (0.72); 7.4822 (0.54); 7.4789 (0.74); 7.4606 (1.25); 7.4417 (1.39); 7.4245 (0.53); 7.4207 (0.36); 7.1002 (0.73); 7.0834 (0.68);

5.2749 (2.71); 2.8902 (2.75); 2.7331 (2.41); 2.5106 (1.90); 2.5063 (2.63); 2.5021 (2.11); 1.4645 (16.00)

›Example 136, Solvent: DMSO, Spectrometer: 400.13 MHz

7.7386 (7.06); 7.7194 (7.83); 7.5623 (1.43); 7.5440 (3.55); 7.5268 (3.76); 7.4980 (6.64); 7.4791 (7.19); 7.4584 (3.89); 7.4491 (2.27); 7.4371

(2.93); 7.4295 (3.06); 7.4180 (1.98); 7.4101 (1.94); 7.3781 (9.20); 7.3675 (8.11); 7.3352 (13.24); 7.3215 (2.70); 7.3138 (2.77); 7.2998 (2.34);

7.0484 (0.99); 7.0341 (1.89); 7.0195 (0.95); 6.9628 (1.01); 6.9490 (1.96); 6.9344 (0.99); 6.7934 (1.31); 6.7841 (2.50); 6.7748 (1.34); 6.5917

(2.68); 6.5833 (3.05); 6.5748 (2.80); 6.5661 (2.71); 6.4748 (2.59); 6.4548 (2.97); 6.4406 (2.08); 5.7694 (4.38); 5.2201 (9.46); 5.2111 (8.76);

5.1866 (0.43); 5.1027 (8.78); 5.0127 (9.99); 4.1298 (2.33); 4.1182 (3.52); 4.1069 (2.32); 3.9865 (2.39); 3.9731 (4.39); 3.9595 (2.38); 3.3566

(261.77); 3.0785 (16.00); 3.0673 (14.86); 2.6802 (0.64); 2.5109 (112.20); 2.3375 (0.71); 1.9968 (0.47); 1.2410 (1.10); 1.1970 (0.52); 1.1808

(0.42)

›Example 137, Solvent: DMSO, Spectrometer: 399.95 MHz

9.5609 (1.79); 7.9684 (1.41); 7.9489 (1.96); 7.8400 (1.34); 7.8209 (1.73); 7.8005 (1.10); 7.7295 (1.84); 7.7268 (2.44); 7.7229 (1.15); 7.7142

(0.72); 7.7091 (3.30); 7.7053 (2.26); 7.5658 (0.46); 7.5539 (0.33); 7.5475 (1.56); 7.5418 (0.45); 7.5326 (0.83); 7.5292 (1.37); 7.5258 (0.68);

7.4984 (2.27); 7.4950 (0.94); 7.4831 (1.54); 7.4793 (2.95); 7.4658 (0.45); 7.4617 (1.19); 7.4584 (0.65); 7.1598 (1.66); 7.1425 (1.61); 5.3806

(6.19); 3.3343 (88.20); 3.0852 (16.00); 2.8907 (0.83); 2.7320 (0.65); 2.7310 (0.64); 2.5252 (0.49); 2.5204 (0.83); 2.5119 (10.80); 2.5073 (21.58);

2.5027 (28.42); 2.4981 (20.44); 2.4935 (9.57); 1.4156 (10.91); 1.1357 (0.90); 1.1262 (2.74); 1.1193 (2.82); 1.1102 (0.97); 0.6700 (1.20); 0.6606

(3.75); 0.6536 (3.64); 0.6438 (1.02); −0.0002 (4.44)

Example, 138, Solvent: DMSO, Spectrometer: 399.95 MHz

9.3214 (4.34); 7.9528 (0.64); 7.8496 (0.82); 7.8288 (1.76); 7.8212 (0.36); 7.8107 (2.04); 7.7894 (1.01); 7.7689 (0.50); 7.7356 (0.75); 7.7272

(3.86); 7.7143 (1.32); 7.7092 (4.15); 7.7061 (3.82); 7.5502 (0.73); 7.5466 (0.64); 7.5390 (1.03); 7.5317 (1.96); 7.5255 (0.93); 7.5214 (0.88);

7.5167 (1.07); 7.5133 (1.47); 7.5101 (0.86); 7.5043 (0.51); 7.4953 (1.42); 7.4917 (0.70); 7.4852 (0.75); 7.4798 (1.52); 7.4753 (3.64); 7.4585

(2.46); 7.4551 (3.67); 7.4412 (0.57); 7.4372 (1.40); 7.4346 (1.10); 7.4021 (0.63); 7.3839 (0.77); 7.3816 (0.78); 7.3634 (0.67); 7.2262 (0.36);

7.1755 (1.67); 7.1702 (0.53); 7.1564 (1.81); 7.1539 (2.14); 7.1411 (0.58); 7.1359 (1.67); 7.1106 (1.67); 7.0906 (1.59); 6.7768 (0.75); 6.7742

(0.60); 6.7586 (3.42); 6.7560 (3.28); 6.7370 (3.18); 6.5114 (0.86); 6.4936 (0.82); 6.3910 (0.88); 6.3707 (0.84); 6.0040 (1.40); 5.3782 (0.80);

5.3568 (5.89); 5.3350 (0.50); 5.1786 (3.26); 3.6697 (0.72); 3.3651 (0.33); 3.3346 (122.05); 3.0915 (2.64); 3.0877 (8.10); 3.0806 (1.02); 3.0724

(16.00); 3.0607 (1.07); 2.9337 (0.41); 2.8904 (5.29); 2.7312 (4.16); 2.6719 (0.33); 2.5251 (0.95); 2.5203 (1.57); 2.5118 (19.46); 2.5073 (38.76);

2.5027 (51.18); 2.4981 (37.17); 2.4936 (17.78); 2.3295 (0.33); 1.2343 (0.35); −0.0002 (6.98)

›Example 139, Solvent: DMSO, Spectrometer: 400.13 MHz

9.8766 (0.82); 8.0302 (0.60); 8.0096 (0.74); 7.8519 (0.47); 7.8325 (0.65); 7.8124 (0.41); 7.6227 (0.35); 7.6169 (0.33); 7.6073 (0.42); 7.6020

(0.38); 7.5973 (0.42); 7.5909 (0.79); 7.5877 (0.75); 7.5458 (0.40); 7.5314 (0.42); 7.4130 (0.32); 7.1691 (0.67); 7.1508 (0.63); 5.7692 (0.38);

5.4057 (2.29); 3.3933 (0.38); 3.3440 (19.84); 3.0759 (5.46); 2.5592 (0.39); 2.5321 (0.47); 2.5186 (7.96); 2.5144 (16.08); 2.5099 (21.64); 2.5055

(15.59); 2.5012 (7.37); 2.4607 (0.32); 1.2391 (16.00)

›Example 140, Solvent: DMSO, Spectrometer: 400.13 MHz

10.5354 (2.37); 8.0859 (1.40); 8.0651 (1.66); 7.8428 (1.32); 7.8234 (1.94); 7.8033 (1.23); 7.6261 (0.71); 7.6221 (1.05); 7.6166 (0.99); 7.6071

(1.24); 7.6035 (1.11); 7.6015 (1.13); 7.5969 (1.29); 7.5905 (2.43); 7.5876 (2.31); 7.5656 (0.79); 7.5515 (0.87); 7.5455 (1.19); 7.5311 (1.25);

7.5261 (0.64); 7.5105 (0.56); 7.4358 (0.56); 7.4331 (0.62); 7.4296 (0.57); 7.4267 (0.53); 7.4118 (1.00); 7.4082 (0.89); 7.3936 (0.45); 7.3909

(0.47); 7.3875 (0.43); 7.3849 (0.38); 7.1570 (2.00); 7.1388 (1.90); 5.7688 (0.56); 5.3810 (6.74); 3.4004 (0.34); 3.3503 (27.17); 3.0553 (16.00);

2.5186 (7.86); 2.5145 (15.63); 2.5101 (20.87); 2.5057 (15.18); 2.4070 (1.91); 2.3887 (3.50); 2.3701 (2.06); 1.5946 (0.49); 1.5764 (1.45); 1.5577

(2.04); 1.5392 (1.53); 1.5202 (0.60); 1.3689 (0.44); 1.3480 (0.33); 1.3294 (1.18); 1.3105 (1.90); 1.2918 (1.90); 1.2736 (1.13); 1.2555 (0.34);

0.9042 (4.19); 0.8859 (8.38); 0.8675 (3.52)

›Example 141, Solvent: DMSO, Spectrometer: 400.13 MHz

8.0012 (0.53); 7.9817 (0.34); 7.4837 (0.42); 7.4665 (0.55); 7.4474 (0.51); 7.4389 (0.48); 7.4274 (0.40); 7.4191 (0.45); 7.3333 (0.33); 7.3321

(0.34); 7.3009 (0.40); 7.2951 (0.47); 7.2910 (0.32); 5.8270 (3.36); 5.4783 (1.27); 3.8397 (3.61); 3.4023 (0.92); 3.1102 (3.32); 2.5841 (0.35);

2.5753 (3.05); 2.5709 (6.29); 2.5664 (8.57); 2.5619 (6.29); 2.5575 (3.16); 1.4626 (0.32); 1.4540 (0.53); 1.4277 (0.56); 1.4127 (16.00)

›Example 142, Solvent: DMSO, Spectrometer: 300.16 MHz

9.9207 (1.35); 7.8411 (0.82); 7.8200 (1.98); 7.5956 (1.21); 7.5715 (0.53); 7.5558 (0.46); 7.4284 (1.27); 7.4118 (1.51); 7.1316 (0.58); 7.1251

(0.56); 7.1112 (0.54); 7.1049 (0.54); 5.3722 (2.91); 3.3955 (6.45); 3.1134 (5.84); 2.5655 (25.41); 2.3954 (4.77); 1.5257 (16.00)

›Example 143, Solvent: DMSO, Spectrometer: 399.95 MHz

12.8077 (1.19); 8.4458 (1.46); 8.4417 (2.61); 8.4376 (1.47); 8.0836 (0.87); 8.0811 (1.17); 8.0771 (0.91); 8.0641 (0.97); 8.0615 (1.19); 8.0601

(1.17); 8.0574 (0.94); 8.0075 (0.87); 8.0050 (1.09); 8.0012 (0.84); 7.9879 (0.96); 7.9852 (1.13); 7.9841 (1.15); 7.9817 (0.86); 7.9533 (0.35);

7.7500 (1.92); 7.7472 (2.58); 7.7432 (1.25); 7.7349 (0.77); 7.7297 (3.37); 7.7259 (2.36); 7.5685 (0.46); 7.5501 (1.63); 7.5442 (0.49); 7.5355

(0.91); 7.5321 (1.50); 7.5285 (0.75); 7.5078 (2.44); 7.5044 (1.05); 7.4929 (1.53); 7.4889 (3.00); 7.4755 (0.48); 7.4713 (1.23); 7.4677 (0.71);

7.3930 (3.28); 7.3685 (1.40); 7.3489 (2.57); 7.3293 (1.27); 5.3839 (5.38); 3.3336 (58.22); 3.0204 (16.00); 2.8913 (2.75); 2.7326 (2.25); 2.7314

(2.13); 2.5259 (0.59); 2.5210 (0.97); 2.5125 (12.27); 2.5080 (24.58); 2.5034 (32.37); 2.4988 (23.49); 2.4942 (11.18); −0.0002 (6.97)

›Example 144, Solvent: DMSO, Spectrometer: 399.95 MHz

10.7760 (2.24); 8.1665 (1.64); 8.1460 (1.99); 7.9514 (3.83); 7.9307 (3.59); 7.9126 (1.28); 7.8932 (1.80); 7.8730 (1.17); 7.7392 (2.03); 7.7368

(2.57); 7.7330 (1.24); 7.7242 (0.77); 7.7190 (3.36); 7.7153 (2.37); 7.5669 (0.47); 7.5551 (0.34); 7.5486 (1.65); 7.5428 (0.48); 7.5336 (0.88);

7.5303 (1.44); 7.5269 (0.72); 7.5005 (2.40); 7.4972 (1.03); 7.4852 (1.63); 7.4814 (3.09); 7.4679 (0.47); 7.4638 (1.22); 7.4605 (0.69); 7.3221

(2.78); 7.3022 (2.64); 7.2180 (1.81); 7.1996 (1.76); 5.4154 (6.26); 3.3274 (26.08); 3.0820 (16.00); 2.8906 (5.83); 2.7320 (4.83); 2.7309 (4.48);

2.5249 (0.62); 2.5200 (0.95); 2.5115 (11.35); 2.5070 (22.54); 2.5024 (29.51); 2.4978 (21.28); 2.4933 (10.05); 2.3820 (9.07); 0.0080

(0.39); −0.0002 (11.73); −0.0085 (0.35)

›Example 145, Solvent: DMSO, Spectrometer: 399.95 MHz

10.2168 (2.70); 7.9531 (1.06); 7.8111 (0.84); 7.7903 (1.73); 7.7721 (1.81); 7.7448 (2.06); 7.7213 (3.16); 7.7082 (0.87); 7.7033 (3.55); 7.6995

(2.49); 7.5627 (0.50); 7.5597 (0.33); 7.5508 (0.38); 7.5443 (1.72); 7.5388 (0.52); 7.5294 (0.93); 7.5262 (1.48); 7.5229 (0.77); 7.4952 (2.56);

7.4797 (1.74); 7.4760 (3.26); 7.4624 (0.51); 7.4584 (1.27); 7.4553 (0.73); 7.3365 (0.59); 7.3230 (10.19); 7.3156 (4.69); 7.3091 (4.05); 7.2942

(0.40); 7.2883 (0.61); 7.2473 (0.38); 7.2388 (0.87); 7.2319 (0.95); 7.2251 (1.17); 7.2172 (0.97); 7.2100 (0.63); 7.2031 (0.48); 7.0974 (1.68);

7.0958 (1.71); 7.0795 (1.65); 7.0778 (1.59); 5.3271 (6.50); 4.2373 (0.82); 4.2206 (0.85); 4.2107 (1.50); 4.1939 (1.60); 4.1628 (1.50); 4.1452

(1.50); 4.1363 (0.84); 4.1185 (0.84); 3.3406 (110.56); 3.1332 (0.56); 3.1158 (1.17); 3.0985 (1.16); 3.0811 (0.62); 3.0707 (0.48); 3.0575 (16.00);

2.8906 (8.37); 2.7315 (6.74); 2.5256 (0.61); 2.5123 (11.84); 2.5078 (23.42); 2.5032 (30.78); 2.4987 (22.39); 2.4942 (10.74); 1.2814 (6.61);

1.2638 (6.42); 1.2341 (0.38); −0.0002 (2.62)

›Example 146, Solvent: DMSO, Spectrometer: 399.95 MHz

10.3818 (2.06); 8.0962 (1.40); 8.0757 (1.65); 7.9536 (0.91); 7.8276 (1.26); 7.8084 (1.74); 7.7881 (1.21); 7.7257 (2.07); 7.7233 (2.63); 7.7195

(1.31); 7.7105 (0.82); 7.7055 (3.58); 7.7017 (2.45); 7.5629 (0.49); 7.5509 (0.36); 7.5446 (1.67); 7.5389 (0.53); 7.5296 (0.87); 7.5262 (1.43);

7.5228 (0.73); 7.4943 (2.46); 7.4909 (1.05); 7.4789 (1.70); 7.4752 (3.19); 7.4616 (0.51); 7.4575 (1.28); 7.4543 (0.72); 7.1423 (1.77); 7.1247

(1.72); 5.3537 (6.07); 4.0414 (0.85); 4.0236 (0.86); 3.3291 (57.76); 3.0882 (0.54); 3.0529 (16.00); 2.8912 (7.65); 2.7324 (6.12); 2.7314 (5.78);

2.5254 (0.58); 2.5206 (0.91); 2.5121 (11.85); 2.5076 (23.77); 2.5030 (31.40); 2.4984 (22.77); 2.4938 (10.80); 2.1529 (5.48); 2.0176 (1.69);

1.9178 (2.86); 1.6667 (1.21); 1.6366 (2.71); 1.6109 (7.81); 1.6055 (7.95); 1.5610 (2.66); 1.2831 (0.33); 1.2352 (0.33); 1.1917 (0.93); 1.1739

(1.88); 1.1561 (0.91); 0.8758 (0.58); 0.8625 (0.33); −0.0002 (6.70)

›Example 147, Solvent: DMSO, Spectrometer: 399.95 MHz

11.9704 (0.36); 10.4304 (2.10); 8.0659 (1.50); 8.0454 (1.81); 7.9529 (0.46); 7.8238 (1.30); 7.8045 (1.86); 7.7843 (1.20); 7.7229 (2.66); 7.7100

(0.84); 7.7050 (3.49); 7.7012 (2.46); 7.5644 (0.48); 7.5526 (0.38); 7.5461 (1.72); 7.5405 (0.50); 7.5312 (0.91); 7.5279 (1.45); 7.5246 (0.77);

7.4971 (2.47); 7.4815 (1.76); 7.4779 (3.20); 7.4642 (0.54); 7.4602 (1.29); 7.4571 (0.72); 7.1333 (1.90); 7.1150 (1.84); 5.3533 (6.54); 3.3413

(110.17); 3.0575 (16.00); 2.8912 (3.64); 2.7322 (2.97); 2.5260 (0.93); 2.5125 (13.33); 2.5081 (25.98); 2.5035 (33.74); 2.4989 (24.85); 2.4945

(12.02); 2.4717 (0.56); 2.1829 (0.57); 2.1739 (0.42); 1.7926 (1.41); 1.7734 (1.25); 1.7574 (1.49); 1.7363 (0.78); 1.7133 (1.18); 1.6766 (0.48);

1.6692 (0.67); 1.6595 (0.74); 1.6472 (1.22); 1.6404 (1.12); 1.5845 (0.37); 1.5584 (0.35); 1.4195 (0.37); 1.3890 (1.02); 1.3595 (1.21); 1.3345

(1.05); 1.2999 (0.93); 1.2800 (1.00); 1.2561 (1.61); 1.2328 (1.38); 1.2257 (1.87); 1.1971 (1.71); 1.1755 (0.81); 1.1456 (0.56)

›Example 148, Solvent: DMSO, Spectrometer: 400.13 MHz

9.8673 (1.22); 8.0280 (0.79); 8.0071 (0.99); 7.8490 (0.51); 7.8296 (0.88); 7.8096 (0.45); 7.7332 (1.37); 7.7139 (1.59); 7.5537 (0.67); 7.5359

(0.65); 7.5048 (1.14); 7.4857 (1.46); 7.4668 (0.56); 7.1608 (0.90); 7.1422 (0.87); 5.3883 (3.07); 4.0449 (0.84); 4.0271 (0.85); 3.3422 (15.57);

3.0829 (5.43); 2.5104 (12.92); 1.9970 (3.42); 1.2408 (16.00); 1.2104 (0.39); 1.1994 (0.97); 1.1816 (1.80); 1.1638 (0.91)

›Example 149, Solvent: DMSO, Spectrometer: 400.13 MHz

10.1013 (2.94); 7.8300 (0.34); 7.8089 (2.20); 7.8021 (2.37); 7.7952 (5.34); 7.7811 (0.55); 7.4210 (1.01); 7.4010 (2.16); 7.3810 (1.59); 7.2843

(1.41); 7.2829 (1.43); 7.2806 (1.29); 7.2674 (0.81); 7.2635 (1.23); 7.2612 (1.04); 7.2457 (1.56); 7.2398 (1.98); 7.2356 (1.44); 7.1433 (1.06);

7.1413 (1.12); 7.1369 (1.02); 7.1350 (0.99); 7.1227 (0.99); 7.1206 (0.97); 7.1162 (1.03); 7.1144 (0.97); 7.1009 (1.29); 7.0939 (1.29); 7.0872

(1.14); 7.0802 (1.26); 5.7687 (0.43); 5.3307 (5.86); 4.9258 (0.42); 4.9130 (0.56); 4.9102 (0.56); 4.9042 (0.55); 4.8976 (0.57); 4.8916 (0.58);

4.8890 (0.58); 4.8762 (0.46); 3.7889 (16.00); 3.7665 (0.33); 3.3998 (0.86); 3.3496 (73.70); 3.3263 (1.03); 3.2994 (0.68); 3.0617 (14.72); 2.5189

(7.09); 2.5145 (14.73); 2.5100 (20.22); 2.5055 (14.96); 2.5011 (7.60); 2.4646 (0.38); 2.4604 (0.36); 1.6952 (0.45); 1.6763 (0.57); 1.6596 (0.56);

1.6432 (0.36); 1.5914 (0.50); 1.5767 (0.41); 1.5700 (0.53); 1.5569 (0.83); 1.5424 (0.58); 1.5357 (0.68); 1.5210 (0.53); 1.3563 (0.60); 1.3439

(0.67); 1.3361 (0.58); 1.3229 (0.90); 1.3096 (0.50); 1.3017 (0.50); 1.2893 (0.45); 1.2349 (6.21); 1.2193 (6.25); 0.9022 (8.57); 0.9003 (8.65);

0.8857 (8.73); 0.8840 (8.67)

›Example 150, Solvent: DMSO, Spectrometer: 400.13 MHz

11.7624 (1.72); 7.6204 (1.22); 7.6135 (1.44); 7.6094 (1.46); 7.5993 (1.11); 7.5894 (3.38); 7.5669 (0.91); 7.5528 (0.99); 7.5467 (1.29); 7.5324

(1.29); 7.5277 (0.82); 7.5116 (0.57); 7.4290 (0.71); 7.4263 (0.71); 7.4230 (0.65); 7.4201 (0.60); 7.4055 (1.11); 7.4010 (0.99); 7.3868 (0.51);

7.3834 (0.54); 7.3781 (0.42); 7.2771 (4.69); 5.3063 (6.66); 4.1630 (2.10); 4.1463 (4.45); 4.1296 (2.18); 3.8448 (0.41); 3.4517 (0.41); 3.4024

(4.01); 3.3520 (239.49); 3.3008 (3.74); 3.0281 (16.00); 2.5629 (0.48); 2.5584 (0.73); 2.5541 (0.67); 2.5165 (16.72); 2.5125 (32.52); 2.5081

(43.23); 2.5037 (32.17); 2.4663 (0.80); 2.4614 (0.88); 2.4568 (1.02); 2.4523 (0.93); 1.9939 (0.36); 1.6609 (0.34); 1.6434 (1.15); 1.6262 (1.84);

1.6090 (1.32); 1.5917 (0.48); 1.3403 (1.18); 1.3309 (2.37); 1.3225 (4.01); 1.3132 (4.03); 1.3043 (2.69); 1.2956 (1.44); 1.2706 (0.71); 1.2614

(0.79); 1.2477 (1.74); 0.8969 (2.16); 0.8795 (6.51); 0.8618 (3.91); 0.8443 (1.16)

›Example 151, Solvent: DMSO, Spectrometer: 399.95 MHz

10.2568 (1.94); 8.1284 (0.84); 8.1089 (1.79); 8.0894 (1.18); 7.9532 (1.46); 7.9072 (1.50); 7.8877 (1.31); 7.8226 (0.43); 7.8016 (1.32); 7.7844

(2.46); 7.7789 (1.82); 7.7618 (0.63); 7.7224 (2.04); 7.7045 (2.68); 7.7009 (1.95); 7.6827 (2.12); 7.6646 (2.48); 7.6613 (1.94); 7.6533 (0.41);

7.5888 (1.38); 7.5700 (1.41); 7.5630 (0.54); 7.5598 (0.47); 7.5498 (0.81); 7.5448 (1.43); 7.5386 (0.70); 7.5305 (1.83); 7.5265 (1.57); 7.5126

(1.12); 7.4958 (2.01); 7.4801 (1.54); 7.4765 (2.51); 7.4631 (0.72); 7.4589 (1.15); 7.4558 (0.79); 7.4437 (1.80); 7.4240 (2.38); 7.4096 (0.72);

7.4055 (1.15); 7.2472 (0.39); 7.2327 (1.41); 7.2243 (8.72); 7.2226 (8.67); 7.2072 (16.00); 7.1951 (2.36); 7.1928 (2.31); 7.1048 (1.03); 7.1010

(1.04); 7.0882 (1.09); 7.0844 (1.03); 6.8776 (2.47); 6.8743 (2.20); 6.8584 (1.24); 6.8007 (0.73); 6.7966 (0.75); 6.7921 (0.63); 6.7797 (0.80);

6.7734 (0.69); 5.5347 (4.39); 5.5234 (0.68); 5.3310 (4.64); 5.3194 (0.69); 4.3017 (1.16); 4.2846 (2.66); 4.2675 (1.36); 3.7328 (12.41); 3.7208

(1.23); 3.3357 (173.12); 3.3243 (22.80); 3.0879 (0.74); 3.0615 (11.06); 3.0496 (1.42); 3.0363 (11.02); 3.0244 (1.26); 2.9232 (1.11); 2.9060

(2.41); 2.8905 (11.62); 2.8787 (1.31); 2.7311 (8.84); 2.7192 (0.91); 2.6720 (0.39); 2.5117 (24.10); 2.5074 (45.12); 2.5028 (58.63); 2.4983

(44.65); 2.4939 (25.55); 2.3297 (0.36); 1.2353 (0.39); −0.0002 (3.12)

›Example 152, Solvent: DMSO, Spectrometer: 400.13 MHz

9.8500 (1.17); 7.7865 (0.75); 7.7690 (0.88); 7.7565 (1.08); 7.7379 (0.50); 7.7277 (1.20); 7.7097 (1.42); 7.7060 (1.09); 7.5572 (0.69); 7.5392

(0.62); 7.5115 (1.08); 7.4923 (1.32); 7.4742 (0.63); 7.4723 (0.63); 7.4608 (0.39); 7.4494 (0.48); 7.4380 (0.45); 7.3483 (0.41); 7.3268 (0.57);

7.0734 (0.64); 7.0712 (0.66); 7.0562 (0.63); 7.0539 (0.62); 5.3333 (2.74); 3.5265 (0.35); 3.5084 (1.15); 3.4902 (1.19); 3.4722 (0.39); 3.3453

(22.18); 3.3219 (0.40); 2.5150 (8.47); 2.5107 (11.39); 2.5064 (8.66); 1.9976 (0.71); 1.4671 (16.00); 1.1820 (0.37); 1.0658 (1.28); 1.0478 (2.81);

1.0296 (1.29)

›Example 153, Solvent: DMSO, Spectrometer: 399.95 MHz

10.6140 (0.42); 10.5013 (1.85); 8.1623 (0.34); 8.1414 (0.40); 8.0435 (1.35); 8.0227 (1.52); 7.9531 (0.49); 7.8376 (1.51); 7.8182 (1.83); 7.7983

(1.11); 7.7252 (2.66); 7.7230 (2.94); 7.7050 (3.90); 7.7013 (2.48); 7.5680 (0.33); 7.5651 (0.59); 7.5620 (0.39); 7.5532 (0.44); 7.5467 (2.08);

7.5411 (0.61); 7.5318 (1.09); 7.5285 (1.74); 7.5252 (0.89); 7.4979 (3.00); 7.4821 (2.09); 7.4786 (3.83); 7.4649 (0.59); 7.4609 (1.45); 7.4578

(0.82); 7.1591 (0.46); 7.1479 (1.80); 7.1299 (1.69); 5.3662 (1.69); 5.3578 (6.59); 5.3316 (0.36); 5.3282 (0.46); 5.3247 (0.42); 5.3136 (0.72);

5.3102 (0.90); 5.3067 (0.70); 5.2956 (0.39); 5.2922 (0.44); 5.2889 (0.33); 3.3428 (149.21); 3.1358 (1.85); 3.1178 (1.81); 3.0690 (0.34); 3.0561

(16.00); 2.8912 (3.85); 2.7321 (3.12); 2.5357 (0.39); 2.5258 (0.83); 2.5126 (14.94); 2.5081 (29.45); 2.5036 (38.64); 2.4990 (28.03); 2.4945

(13.33); 1.7118 (0.83); 1.6998 (6.01); 1.6979 (5.93); 1.6335 (6.78); 1.5716 (0.89); 1.2939 (1.08); 1.0457 (2.97); 1.0288 (2.90); −0.0002 (4.84)

›Example 154, Solvent: DMSO, Spectrometer: 400.13 MHz

11.8962 (1.28); 7.7434 (1.36); 7.7246 (1.52); 7.5551 (0.66); 7.5374 (0.68); 7.5120 (1.16); 7.4928 (1.43); 7.4746 (0.54); 7.2893 (1.70); 5.3425

(2.96); 3.3434 (23.50); 3.0088 (5.43); 2.5109 (19.23); 1.2319 (16.00)

›Example 155, Solvent: DMSO, Spectrometer: 399.95 MHz

12.5650 (1.08); 7.9538 (0.99); 7.7368 (2.77); 7.7329 (1.34); 7.7241 (0.85); 7.7191 (3.52); 7.7153 (2.44); 7.5658 (0.49); 7.5543 (0.36); 7.5474

(1.71); 7.5416 (0.51); 7.5327 (0.96); 7.5293 (1.53); 7.5259 (0.77); 7.5029 (2.58); 7.4995 (1.11); 7.4877 (1.71); 7.4838 (3.20); 7.4703 (0.51);

7.4663 (1.26); 7.4628 (0.74); 7.3463 (4.44); 7.2683 (0.96); 7.2485 (2.03); 7.2276 (1.27); 7.1611 (1.14); 7.1564 (3.43); 7.1530 (4.31); 7.1368

(1.05); 7.1349 (1.09); 7.1327 (0.87); 6.9486 (1.01); 6.9440 (1.17); 6.9403 (0.95); 6.9276 (0.96); 6.9258 (0.97); 6.9215 (0.97); 6.9197 (0.88);

5.3438 (5.92); 5.1215 (0.40); 5.1050 (1.46); 5.0885 (1.47); 5.0721 (0.39); 3.3355 (43.51); 3.0149 (16.00); 2.8911 (7.80); 2.7329 (6.23); 2.7319

(6.31); 2.5263 (0.48); 2.5130 (8.25); 2.5085 (16.33); 2.5039 (21.44); 2.4993 (15.57); 2.4948 (7.44); 1.5457 (5.67); 1.5292 (5.62); −0.0002 (3.37)

›Example 156, Solvent: DMSO, Spectrometer: 399.95 MHz

10.2194 (2.13); 8.0945 (1.45); 8.0744 (1.77); 7.8905 (1.26); 7.8711 (1.77); 7.8510 (1.13); 7.7273 (1.91); 7.7246 (2.59); 7.7208 (1.24); 7.7119

(0.80); 7.7069 (3.44); 7.7031 (2.36); 7.5659 (0.49); 7.5539 (0.37); 7.5476 (1.62); 7.5419 (0.48); 7.5326 (0.86); 7.5293 (1.41); 7.5259 (0.72);

7.4971 (2.37); 7.4936 (1.01); 7.4816 (1.63); 7.4779 (3.06); 7.4643 (0.48); 7.4602 (1.23); 7.4571 (0.70); 7.3823 (0.60); 7.3674 (7.84); 7.3618

(3.51); 7.3530 (2.93); 7.3513 (3.54); 7.3458 (0.67); 7.3369 (0.52); 7.3336 (0.70); 7.3314 (0.82); 7.3117 (0.67); 7.3058 (0.87); 7.2985 (0.72);

7.2899 (0.82); 7.2803 (0.38); 7.2750 (0.33); 7.2003 (1.75); 7.1828 (1.68); 5.3733 (6.02); 4.5879 (1.41); 4.5586 (2.66); 4.4973 (2.65); 4.4680

(1.48); 4.2677 (0.40); 4.2512 (1.53); 4.2345 (1.55); 4.2179 (0.42); 3.3374 (102.65); 3.0625 (16.00); 2.8906 (1.22); 2.7321 (0.92); 2.7311 (0.96);

2.5255 (0.57); 2.5208 (0.91); 2.5122 (11.80); 2.5077 (23.81); 2.5031 (31.59); 2.4984 (23.00); 2.4939 (11.00); 1.3643 (5.95); 1.3476

(5.91); −0.0002 (1.54)

›Example 157, Solvent: DMSO, Spectrometer: 400.13 MHz

7.8410 (0.48); 7.8218 (0.77); 7.8019 (0.57); 7.6923 (0.55); 7.6851 (3.99); 7.6802 (1.34); 7.6677 (1.45); 7.6628 (4.40); 7.6554 (0.54); 7.0545

(0.53); 7.0471 (4.16); 7.0422 (1.32); 7.0296 (1.29); 7.0248 (3.89); 7.0172 (0.46); 6.8597 (1.73); 6.8415 (1.42); 5.2972 (5.30); 3.8208 (16.00);

3.7716 (0.47); 3.6367 (0.75); 3.6188 (0.71); 3.0550 (0.56); 3.0434 (15.06); 2.5183 (7.32); 2.5142 (15.39); 2.5098 (21.16); 2.5054 (15.45);

1.2602 (0.34); 1.2444 (0.39)

›Example 158, Solvent: DMSO, Spectrometer: 399.95 MHz

12.6738 (2.31); 7.9545 (3.14); 7.9353 (1.86); 7.7430 (1.97); 7.7404 (2.69); 7.7364 (1.29); 7.7279 (0.80); 7.7227 (3.49); 7.7189 (2.40); 7.5644

(0.47); 7.5530 (0.35); 7.5460 (1.68); 7.5401 (0.54); 7.5312 (1.33); 7.5280 (1.73); 7.5244 (1.06); 7.5183 (3.77); 7.5115 (2.42); 7.5029 (4.15); 7.4879

(1.66); 7.4839 (3.45); 7.4706 (0.52); 7.4664 (1.26); 7.4628 (0.71); 7.3942 (3.61); 7.2815 (0.90); 7.2743 (0.90); 7.2661 (0.77); 7.2617 (0.93); 7.2588

(0.88); 7.2548 (0.88); 7.2459 (0.73); 7.2389 (0.73); 5.3636 (5.71); 3.3280 (66.85); 3.0512 (16.00); 2.8901 (13.73); 2.7310 (10.63); 2.7305 (10.71);

2.5242 (0.78); 2.5193 (1.22); 2.5108 (14.68); 2.5063 (29.26); 2.5017 (38.58); 2.4971 (27.93); 2.4926 (13.22); 0.0079 (0.34); −0.0002 (9.89)

›Example 159, Solvent: DMSO, Spectrometer: 399.95 MHz

12.4204 (0.90); 7.7407 (3.17); 7.7229 (3.69); 7.7193 (2.84); 7.6158 (1.59); 7.6119 (1.72); 7.5961 (1.73); 7.5922 (1.77); 7.5674 (0.52); 7.5559

(0.38); 7.5488 (1.87); 7.5434 (0.59); 7.5311 (1.65); 7.5058 (2.97); 7.4864 (3.56); 7.4691 (1.29); 7.4660 (0.85); 7.3402 (5.55); 7.3197 (1.49);

7.3023 (0.98); 7.2985 (0.96); 7.0249 (1.83); 7.0066 (1.50); 7.0041 (1.59); 6.9432 (0.97); 6.9403 (1.00); 6.9238 (1.69); 6.9214 (1.65); 6.9051

(0.86); 6.9021 (0.84); 5.3429 (6.98); 4.9715 (7.89); 3.3432 (128.35); 3.0349 (16.00); 3.0233 (1.12); 2.5075 (28.50); 2.5030 (37.51); 2.4986

(28.09); 2.4944 (14.15); 2.2229 (0.46); −0.0002 (1.60)

›Example 160, Solvent: DMSO, Spectrometer: 399.95 MHz

11.8369 (1.56); 7.7378 (1.60); 7.7349 (2.16); 7.7309 (1.01); 7.7226 (0.64); 7.7173 (2.88); 7.7136 (1.93); 7.5647 (0.40); 7.5465 (1.37); 7.5405

(0.40); 7.5317 (0.76); 7.5283 (1.26); 7.5247 (0.61); 7.5019 (2.03); 7.4985 (0.83); 7.4870 (1.30); 7.4830 (2.50); 7.4696 (0.39); 7.4655 (1.03);

7.4619 (0.54); 7.2695 (3.52); 5.3364 (4.71); 3.3293 (35.22); 2.9884 (13.82); 2.8909 (1.97); 2.7324 (1.59); 2.7311 (1.56); 2.5253 (0.45); 2.5206

(0.70); 2.5120 (9.18); 2.5074 (18.49); 2.5028 (24.47); 2.4981 (17.64); 2.4936 (8.27); 1.6349 (0.85); 1.6150 (0.75); 1.6052 (0.61); 1.5935 (1.00);

1.2519 (0.49); 1.2336 (1.26); 1.2150 (1.41); 1.1966 (1.13); 1.1830 (16.00); 1.1212 (0.34); 1.1095 (0.42); 1.1017 (0.70); 1.0936 (0.58); 1.0831

(0.72); 1.0742 (0.56); 1.0664 (0.41); 1.0608 (0.46); 0.8419 (2.99); 0.8239 (6.18); 0.8055 (2.43); −0.0002 (8.03)

›Example 161, Solvent: CDCl3, Spectrometer: 300.16 MHz

7.9406 (2.10); 7.9128 (2.66); 7.7328 (1.48); 7.7061 (2.57); 7.6756 (2.97); 7.6512 (2.98); 7.6464 (3.09); 7.6288 (2.56); 7.3615 (2.79); 7.2652

(6.26); 7.1386 (2.32); 7.1116 (4.45); 7.0842 (2.21); 7.0246 (2.66); 7.0000 (2.47); 5.2881 (10.14); 4.2019 (2.57); 4.1799 (5.23); 4.1577 (2.69);

3.1032 (16.00); 2.0111 (5.35); 1.7072 (1.74); 1.6858 (2.72); 1.6644 (2.07); 1.6327 (10.56); 1.3657 (5.67); 1.3562 (5.80); 1.2538 (0.45); 0.9358

(2.93); 0.9175 (6.36); −0.0002 (2.29)

›Example 162, Solvent: DMSO, Spectrometer: 400.13 MHz

10.7979 (1.40); 7.8362 (1.62); 7.8338 (1.77); 7.8180 (1.00); 7.7270 (1.29); 7.7141 (0.41); 7.7092 (1.65); 7.7055 (1.18); 7.5504 (0.79); 7.5354

(0.43); 7.5322 (0.68); 7.5289 (0.37); 7.5008 (1.19); 7.4853 (0.83); 7.4816 (1.51); 7.4639 (0.65); 7.4608 (0.41); 7.1546 (0.64); 7.1497 (0.61);

7.1387 (0.63); 7.1338 (0.62); 5.7666 (2.26); 5.3476 (3.10); 3.3401 (13.01); 3.0584 (7.68); 2.5301 (0.33); 2.5165 (7.09); 2.5122 (14.63); 2.5077

(19.78); 2.5032 (14.18); 2.4989 (6.70); 2.4701 (0.32); 1.4799 (16.00); 1.4489 (0.54)

›Example 163, Solvent: DMSO, Spectrometer: 400.13 MHz

7.7383 (2.71); 7.7257 (0.99); 7.7206 (3.40); 7.7168 (2.51); 7.5614 (0.51); 7.5582 (0.38); 7.5499 (0.42); 7.5431 (1.67); 7.5373 (0.61); 7.5283

(1.02); 7.5250 (1.54); 7.5216 (0.88); 7.4989 (2.58); 7.4836 (1.78); 7.4798 (3.19); 7.4664 (0.64); 7.4623 (1.28); 7.4589 (0.81); 7.3854 (1.22);

7.3673 (1.53); 7.3646 (1.53); 7.3466 (1.35); 6.5468 (0.66); 6.5332 (1.27); 6.5195 (0.71); 6.4895 (1.95); 6.4719 (1.90); 6.4059 (1.90); 6.3852

(1.87); 5.7595 (1.92); 5.2000 (6.69); 3.3207 (26.40); 3.2065 (0.92); 3.1892 (1.85); 3.1747 (1.86); 3.1575 (0.98); 3.0772 (16.00); 3.0516 (0.47);

2.5157 (7.56); 2.5113 (14.94); 2.5068 (20.08); 2.5023 (14.74); 2.4980 (7.57); 1.5122 (0.93); 1.4943 (1.51); 1.4769 (1.25); 1.4582 (0.55); 1.3430

(0.33); 1.3252 (0.87); 1.3042 (1.36); 1.2973 (1.36); 1.2867 (1.80); 1.2827 (1.83); 1.2711 (2.95); 1.2650 (4.03); 1.2586 (2.86); 0.8750 (1.85);

0.8582 (5.67); 0.8408 (2.18)

›Example 164, Solvent: DMSO, Spectrometer: 399.95 MHz

12.4389 (1.06); 7.9528 (1.21); 7.7388 (2.70); 7.7348 (1.29); 7.7262 (0.79); 7.7211 (3.47); 7.7172 (2.40); 7.5668 (0.48); 7.5554 (0.35); 7.5484

(1.69); 7.5425 (0.50); 7.5337 (0.93); 7.5303 (1.51); 7.5269 (0.76); 7.5047 (2.54); 7.5014 (1.08); 7.4896 (1.62); 7.4857 (3.14); 7.4723 (0.48);

7.4681 (1.23); 7.4646 (0.68); 7.3645 (0.37); 7.3555 (4.27); 7.3499 (1.34); 7.3384 (5.86); 7.3329 (4.92); 7.3240 (0.44); 7.0133 (0.44); 7.0044

(4.67); 6.9987 (1.31); 6.9874 (1.24); 6.9818 (4.12); 6.9728 (0.33); 5.3422 (5.94); 4.8586 (7.30); 3.3327 (63.87); 3.0226 (16.00); 2.8904 (9.87);

2.7317 (7.82); 2.7309 (7.72); 2.5249 (0.72); 2.5201 (1.13); 2.5116 (13.74); 2.5071 (27.47); 2.5025 (36.24); 2.4979 (26.26); 2.4934 (12.45); −0.0002

(3.18)

›Example 165, Solvent: DMSO, Spectrometer: 399.95 MHz

8.2664 (2.30); 8.0307 (1.57); 8.0107 (1.97); 7.9530 (0.67); 7.8574 (1.31); 7.8380 (1.80); 7.8179 (1.14); 7.6823 (2.54); 7.6785 (1.23); 7.6696

(0.77); 7.6645 (3.45); 7.6608 (2.39); 7.5610 (0.50); 7.5488 (0.38); 7.5426 (1.63); 7.5371 (0.50); 7.5247 (2.61); 7.5214 (2.96); 7.5165 (0.73);

7.5043 (3.21); 7.5015 (2.76); 7.4945 (0.67); 7.4889 (2.41); 7.4854 (1.00); 7.4732 (1.70); 7.4696 (3.11); 7.4518 (2.07); 7.4501 (2.19); 7.4324

(3.32); 7.4284 (1.43); 7.4170 (0.90); 7.4135 (1.79); 7.3907 (0.78); 7.3871 (1.42); 7.3836 (0.77); 7.3753 (0.51); 7.3690 (1.60); 7.3624 (0.32);

7.3510 (0.47); 7.1435 (1.78); 7.1257 (1.70); 5.2672 (6.28); 3.3380 (136.98); 2.9697 (16.00); 2.8908 (5.49); 2.7313 (4.41); 2.5256 (0.64); 2.5208

(1.02); 2.5122 (13.67); 2.5077 (27.43); 2.5031 (36.24); 2.4985 (26.25); 2.4940 (12.46); 1.5356 (1.14); 1.5253 (3.03); 1.5180 (3.27); 1.5084

(1.26); 1.1924 (1.32); 1.1826 (3.22); 1.1753 (3.11); 1.1648 (1.11); −0.0002 (4.98)

›Example 166, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5501 (2.03); 8.0599 (1.22); 8.0393 (1.45); 7.9534 (0.44); 7.8305 (1.29); 7.8112 (1.76); 7.7910 (1.16); 7.7266 (2.05); 7.7241 (2.63); 7.7202

(1.31); 7.7114 (0.89); 7.7063 (3.47); 7.7025 (2.39); 7.5647 (0.49); 7.5615 (0.32); 7.5528 (0.38); 7.5464 (1.65); 7.5407 (0.50); 7.5315 (0.93);

7.5281 (1.43); 7.5247 (0.74); 7.4971 (2.42); 7.4938 (1.06); 7.4817 (1.73); 7.4780 (3.09); 7.4644 (0.51); 7.4603 (1.25); 7.4571 (0.72); 7.1395

(1.79); 7.1220 (1.72); 5.3563 (6.32); 3.3289 (56.12); 3.0729 (0.34); 3.0531 (16.00); 2.8908 (3.54); 2.7321 (2.78); 2.7311 (2.79); 2.5252 (0.66);

2.5119 (11.40); 2.5074 (22.31); 2.5028 (29.21); 2.4982 (21.28); 2.4937 (10.21); 2.4667 (1.73); 2.4507 (1.38); 2.4472 (1.93); 2.4426 (1.27);

2.4273 (1.81); 1.5443 (1.77); 1.5289 (1.28); 1.5243 (1.88); 1.5049 (1.63); 1.0161 (12.01); 0.3017 (0.81); 0.2870 (3.12); 0.2784 (1.31); 0.2105

(1.59); 0.2019 (3.43); 0.1979 (2.76); 0.1869 (0.94); −0.0002 (7.31)

›Example 167, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5191 (2.06); 8.0722 (1.29); 8.0515 (1.54); 7.8334 (1.30); 7.8141 (1.82); 7.7938 (1.19); 7.7237 (2.64); 7.7199 (1.26); 7.7110 (0.85); 7.7059

(3.48); 7.7022 (2.41); 7.5646 (0.49); 7.5527 (0.37); 7.5463 (1.67); 7.5406 (0.49); 7.5313 (0.92); 7.5280 (1.44); 7.5246 (0.73); 7.4970 (2.44);

7.4936 (1.04); 7.4815 (1.70); 7.4778 (3.15); 7.4643 (0.50); 7.4602 (1.25); 7.4570 (0.73); 7.1424 (1.83); 7.1241 (1.78); 5.8288 (0.61); 5.8200

(0.32); 5.8032 (0.93); 5.7861 (0.96); 5.7771 (0.36); 5.7693 (0.36); 5.7605 (0.72); 5.7438 (0.35); 5.3547 (6.44); 5.0386 (0.46); 5.0347 (1.07);

5.0294 (1.17); 5.0255 (0.52); 4.9957 (0.42); 4.9918 (0.97); 4.9865 (1.05); 4.9825 (0.47); 4.9614 (0.58); 4.9587 (1.12); 4.9559 (0.99); 4.9533

(0.96); 4.9504 (0.47); 4.9360 (0.56); 4.9332 (1.06); 4.9305 (0.94); 4.9278 (0.90); 4.9249 (0.44); 3.3316 (55.34); 3.0536 (16.00); 2.5255 (0.49);

2.5122 (10.21); 2.5077 (20.28); 2.5031 (26.66); 2.4985 (19.39); 2.4940 (9.34); 2.4075 (1.65); 2.3892 (3.19); 2.3707 (1.80); 2.0637 (0.63);

2.0459 (1.61); 2.0278 (1.67); 2.0101 (0.71); 1.6166 (0.38); 1.5984 (1.10); 1.5796 (1.50); 1.5606 (1.21); 1.5416 (0.52); 1.4055 (0.53); 1.3860

(1.32); 1.3740 (0.71); 1.3678 (1.66); 1.3485 (1.02); 1.3303 (0.34); −0.0002 (6.33)

›Example 168, Solvent: DMSO, Spectrometer: 400.13 MHz

10.3988 (3.23); 7.8325 (2.66); 7.8280 (2.70); 7.8199 (5.62); 7.8070 (0.37); 7.7283 (2.85); 7.7104 (3.50); 7.7067 (2.57); 7.5678 (0.49); 7.5556

(0.39); 7.5494 (1.74); 7.5440 (0.55); 7.5343 (0.95); 7.5313 (1.46); 7.5001 (2.59); 7.4808 (3.30); 7.4670 (0.58); 7.4631 (1.27); 7.4434 (0.94);

7.4387 (1.38); 7.4221 (3.80); 7.4186 (3.57); 7.4155 (3.08); 7.4131 (3.06); 7.4077 (0.72); 7.3956 (3.66); 7.3913 (1.23); 7.3766 (1.50); 7.3598

(0.81); 7.3554 (1.28); 7.3507 (0.64); 7.3455 (0.54); 7.3383 (1.27); 7.3213 (0.41); 7.1244 (1.33); 7.1162 (1.38); 7.1119 (1.20); 7.1036 (1.28);

5.3428 (7.01); 5.1856 (7.82); 3.4027 (0.64); 3.4003 (0.81); 3.3515 (109.79); 3.3027 (0.64); 3.2998 (0.47); 3.0703 (16.00); 2.5586 (0.43); 2.5319

(0.81); 2.5182 (17.55); 2.5141 (35.67); 2.5097 (48.03); 2.5054 (34.89); 2.4613 (0.41); 2.4576 (0.36); 1.9966 (0.63); 1.2515 (0.57); 1.1808 (0.33);

0.8643 (0.76)

›Example 169, Solvent: DMSO, Spectrometer: 400.13 MHz

12.1300 (1.69); 7.6226 (3.42); 7.6020 (3.93); 7.3078 (3.21); 7.2876 (2.83); 7.2488 (4.77); 5.2968 (6.30); 3.4115 (4.99); 3.3986 (0.39); 3.3615

(311.04); 3.3119 (1.57); 3.2615 (0.34); 2.9987 (16.00); 2.5622 (0.56); 2.5577 (0.71); 2.5533 (0.52); 2.5301 (0.86); 2.5164 (17.19); 2.5122

(34.56); 2.5078 (46.09); 2.5033 (33.23); 2.4992 (15.91); 2.4585 (0.33); 2.4287 (2.01); 2.4104 (3.66); 2.3916 (2.19); 2.3530 (9.91); 2.3347 (0.47);

2.3301 (0.34); 1.9936 (0.47); 1.6039 (0.49); 1.5856 (1.45); 1.5669 (2.00); 1.5483 (1.52); 1.5294 (0.60); 1.3376 (0.32); 1.3191 (1.18); 1.3002

(1.99); 1.2815 (2.12); 1.2632 (1.48); 1.2453 (1.39); 0.8946 (4.19); 0.8763 (8.85); 0.8609 (2.45); 0.8580 (3.91); 0.8438 (0.71)

›Example 170, Solvent: DMSO, Spectrometer: 399.95 MHz

9.8542 (2.06); 8.0824 (1.56); 8.0624 (1.96); 7.9536 (0.38); 7.9015 (1.29); 7.8821 (1.84); 7.8620 (1.14); 7.7978 (2.41); 7.7937 (2.42); 7.7383

(1.95); 7.7359 (2.53); 7.7320 (1.25); 7.7232 (0.83); 7.7181 (3.37); 7.7143 (2.36); 7.5659 (0.48); 7.5541 (0.36); 7.5476 (1.64); 7.5418 (0.50);

7.5327 (0.90); 7.5293 (1.44); 7.5259 (0.75); 7.4993 (2.41); 7.4959 (1.08); 7.4840 (1.62); 7.4801 (3.09); 7.4666 (0.49); 7.4625 (1.23); 7.4592

(0.70); 7.2092 (1.76); 7.1914 (1.71); 6.6034 (2.47); 6.5995 (2.48); 5.3974 (6.35); 3.3312 (63.44); 3.0917 (16.00); 2.8911 (3.05); 2.7324 (2.43);

2.7314 (2.38); 2.5254 (0.60); 2.5206 (0.94); 2.5121 (11.56); 2.5076 (23.08); 2.5030 (30.37); 2.4984 (22.06); 2.4939 (10.54); 2.3490 (12.91);

2.2917 (0.43); 1.2864 (0.50); 0.8757 (0.49); −0.0002 (7.45)

›Example 171, Solvent: DMSO, Spectrometer: 399.95 MHz

12.3285 (0.78); 7.9532 (0.64); 7.7436 (1.99); 7.7411 (2.68); 7.7371 (1.32); 7.7286 (0.79); 7.7235 (3.42); 7.7196 (2.40); 7.5665 (0.48); 7.5551

(0.34); 7.5481 (1.69); 7.5422 (0.50); 7.5335 (0.93); 7.5301 (1.53); 7.5266 (0.77); 7.5049 (2.55); 7.5016 (1.09); 7.4898 (1.60); 7.4858 (3.10);

7.4725 (0.48); 7.4683 (1.22); 7.4648 (0.68); 7.3320 (4.62); 7.0182 (0.93); 7.0143 (1.00); 6.9981 (1.90); 6.9943 (1.82); 6.9657 (0.88); 6.9613

(0.98); 6.9480 (1.19); 6.9437 (1.46); 6.9264 (1.19); 6.9235 (1.48); 6.9061 (2.27); 6.9019 (1.50); 6.8777 (1.37); 6.8737 (1.33); 6.8599 (1.04);

6.8564 (1.15); 6.8537 (0.76); 6.8399 (0.48); 6.8359 (0.48); 5.3424 (5.87); 4.8205 (7.49); 3.7826 (16.00); 3.3351 (33.96); 3.0278 (15.32); 3.0143

(0.35); 2.8899 (5.11); 2.7319 (4.05); 2.7310 (4.09); 2.5253 (0.33); 2.5205 (0.52); 2.5120 (6.64); 2.5075 (13.33); 2.5029 (17.62); 2.4983 (12.81);

2.4938 (6.12); −0.0002 (3.49)

›Example 172, Solvent: DMSO, Spectrometer: 400.13 MHz

10.5339 (4.60); 8.1018 (3.12); 8.0812 (3.70); 7.8447 (2.73); 7.8254 (3.85); 7.8052 (2.65); 7.7302 (5.81); 7.7175 (2.02); 7.7124 (7.41); 7.7087

(5.49); 7.6920 (0.36); 7.5781 (1.04); 7.5750 (0.78); 7.5664 (0.88); 7.5597 (3.57); 7.5541 (1.30); 7.5449 (2.12); 7.5416 (3.23); 7.5383 (1.88);

7.5128 (5.44); 7.4974 (3.73); 7.4937 (6.78); 7.4802 (1.29); 7.4761 (2.70); 7.4729 (1.68); 7.1465 (3.95); 7.1288 (3.77); 5.3725 (13.34); 5.3456

(0.42); 3.5039 (1.80); 3.4858 (5.88); 3.4676 (6.08); 3.4494 (1.97); 3.3912 (0.65); 3.3409 (43.04); 3.2907 (0.61); 2.7173 (0.66); 2.6973 (1.20);

2.6836 (1.59); 2.6798 (1.72); 2.6665 (0.88); 2.5696 (0.40); 2.5652 (0.88); 2.5608 (1.23); 2.5562 (0.91); 2.5516 (0.50); 2.5328 (1.90); 2.5193

(33.14); 2.5150 (69.27); 2.5105 (95.86); 2.5060 (71.93); 2.5016 (37.19); 2.4697 (1.83); 2.4650 (1.90); 2.4605 (1.93); 2.4559 (1.48); 2.3420

(0.50); 2.3374 (0.65); 2.3329 (0.49); 1.6154 (0.48); 1.6040 (0.62); 1.5956 (1.03); 1.5916 (0.90); 1.5815 (1.09); 1.5751 (1.27); 1.5699 (0.96);

1.5603 (1.26); 1.5394 (0.55); 1.3744 (0.48); 1.3451 (0.43); 1.3314 (0.93); 1.3193 (1.27); 1.3133 (0.94); 1.3063 (1.87); 1.2930 (2.04); 1.2870

(2.27); 1.2724 (3.51); 1.2619 (2.10); 1.2537 (3.00); 1.2384 (3.01); 1.2255 (1.23); 1.2207 (1.30); 1.2136 (0.94); 1.1807 (0.33); 1.1033 (0.37);

1.0903 (0.42); 1.0700 (13.27); 1.0582 (9.12); 1.0530 (15.18); 1.0403 (16.00); 1.0220 (7.07); 0.9902 (0.47); 0.8832 (6.32); 0.8653 (12.63);

0.8474 (5.25); 0.8151 (0.38)

›Example 173, Solvent: DMSO, Spectrometer: 399.95 MHz

10.4268 (0.85); 8.0973 (0.65); 8.0770 (0.77); 7.8320 (0.59); 7.8127 (0.78); 7.7924 (0.55); 7.7253 (0.86); 7.7226 (1.15); 7.7186 (0.54); 7.7100

(0.33); 7.7048 (1.57); 7.7011 (1.07); 7.5453 (0.75); 7.5303 (0.39); 7.5270 (0.66); 7.5235 (0.32); 7.4953 (1.08); 7.4918 (0.44); 7.4800 (0.73);

7.4762 (1.40); 7.4585 (0.58); 7.1465 (0.78); 7.1452 (0.79); 7.1280 (0.76); 7.1266 (0.73); 5.3564 (2.81); 3.3292 (22.20); 3.0495 (7.72); 2.8909

(2.42); 2.7323 (1.92); 2.7311 (1.89); 2.5206 (0.38); 2.5120 (5.12); 2.5075 (10.41); 2.5028 (13.85); 2.4982 (10.00); 2.4936 (4.73); 2.2811 (3.18);

1.0017 (16.00); −0.0002 (0.61)

›Example 174, Solvent: DMSO, Spectrometer: 399.95 MHz

11.0174 (0.49); 10.9652 (2.77); 8.3621 (0.52); 8.3585 (0.37); 8.1522 (1.93); 8.1315 (2.48); 8.1187 (0.63); 7.9520 (1.28); 7.9233 (1.46); 7.9025

(5.11); 7.8812 (5.99); 7.8682 (1.35); 7.7992 (4.69); 7.7947 (2.16); 7.7826 (1.87); 7.7780 (3.76); 7.7644 (0.81); 7.7328 (3.18); 7.7150 (4.28);

7.7114 (3.40); 7.5664 (0.57); 7.5545 (0.53); 7.5480 (2.03); 7.5425 (0.92); 7.5299 (1.94); 7.4997 (2.99); 7.4804 (4.14); 7.4668 (1.49); 7.4629

(1.94); 7.3170 (0.51); 7.2339 (2.11); 7.2155 (2.23); 7.2036 (0.54); 5.4129 (7.30); 5.4004 (2.02); 3.3336 (259.50); 3.3254 (85.59); 3.2568 (0.38);

3.0748 (16.00); 3.0613 (3.35); 2.8906 (8.49); 2.8772 (1.53); 2.7508 (0.32); 2.7311 (7.17); 2.7175 (1.42); 2.6760 (0.42); 2.6715 (0.61); 2.6669

(0.52); 2.5244 (1.68); 2.5111 (31.96); 2.5068 (67.85); 2.5023 (96.64); 2.4978 (83.97); 2.4934 (59.44); 2.3335 (0.48); 2.3291 (0.67); 2.3245

(0.59); 1.2341 (0.71); 0.0080 (0.55); −0.0002 (16.64); −0.0084 (2.01); −0.0139 (2.74)

›Example 175, Solvent: DMSO, Spectrometer: 399.95 MHz

10.1866 (2.65); 7.9531 (0.97); 7.8234 (0.52); 7.8024 (1.91); 7.7867 (3.90); 7.7836 (2.80); 7.7670 (0.56); 7.7226 (2.65); 7.7188 (1.31); 7.7098

(0.80); 7.7048 (3.41); 7.7010 (2.41); 7.5633 (0.48); 7.5515 (0.36); 7.5449 (1.65); 7.5393 (0.49); 7.5300 (0.88); 7.5267 (1.43); 7.5234 (0.75);

7.4963 (2.45); 7.4809 (1.66); 7.4771 (3.12); 7.4635 (0.49); 7.4595 (1.22); 7.4563 (0.70); 7.2432 (0.55); 7.2390 (0.75); 7.2192 (3.18); 7.2006

(2.92); 7.1029 (1.35); 7.0982 (1.36); 7.0869 (1.23); 7.0822 (1.30); 6.9777 (1.59); 6.9580 (1.43); 6.9009 (0.95); 6.8985 (0.93); 6.8824 (1.72);

6.8802 (1.57); 6.8640 (0.79); 6.8616 (0.75); 5.3288 (6.32); 4.2549 (1.61); 4.2373 (3.54); 4.2196 (1.69); 3.7772 (16.00); 3.3389 (97.25); 3.0633

(15.72); 2.9347 (1.51); 2.9171 (3.04); 2.8995 (1.52); 2.8906 (7.73); 2.7322 (6.02); 2.7313 (6.13); 2.5256 (0.56); 2.5122 (11.48); 2.5077 (22.92);

2.5031 (30.26); 2.4985 (22.17); 2.4940 (10.74); −0.0002 (2.39)

›Example 176, Solvent: DMSO, Spectrometer: 400.13 MHz

10.5325 (4.18); 8.0778 (2.47); 8.0571 (2.95); 7.8416 (2.45); 7.8222 (3.52); 7.8021 (2.27); 7.7285 (5.15); 7.7157 (1.61); 7.7108 (6.55); 7.7070

(4.71); 7.5773 (0.91); 7.5741 (0.62); 7.5654 (0.75); 7.5589 (3.16); 7.5532 (1.01); 7.5440 (1.83); 7.5407 (2.80); 7.5375 (1.51); 7.5121 (4.79);

7.4967 (3.19); 7.4930 (5.96); 7.4794 (0.96); 7.4754 (2.26); 7.4721 (1.34); 7.1384 (3.59); 7.1205 (3.43); 5.3672 (12.41); 3.5051 (1.58); 3.4870

(5.34); 3.4688 (5.44); 3.4507 (1.66); 3.3929 (0.46); 3.3429 (38.50); 3.2931 (0.40); 2.6832 (0.41); 2.6787 (0.55); 2.6742 (0.40); 2.5641 (0.83);

2.5597 (1.13); 2.5553 (0.83); 2.5321 (1.45); 2.5185 (33.63); 2.5142 (70.52); 2.5097 (96.23); 2.5052 (69.78); 2.5009 (33.26); 2.4688 (0.65);

2.4644 (0.94); 2.4599 (1.16); 2.4554 (0.91); 2.4056 (3.54); 2.3873 (6.46); 2.3686 (3.85); 2.3410 (0.52); 2.3366 (0.71); 2.3321 (0.52); 1.5944

(0.88); 1.5762 (2.64); 1.5575 (3.67); 1.5391 (2.77); 1.5201 (1.13); 1.3728 (0.33); 1.3474 (0.61); 1.3288 (2.14); 1.3099 (3.42); 1.2911 (3.47);

1.2729 (2.15); 1.2548 (0.78); 1.2408 (0.39); 1.0603 (6.03); 1.0423 (13.70); 1.0240 (5.88); 0.9037 (7.83); 0.8854 (16.00); 0.8670 (6.78); 0.8512

(0.34)

›Example 177, Solvent: DMSO, Spectrometer: 399.95 MHz

10.4940 (1.73); 8.0791 (1.46); 8.0588 (1.73); 7.8363 (1.30); 7.8170 (1.73); 7.7968 (1.18); 7.7266 (1.92); 7.7243 (2.52); 7.7204 (1.19); 7.7116

(0.75); 7.7065 (3.35); 7.7026 (2.29); 7.5652 (0.48); 7.5533 (0.35); 7.5468 (1.62); 7.5411 (0.46); 7.5319 (0.85); 7.5286 (1.39); 7.5252 (0.69);

7.4978 (2.35); 7.4944 (0.97); 7.4825 (1.58); 7.4787 (3.02); 7.4651 (0.46); 7.4611 (1.20); 7.4578 (0.65); 7.1433 (1.74); 7.1257 (1.68); 5.3595

(6.26); 3.3326 (58.89); 3.0590 (16.00); 2.8910 (1.13); 2.7735 (0.82); 2.7564 (1.15); 2.7393 (0.88); 2.7322 (0.95); 2.7223 (0.33); 2.5257 (0.50);

2.5208 (0.83); 2.5123 (9.61); 2.5078 (19.11); 2.5032 (25.17); 2.4986 (18.15); 2.4940 (8.58); 1.0854 (13.94); 1.0684 (13.71); 1.0488 (0.41); −0.0002

(0.91)

›Example 178, Solvent: DMSO, Spectrometer: 399.95 MHz

11.1105 (2.12); 8.1675 (0.51); 8.1474 (0.58); 7.9532 (0.83); 7.9310 (1.18); 7.9115 (1.71); 7.8914 (1.06); 7.7368 (0.39); 7.7312 (2.06); 7.7284

(2.75); 7.7246 (1.48); 7.7159 (0.85); 7.7108 (3.55); 7.7070 (2.57); 7.5710 (1.12); 7.5671 (1.41); 7.5609 (0.50); 7.5524 (1.88); 7.5458 (2.62);

7.5406 (1.50); 7.5309 (1.41); 7.5274 (2.18); 7.5241 (2.81); 7.5212 (2.24); 7.5057 (1.23); 7.5014 (1.68); 7.4967 (2.69); 7.4933 (1.30); 7.4877

(1.92); 7.4816 (2.44); 7.4776 (3.38); 7.4678 (1.11); 7.4635 (1.23); 7.4599 (1.43); 7.4567 (0.80); 7.4411 (1.38); 7.4374 (1.30); 7.4227 (1.64);

7.4191 (1.67); 7.4044 (0.68); 7.4008 (0.62); 7.2419 (1.69); 7.2234 (1.60); 5.3769 (4.33); 3.3314 (18.88); 3.0797 (16.00); 3.0662 (0.84); 3.0592

(0.39); 2.8902 (6.68); 2.7320 (5.26); 2.7308 (5.21); 2.5251 (0.50); 2.5203 (0.77); 2.5117 (9.24); 2.5072 (18.61); 2.5026 (24.66); 2.4980 (17.91);

2.4934 (8.52); 1.2347 (0.46); 0.9274 (0.36); 0.9106 (0.36); −0.0002 (6.89)

›Example 179, Solvent: DMSO, Spectrometer: 399.95 MHz

10.8683 (2.02); 8.0121 (1.14); 7.9916 (1.50); 7.9531 (0.80); 7.8734 (1.31); 7.8542 (1.74); 7.8339 (1.11); 7.7296 (1.95); 7.7271 (2.56); 7.7232

(1.23); 7.7144 (0.76); 7.7093 (3.42); 7.7055 (2.38); 7.5673 (0.49); 7.5554 (0.35); 7.5491 (1.64); 7.5434 (0.48); 7.5340 (0.85); 7.5307 (1.42);

7.5273 (0.72); 7.4982 (2.36); 7.4947 (0.99); 7.4827 (1.68); 7.4790 (3.08); 7.4653 (0.49); 7.4613 (1.27); 7.4581 (0.70); 7.2691 (0.77); 7.2488

(1.95); 7.2318 (0.43); 7.2276 (1.43); 7.2089 (1.74); 7.1914 (1.68); 7.1453 (3.72); 7.1413 (4.09); 7.1375 (1.20); 7.1265 (1.03); 7.1245 (1.07);

7.1223 (0.79); 7.1201 (0.60); 6.9514 (0.95); 6.9471 (1.32); 6.9429 (0.89); 6.9303 (0.89); 6.9283 (0.88); 6.9242 (0.89); 6.9223 (0.79); 5.3899

(5.81); 5.1185 (0.97); 5.1021 (0.98); 3.3336 (96.07); 3.0642 (16.00); 2.8909 (6.73); 2.7324 (5.27); 2.7313 (5.16); 2.5257 (0.66); 2.5209 (1.02);

2.5123 (13.79); 2.5077 (27.87); 2.5031 (36.97); 2.4985 (26.80); 2.4940 (12.70); 1.5333 (5.24); 1.5169 (5.22); −0.0002 (3.65)

›Example 180, Solvent: DMSO, Spectrometer: 399.95 MHz

12.6387 (1.10); 8.0024 (3.31); 7.9817 (3.46); 7.9534 (1.30); 7.7464 (2.73); 7.7424 (1.31); 7.7339 (0.75); 7.7288 (3.40); 7.7249 (2.36); 7.5674

(0.46); 7.5561 (0.33); 7.5490 (1.67); 7.5431 (0.50); 7.5345 (0.92); 7.5310 (1.54); 7.5275 (0.78); 7.5068 (2.57); 7.5035 (1.10); 7.4918 (1.57);

7.4878 (3.11); 7.4745 (0.47); 7.4703 (1.22); 7.4667 (0.72); 7.3618 (4.47); 7.3566 (2.93); 7.3363 (2.54); 5.3801 (5.76); 3.3299 (37.79); 3.0182

(16.00); 2.8906 (10.49); 2.7313 (8.46); 2.5253 (0.56); 2.5205 (0.87); 2.5120 (10.77); 2.5075 (21.56); 2.5029 (28.46); 2.4983 (20.56); 2.4938

(9.71); 2.3857 (8.82); −0.0002 (7.41)

›Example 181, Solvent: DMSO, Spectrometer: 399.95 MHz

10.4711 (2.24); 8.2403 (1.27); 8.2197 (1.46); 7.9535 (0.44); 7.9239 (1.22); 7.9043 (1.82); 7.8968 (1.39); 7.8923 (1.45); 7.8844 (1.25); 7.8775

(1.48); 7.8730 (1.42); 7.7447 (1.95); 7.7421 (2.54); 7.7381 (1.21); 7.7295 (0.81); 7.7244 (3.40); 7.7206 (2.31); 7.5964 (0.73); 7.5919 (0.72);

7.5781 (0.95); 7.5753 (1.12); 7.5739 (1.08); 7.5708 (1.07); 7.5668 (0.57); 7.5635 (0.38); 7.5572 (1.05); 7.5526 (1.08); 7.5485 (1.67); 7.5427

(0.49); 7.5336 (0.90); 7.5302 (1.45); 7.5268 (0.72); 7.5016 (2.35); 7.4981 (0.99); 7.4864 (1.59); 7.4825 (3.02); 7.4690 (0.48); 7.4649 (1.22);

7.4615 (0.67); 7.2578 (1.68); 7.2377 (1.50); 7.2228 (1.74); 7.2043 (1.69); 7.1388 (0.99); 7.1366 (0.95); 7.1198 (1.64); 7.1183 (1.58); 7.1013

(0.90); 7.0991 (0.83); 5.4054 (6.07); 3.9637 (13.31); 3.3374 (70.18); 3.1119 (16.00); 2.8910 (3.66); 2.7326 (2.89); 2.7316 (2.80); 2.5260 (0.49);

2.5212 (0.79); 2.5126 (9.51); 2.5081 (18.83); 2.5035 (24.63); 2.4989 (17.69); 2.4944 (8.33); −0.0002 (3.28)

›Example 182, Solvent: DMSO, Spectrometer: 399.95 MHz

10.1856 (0.61); 10.1708 (2.08); 7.8299 (0.39); 7.8088 (2.07); 7.8008 (1.98); 7.7943 (5.27); 7.7799 (0.39); 7.7219 (2.53); 7.7086 (0.83); 7.7038

(3.15); 7.7000 (2.27); 7.5625 (0.48); 7.5507 (0.37); 7.5442 (1.69); 7.5386 (0.50); 7.5293 (0.89); 7.5260 (1.43); 7.5227 (0.74); 7.4957 (2.45);

7.4801 (1.70); 7.4764 (3.15); 7.4627 (0.50); 7.4587 (1.21); 7.4555 (0.69); 7.1015 (1.27); 7.0948 (1.08); 7.0870 (1.13); 7.0808 (1.20); 5.3296

(5.58); 4.1394 (1.64); 4.1223 (3.47); 4.1053 (1.70); 3.9744 (0.34); 3.9590 (0.35); 3.9160 (0.35); 3.8994 (0.35); 3.3428 (190.68); 3.0647 (16.00);

2.8912 (0.69); 2.7321 (0.56); 2.5257 (0.80); 2.5124 (16.78); 2.5079 (33.61); 2.5033 (44.43); 2.4987 (32.45); 2.4943 (15.78); 1.7102 (0.62);

1.6935 (0.82); 1.6767 (0.71); 1.6601 (0.40); 1.5327 (0.98); 1.5156 (2.85); 1.4985 (2.56); 1.4814 (0.80); 1.2348 (0.32); 0.9270 (0.58); 0.9146

(15.37); 0.8980 (14.95); 0.8892 (1.21); 0.8826 (1.81); 0.8725 (0.88); 0.8639 (0.71); −0.0002 (5.02)

›Example 183, Solvent: DMSO, Spectrometer: 400.13 MHz

11.4550 (1.75); 7.9097 (0.81); 7.8897 (1.65); 7.8706 (1.15); 7.7324 (2.64); 7.7197 (0.87); 7.7146 (3.39); 7.7109 (2.39); 7.5698 (0.50); 7.5667

(0.34); 7.5578 (0.39); 7.5516 (1.64); 7.5459 (0.50); 7.5366 (0.89); 7.5333 (1.40); 7.5300 (0.73); 7.5010 (2.35); 7.4854 (1.69); 7.4818 (3.05);

7.4681 (0.49); 7.4641 (1.20); 7.4610 (0.69); 7.2522 (1.52); 7.2320 (1.44); 5.3849 (6.33); 4.4679 (1.79); 4.4515 (3.80); 4.4352 (1.82); 3.3999

(2.05); 3.3497 (219.89); 3.3000 (1.99); 3.0666 (16.00); 2.6767 (0.38); 2.5624 (0.48); 2.5580 (0.61); 2.5535 (0.42); 2.5302 (1.07); 2.5254 (1.80);

2.5167 (22.34); 2.5123 (45.93); 2.5078 (61.94); 2.5033 (44.09); 2.4989 (20.54); 2.4671 (0.41); 2.4627 (0.57); 2.4581 (0.65); 2.4536 (0.42);

2.3346 (0.38); 1.7159 (0.45); 1.6992 (1.32); 1.6923 (0.50); 1.6814 (1.62); 1.6619 (1.41); 1.6455 (0.56); 1.4150 (0.94); 1.3961 (1.55); 1.3773

(1.55); 1.3590 (0.90); 0.9199 (3.53); 0.9015 (7.19); 0.8829 (3.09)

›Example 184, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5439 (1.97); 8.0731 (1.14); 8.0525 (1.36); 7.9531 (0.35); 7.8385 (1.18); 7.8193 (1.58); 7.7990 (1.10); 7.7241 (1.82); 7.7215 (2.39); 7.7176

(1.17); 7.7088 (0.75); 7.7037 (3.21); 7.7000 (2.23); 7.5641 (0.46); 7.5522 (0.34); 7.5458 (1.53); 7.5401 (0.46); 7.5309 (0.80); 7.5275 (1.33);

7.5241 (0.66); 7.4964 (2.23); 7.4929 (0.95); 7.4810 (1.50); 7.4772 (2.86); 7.4637 (0.44); 7.4596 (1.16); 7.4564 (0.63); 7.1985 (0.52); 7.1941

(0.72); 7.1784 (0.84); 7.1743 (1.30); 7.1678 (1.35); 7.1639 (0.95); 7.1602 (0.69); 7.1556 (1.16); 7.1489 (1.55); 7.1438 (2.16); 7.1247 (1.57);

6.9539 (1.59); 6.9336 (1.43); 6.8677 (0.97); 6.8652 (0.85); 6.8492 (1.72); 6.8467 (1.47); 6.8308 (0.79); 6.8282 (0.68); 5.3494 (5.50); 4.0439

(0.51); 4.0261 (0.52); 3.7797 (16.00); 3.3330 (71.39); 3.0469 (15.02); 2.8904 (3.02); 2.8664 (1.01); 2.8485 (1.83); 2.8280 (1.46); 2.8011 (0.32);

2.7321 (2.37); 2.7310 (2.30); 2.6673 (1.68); 2.6506 (1.16); 2.6466 (2.01); 2.6285 (1.02); 2.5461 (0.35); 2.5257 (0.87); 2.5205 (0.88); 2.5119

(10.15); 2.5074 (20.41); 2.5027 (26.76); 2.4981 (19.33); 2.4936 (9.10); 1.1700 (0.58); 1.1522 (1.22); 1.1345 (0.56); 0.8757 (0.43); −0.0002 (5.23)

›Example 185, Solvent: CDCl3, Spectrometer: 300.16 MHz

7.9283 (2.16); 7.9007 (2.74); 7.7163 (1.49); 7.6905 (2.60); 7.6646 (1.29); 7.5846 (4.48); 7.5581 (4.95); 7.2637 (7.93); 7.0223 (2.69); 6.9980

(2.54); 6.9266 (5.31); 6.9007 (4.85); 6.7759 (0.57); 5.3056 (0.37); 5.2570 (10.02); 5.1202 (0.33); 5.0276 (0.79); 5.0079 (1.48); 4.9879 (1.42);

4.9693 (0.79); 3.8411 (16.00); 3.2810 (0.32); 3.0929 (15.51); 1.7320 (0.47); 1.7110 (0.96); 1.6882 (1.31); 1.6508 (1.63); 1.6204 (4.25); 1.5870

(1.42); 1.5647 (0.73); 1.3395 (1.47); 1.3167 (1.80); 1.2930 (9.08); 1.2726 (8.98); 0.9350 (15.38); 0.9144 (14.64); −0.0002 (4.37)

›Example 186, Solvent: DMSO, Spectrometer: 399.95 MHz

10.2345 (2.80); 7.9531 (0.71); 7.8221 (0.75); 7.8011 (1.81); 7.7836 (2.16); 7.7726 (2.19); 7.7703 (2.28); 7.7520 (0.86); 7.7220 (2.79); 7.7040

(3.52); 7.7003 (2.46); 7.5624 (0.52); 7.5594 (0.35); 7.5504 (0.42); 7.5441 (1.74); 7.5385 (0.54); 7.5290 (0.99); 7.5259 (1.47); 7.5226 (0.75);

7.4952 (2.57); 7.4795 (1.87); 7.4760 (3.27); 7.4622 (0.54); 7.4583 (1.25); 7.4552 (0.72); 7.4225 (0.67); 7.4184 (0.65); 7.4035 (1.22); 7.3990

(1.26); 7.3833 (0.68); 7.3800 (0.70); 7.3034 (0.37); 7.2987 (0.77); 7.2840 (0.75); 7.2783 (0.92); 7.2739 (0.52); 7.2645 (0.51); 7.2602 (0.43);

7.2240 (0.42); 7.2070 (0.75); 7.1870 (1.03); 7.1664 (2.07); 7.1500 (1.89); 7.1475 (1.62); 7.1433 (0.86); 7.1316 (0.81); 7.1289 (0.65); 7.1048

(1.62); 7.1022 (1.59); 7.0873 (1.57); 7.0847 (1.47); 5.3288 (6.75); 4.3161 (1.77); 4.2992 (3.90); 4.2823 (1.81); 3.3288 (77.85); 3.0613 (16.00);

3.0360 (0.56); 2.9986 (1.39); 2.9818 (2.76); 2.9650 (1.29); 2.8906 (5.36); 2.7317 (4.48); 2.5113 (19.22); 2.5069 (35.97); 2.5024 (45.95); 2.4978

(33.18); 2.4935 (15.90); 1.2349 (0.43); 0.0079 (0.47); −0.0002 (10.29); −0.0085 (0.33)

›Example 187, Solvent: DMSO, Spectrometer: 399.95 MHz

10.9980 (2.26); 8.1570 (1.59); 8.1370 (1.93); 7.9746 (0.46); 7.9685 (3.76); 7.9636 (1.22); 7.9520 (2.11); 7.9469 (4.65); 7.9408 (0.60); 7.9287

(1.28); 7.9094 (1.76); 7.8891 (1.15); 7.7352 (2.97); 7.7302 (5.32); 7.7251 (1.54); 7.7173 (3.55); 7.7135 (3.43); 7.7085 (3.88); 7.7023 (0.45);

7.5675 (0.48); 7.5557 (0.35); 7.5492 (1.63); 7.5434 (0.48); 7.5343 (0.86); 7.5309 (1.42); 7.5275 (0.70); 7.5008 (2.38); 7.4973 (1.01); 7.4854

(1.61); 7.4816 (3.06); 7.4681 (0.47); 7.4640 (1.22); 7.4607 (0.68); 7.2402 (1.74); 7.2219 (1.69); 5.4168 (6.02); 3.3313 (54.91); 3.0774 (16.00);

2.8908 (7.50); 2.7321 (6.14); 2.7311 (5.80); 2.5252 (0.66); 2.5204 (1.09); 2.5119 (12.91); 2.5074 (25.67); 2.5028 (33.69); 2.4982 (24.28);

2.4936 (11.37); 0.0080 (0.32); −0.0002 (9.68)

›Example 188, Solvent: DMSO, Spectrometer: 399.95 MHz

10.6228 (1.66); 8.0751 (0.94); 8.0544 (1.13); 7.9527 (0.34); 7.8495 (1.04); 7.8300 (1.49); 7.8099 (0.95); 7.7229 (2.22); 7.7101 (0.72); 7.7052

(2.81); 7.7015 (2.00); 7.5646 (0.40); 7.5462 (1.33); 7.5406 (0.42); 7.5313 (0.73); 7.5280 (1.17); 7.5247 (0.64); 7.4971 (2.06); 7.4816 (1.43);

7.4779 (2.59); 7.4644 (0.45); 7.4603 (1.02); 7.4572 (0.62); 7.1583 (1.54); 7.1398 (1.45); 5.3617 (5.31); 3.3370 (87.40); 3.0555 (12.82); 2.8905

(2.63); 2.7445 (0.65); 2.7306 (3.30); 2.7289 (3.34); 2.7171 (3.13); 2.7095 (2.99); 2.6982 (2.32); 2.6821 (0.62); 2.6721 (0.42); 2.5252 (0.62);

2.5117 (10.99); 2.5074 (21.33); 2.5028 (27.84); 2.4983 (20.51); 2.4938 (10.05); 2.0764 (16.00); −0.0002 (2.01)

›Example 189, Solvent: DMSO, Spectrometer: 399.95 MHz

11.1037 (1.84); 8.0165 (1.21); 7.9960 (1.59); 7.9531 (1.28); 7.8721 (1.31); 7.8530 (1.73); 7.8326 (1.15); 7.7282 (2.05); 7.7255 (2.60); 7.7216

(1.30); 7.7129 (0.89); 7.7077 (3.59); 7.7040 (2.47); 7.5647 (0.52); 7.5615 (0.32); 7.5527 (0.38); 7.5464 (1.67); 7.5408 (0.50); 7.5314 (0.89);

7.5281 (1.45); 7.5247 (0.74); 7.4953 (2.39); 7.4918 (1.01); 7.4799 (1.69); 7.4761 (3.12); 7.4625 (0.50); 7.4584 (1.27); 7.4553 (0.70); 7.1973

(1.70); 7.1799 (1.65); 5.3952 (5.72); 3.3590 (0.49); 3.3334 (125.04); 3.0610 (16.00); 2.8911 (10.61); 2.7322 (8.55); 2.7310 (8.21); 2.5253 (0.85);

2.5205 (1.37); 2.5120 (16.39); 2.5075 (32.58); 2.5028 (42.74); 2.4982 (30.83); 2.4937 (14.55); 2.4377 (0.45); 2.4190 (0.62); 2.4008 (0.64);

2.3823 (0.49); 2.2072 (0.39); 2.1911 (1.52); 2.1747 (1.58); 2.1584 (0.40); 1.4256 (0.51); 1.4069 (0.72); 1.3887 (0.73); 1.3702 (0.61); 1.2832

(0.45); 1.1985 (6.18); 1.1822 (5.98); 0.8909 (2.37); 0.8724 (5.19); 0.8626 (0.89); 0.8536 (2.23); 0.0080 (0.43); −0.0002 (12.63); −0.0085 (0.36)

›Example 190, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5608 (1.34); 8.0228 (0.72); 8.0021 (0.89); 7.9528 (0.38); 7.8316 (0.76); 7.8122 (1.10); 7.7920 (0.69); 7.7302 (1.64); 7.7124 (2.01); 7.7087

(1.45); 7.5489 (0.97); 7.5436 (0.32); 7.5340 (0.53); 7.5309 (0.83); 7.5277 (0.47); 7.5005 (1.48); 7.4847 (1.03); 7.4813 (1.85); 7.4636 (0.69);

7.4606 (0.43); 7.1509 (1.12); 7.1325 (1.07); 6.8993 (1.12); 6.8772 (1.75); 6.8389 (1.14); 6.8314 (1.58); 6.8066 (1.21); 6.7989 (0.76); 6.7846

(0.72); 6.7769 (0.52); 5.3707 (3.71); 3.6870 (16.00); 3.5449 (0.32); 3.3313 (39.68); 3.0634 (8.83); 2.8898 (2.88); 2.7309 (2.40); 2.5110 (7.31);

2.5067 (13.78); 2.5022 (17.78); 2.4977 (13.04); 2.4933 (6.37); 1.1676 (0.35); −0.0002 (3.10)

›Example 191, Solvent: DMSO, Spectrometer: 499.93 MHz

12.1460 (2.13); 8.0017 (0.91); 7.9855 (2.03); 7.9703 (1.79); 7.9417 (2.55); 7.9255 (1.40); 7.7986 (0.34); 7.7938 (0.42); 7.6739 (4.00); 7.6699

(2.08); 7.6561 (4.45); 7.3455 (1.98); 7.3308 (1.92); 7.0396 (4.23); 7.0218 (4.19); 5.7761 (3.49); 5.3920 (6.96); 5.3772 (0.52); 5.2861 (0.72);

3.8283 (0.81); 3.8147 (16.00); 3.3674 (5.04); 3.3439 (0.35); 3.1634 (0.42); 3.0586 (15.02); 2.5170 (2.29); 2.5137 (3.03); 2.5104 (2.41); 1.9994

(0.56); 1.2582 (0.59); 1.2457 (0.67); 1.2342 (0.58); 1.2218 (0.52); 0.8992 (0.72); 0.8879 (0.71); 0.8862 (0.72)

›Example 192, Solvent: DMSO, Spectrometer: 399.95 MHz

10.1742 (2.55); 7.9535 (0.41); 7.8300 (0.54); 7.8090 (1.93); 7.7933 (4.11); 7.7896 (2.83); 7.7732 (0.60); 7.7260 (1.98); 7.7233 (2.58); 7.7195

(1.26); 7.7108 (0.78); 7.7056 (3.39); 7.7019 (2.37); 7.5632 (0.49); 7.5513 (0.36); 7.5449 (1.63); 7.5391 (0.49); 7.5300 (0.88); 7.5266 (1.43);

7.5232 (0.73); 7.4962 (2.40); 7.4928 (1.03); 7.4809 (1.64); 7.4771 (3.06); 7.4635 (0.47); 7.4595 (1.22); 7.4562 (0.68); 7.1022 (1.35); 7.0975

(1.36); 7.0861 (1.24); 7.0815 (1.28); 5.3340 (6.35); 4.0253 (4.21); 4.0105 (4.19); 3.3444 (106.79); 3.3202 (0.53); 3.0655 (16.00); 2.8915 (3.26);

2.7329 (2.64); 2.7317 (2.60); 2.5264 (0.50); 2.5216 (0.82); 2.5131 (9.67); 2.5086 (19.27); 2.5040 (25.37); 2.4994 (18.43); 2.4948 (8.78); 1.5324

(0.68); 1.5169 (1.01); 1.5013 (0.84); 1.4858 (0.41); 1.3872 (0.69); 1.3779 (0.56); 1.3682 (1.83); 1.3595 (1.77); 1.3495 (2.08); 1.3419 (2.25);

1.3336 (1.60); 1.3247 (1.84); 1.3149 (0.57); 1.3067 (0.76); 0.8918 (6.94); 0.8827 (0.78); 0.8733 (14.45); 0.8545 (5.92); −0.0002 (1.59)

›Example 193, Solvent: DMSO, Spectrometer: 400.13 MHz

9.8075 (1.18); 7.8067 (0.34); 7.7858 (0.74); 7.7676 (0.77); 7.7440 (0.93); 7.7250 (0.43); 7.6041 (0.34); 7.5968 (0.55); 7.5913 (0.40); 7.5840

(0.43); 7.5770 (0.75); 7.5580 (0.36); 7.3637 (0.39); 7.3434 (0.40); 7.3361 (0.53); 7.3329 (0.66); 7.3142 (1.09); 7.2951 (0.38); 7.2926 (0.33);

7.1170 (0.69); 7.1003 (0.64); 5.3220 (2.56); 3.3496 (6.90); 2.5169 (3.21); 2.5126 (6.45); 2.5081 (8.62); 2.5037 (6.15); 2.4994 (2.89); 1.4659

(16.00); 1.3779 (0.32)

›Example 194, Solvent: DMSO, Spectrometer: 399.95 MHz

12.1539 (1.39); 7.7436 (0.41); 7.7375 (1.92); 7.7348 (2.58); 7.7308 (1.30); 7.7224 (0.96); 7.7172 (3.36); 7.7134 (2.30); 7.5640 (0.50); 7.5608

(0.34); 7.5527 (0.38); 7.5457 (1.64); 7.5398 (0.52); 7.5310 (1.00); 7.5276 (1.52); 7.5241 (0.76); 7.5018 (2.48); 7.4984 (1.12); 7.4868 (1.72);

7.4828 (3.05); 7.4695 (0.57); 7.4653 (1.22); 7.4618 (0.68); 7.3763 (7.33); 7.3708 (3.59); 7.3602 (3.85); 7.3533 (3.47); 7.3461 (1.39); 7.3429

(1.36); 7.3404 (1.38); 7.3198 (3.36); 7.3085 (0.92); 7.2970 (1.17); 7.2847 (0.33); 5.4850 (0.46); 5.3745 (0.36); 5.3310 (4.73); 5.1949 (0.66);

5.1861 (0.60); 5.1812 (0.78); 4.9241 (1.28); 4.9149 (1.23); 4.9102 (0.96); 4.9057 (1.15); 4.8977 (1.97); 4.8879 (0.35); 4.8592 (0.62); 4.8455

(0.58); 4.8349 (0.77); 4.7813 (1.01); 4.5853 (6.58); 4.5680 (2.97); 4.5464 (0.58); 4.2871 (2.56); 4.2709 (0.78); 4.2462 (6.50); 4.1258 (0.96);

4.1098 (0.95); 3.8443 (0.78); 3.6800 (2.12); 3.3842 (0.41); 3.3326 (338.47); 3.0557 (0.36); 3.0468 (0.32); 3.0156 (16.00); 2.8903 (0.99); 2.7304

(0.77); 2.6800 (0.32); 2.6756 (0.70); 2.6711 (0.96); 2.6664 (0.68); 2.5244 (2.76); 2.5196 (4.50); 2.5110 (56.29); 2.5065 (112.47); 2.5019

(148.17); 2.4973 (107.53); 2.4928 (51.23); 2.3377 (0.36); 2.3333 (0.74); 2.3287 (0.99); 2.3242 (0.72); 2.3197 (0.36); 1.2352 (0.66); 0.0080

(0.97); −0.0002 (29.69); −0.0086 (0.88)

›Example 195, Solvent: DMSO, Spectrometer: 399.95 MHz

11.9972 (1.78); 7.9529 (0.44); 7.7372 (1.98); 7.7347 (2.59); 7.7307 (1.25); 7.7222 (0.80); 7.7170 (3.40); 7.7132 (2.33); 7.5641 (0.46); 7.5527

(0.34); 7.5458 (1.66); 7.5399 (0.49); 7.5311 (0.92); 7.5277 (1.48); 7.5242 (0.74); 7.5018 (2.47); 7.4985 (1.05); 7.4868 (1.61); 7.4828 (3.05);

7.4694 (0.48); 7.4653 (1.20); 7.4618 (0.66); 7.3106 (4.44); 5.3305 (6.05); 4.1165 (9.21); 4.0002 (0.65); 3.9902 (0.90); 3.9804 (0.78); 3.3322

(59.45); 3.0125 (16.00); 2.8908 (3.55); 2.7320 (2.85); 2.7310 (2.79); 2.5251 (0.57); 2.5117 (11.15); 2.5072 (22.21); 2.5026 (29.22); 2.4980

(21.22); 2.4935 (10.14); 1.6846 (0.35); 1.6746 (0.78); 1.6707 (0.89); 1.6578 (2.44); 1.6550 (2.68); 1.6490 (3.72); 1.6465 (3.44); 1.6385 (4.46);

1.6298 (1.54); 1.6187 (0.74); 1.6075 (0.55); 1.6028 (0.52); 1.4829 (1.01); 1.4761 (1.08); 1.4665 (0.90); 0.0080 (0.33); −0.0002 (10.02)

›Example 196, Solvent: DMSO, Spectrometer: 399.95 MHz

10.8301 (1.89); 8.0235 (1.08); 8.0028 (1.34); 7.9533 (0.96); 7.8389 (1.29); 7.8197 (1.72); 7.7993 (1.14); 7.7256 (1.93); 7.7231 (2.55); 7.7192

(1.20); 7.7104 (0.77); 7.7053 (3.41); 7.7015 (2.34); 7.5655 (0.49); 7.5536 (0.36); 7.5472 (1.63); 7.5415 (0.48); 7.5322 (0.86); 7.5289 (1.40);

7.5255 (0.69); 7.4972 (2.36); 7.4938 (0.98); 7.4818 (1.62); 7.4781 (3.04); 7.4644 (0.47); 7.4604 (1.22); 7.4572 (0.67); 7.3943 (0.94); 7.3926

(0.74); 7.3874 (0.54); 7.3790 (0.90); 7.3722 (7.83); 7.3690 (2.87); 7.3644 (6.62); 7.3575 (0.74); 7.3490 (0.45); 7.3422 (0.88); 7.1637 (1.72);

7.1463 (1.66); 5.3697 (5.94); 3.7272 (5.85); 3.3342 (102.59); 3.0507 (16.00); 2.8907 (8.08); 2.7321 (6.25); 2.7311 (6.24); 2.5255 (0.68); 2.5207

(1.08); 2.5122 (13.38); 2.5076 (26.78); 2.5030 (35.23); 2.4984 (25.41); 2.4938 (11.94); −0.0002 (5.23)

›Example 197, Solvent: DMSO, Spectrometer: 499.93 MHz

7.7531 (2.74); 7.7426 (0.97); 7.7387 (3.35); 7.7358 (2.51); 7.5661 (0.54); 7.5637 (0.38); 7.5561 (0.44); 7.5514 (1.70); 7.5472 (0.66); 7.5390

(1.14); 7.5368 (1.54); 7.5343 (0.91); 7.5244 (0.43); 7.5060 (2.59); 7.5029 (2.05); 7.4904 (3.82); 7.4796 (0.97); 7.4762 (1.65); 7.4739 (1.33);

7.4713 (1.47); 7.3695 (0.33); 7.3009 (0.60); 7.2960 (0.34); 7.2920 (0.74); 7.2847 (0.62); 7.1964 (0.41); 6.5446 (1.64); 6.5402 (2.15); 6.5263

(2.97); 5.7777 (2.34); 5.2802 (0.36); 5.2431 (6.80); 3.9093 (0.44); 3.7593 (1.82); 3.6223 (0.46); 3.6209 (0.46); 3.4938 (1.50); 3.4798 (4.87);

3.4658 (5.01); 3.4519 (1.70); 3.3664 (2.18); 3.3406 (0.69); 3.0694 (16.00); 3.0540 (0.46); 3.0210 (0.67); 2.5204 (1.77); 2.5171 (3.78); 2.5136

(5.21); 2.5100 (3.94); 2.5067 (2.01); 2.3165 (1.95); 2.2189 (0.71); 1.6012 (0.53); 1.4713 (0.51); 1.4334 (0.97); 1.2419 (0.47); 1.0913 (5.78);

1.0774 (13.03); 1.0634 (5.98)

›Example 198, Solvent: DMSO, Spectrometer: 400.13 MHz

12.1310 (3.72); 7.7440 (4.00); 7.7247 (4.54); 7.5710 (0.65); 7.5531 (1.97); 7.5354 (1.98); 7.5100 (3.43); 7.4909 (4.23); 7.4724 (1.53); 7.2682

(5.13); 5.3276 (8.77); 4.0450 (0.91); 4.0271 (0.91); 3.3442 (36.64); 3.0208 (16.00); 2.5109 (29.55); 2.4248 (2.36); 2.4065 (4.70); 2.3881 (2.63);

1.9971 (3.67); 1.6264 (0.57); 1.6080 (1.91); 1.5902 (2.77); 1.5725 (1.95); 1.5551 (0.63); 1.3164 (0.70); 1.3013 (1.67); 1.2772 (4.42); 1.2699

(4.39); 1.2406 (1.32); 1.1996 (1.03); 1.1818 (1.92); 1.1640 (0.99); 1.1305 (0.56); 1.1154 (0.55); 0.8807 (3.55); 0.8646 (7.48); 0.8471 (3.55)

›Example 199, Solvent: DMSO, Spectrometer: 400.13 MHz

10.2386 (3.75); 7.8908 (0.59); 7.8698 (2.25); 7.8535 (5.80); 7.8338 (0.76); 7.7875 (3.92); 7.7688 (4.45); 7.6246 (0.65); 7.6068 (1.98); 7.5890

(1.85); 7.5583 (3.28); 7.5391 (4.18); 7.5208 (1.54); 7.1635 (2.05); 7.1473 (1.94); 5.8248 (3.93); 5.3893 (8.72); 5.0345 (0.71); 5.0193 (1.26);

5.0073 (1.31); 4.9917 (0.76); 3.5848 (0.76); 3.5613 (1.84); 3.5439 (2.34); 3.5280 (4.17); 3.5098 (4.87); 3.4924 (1.20); 3.4863 (1.02); 3.3996

(33.79); 3.3760 (2.77); 3.1356 (16.00); 2.5664 (53.52); 2.3924 (0.33); 1.2763 (7.71); 1.2602 (7.72); 1.1786 (4.44); 1.1611 (8.80); 1.1437

(4.38); −0.0002 (0.32)

›Example 200, Solvent: DMSO, Spectrometer: 399.95 MHz

10.0669 (2.72); 7.9531 (0.43); 7.8220 (0.42); 7.8009 (2.26); 7.7921 (2.46); 7.7862 (5.44); 7.7712 (0.51); 7.7224 (2.73); 7.7186 (1.39); 7.7097

(0.86); 7.7046 (3.50); 7.7009 (2.49); 7.5625 (0.51); 7.5593 (0.34); 7.5506 (0.38); 7.5441 (1.66); 7.5384 (0.53); 7.5292 (0.91); 7.5259 (1.47);

7.5225 (0.79); 7.4957 (2.51); 7.4924 (1.15); 7.4803 (1.70); 7.4765 (3.17); 7.4630 (0.52); 7.4589 (1.25); 7.4557 (0.73); 7.0955 (1.33); 7.0893

(1.34); 7.0810 (1.17); 7.0748 (1.30); 5.3256 (6.60); 4.8229 (0.50); 4.8074 (0.82); 4.7906 (0.83); 4.7751 (0.51); 3.3495 (128.02); 3.0714 (16.00);

2.8916 (3.46); 2.7321 (2.77); 2.5266 (0.61); 2.5134 (10.19); 2.5089 (20.15); 2.5043 (26.68); 2.4998 (19.80); 2.4953 (9.87); 1.5837 (0.40);

1.5731 (0.52); 1.5645 (0.45); 1.5596 (0.43); 1.5548 (0.51); 1.5393 (0.62); 1.5248 (0.57); 1.5183 (0.44); 1.5046 (0.40); 1.3356 (0.55); 1.3080

(1.81); 1.2994 (2.11); 1.2965 (2.07); 1.2850 (1.55); 1.2719 (0.77); 1.2598 (0.36); 1.2534 (0.33); 1.2303 (6.88); 1.2147 (6.76); 0.8885 (1.66);

0.8715 (3.87); 0.8536 (1.45); −0.0002 (0.79)

›Example 201, Solvent: DMSO, Spectrometer: 400.13 MHz

10.3873 (6.45); 7.8543 (1.01); 7.8332 (4.47); 7.8216 (5.37); 7.8174 (9.45); 7.8009 (1.23); 7.7953 (0.41); 7.7250 (5.85); 7.7123 (1.79); 7.7072

(7.41); 7.7035 (5.23); 7.5769 (0.64); 7.5738 (1.12); 7.5706 (0.83); 7.5619 (0.96); 7.5554 (3.69); 7.5497 (1.21); 7.5406 (2.12); 7.5373 (3.23);

7.5339 (1.73); 7.5087 (5.41); 7.4934 (3.70); 7.4896 (6.72); 7.4761 (1.15); 7.4720 (2.75); 7.4687 (1.67); 7.4404 (2.11); 7.4358 (2.89); 7.4192

(7.93); 7.4152 (7.60); 7.4135 (7.36); 7.4107 (6.78); 7.4052 (1.46); 7.3934 (7.72); 7.3889 (2.42); 7.3785 (1.83); 7.3742 (2.89); 7.3582 (1.70);

7.3537 (2.67); 7.3487 (1.41); 7.3439 (1.17); 7.3365 (2.54); 7.3291 (0.96); 7.3238 (0.83); 7.3171 (1.39); 7.1149 (2.86); 7.1095 (2.85); 7.0996

(2.59); 7.0942 (2.75); 5.3506 (13.87); 5.1862 (16.00); 4.5052 (0.38); 4.4907 (0.37); 3.5221 (1.78); 3.5040 (6.02); 3.4858 (6.14); 3.4676 (1.85);

3.3953 (2.45); 3.3454 (152.36); 3.3218 (1.12); 3.2955 (1.14); 2.6792 (0.38); 2.5689 (0.38); 2.5646 (0.74); 2.5600 (1.00); 2.5556 (0.73); 2.5511

(0.37); 2.5325 (0.86); 2.5191 (22.11); 2.5147 (46.04); 2.5102 (62.64); 2.5057 (44.54); 2.5013 (20.50); 2.4602 (0.44); 2.4558 (0.38); 2.3369

(0.38); 1.9972 (1.37); 1.3708 (1.12); 1.3237 (0.55); 1.2407 (0.43); 1.1994 (0.42); 1.1817 (0.76); 1.1639 (0.38); 1.0551 (6.72); 1.0370 (15.39);

1.0187 (6.58)

›Example 202, Solvent: DMSO, Spectrometer: 399.95 MHz

11.0982 (2.23); 8.1505 (1.59); 8.1306 (1.94); 7.9528 (0.93); 7.9484 (1.54); 7.9289 (1.82); 7.9087 (1.18); 7.7624 (1.46); 7.7567 (1.82); 7.7440

(1.37); 7.7412 (2.11); 7.7380 (3.00); 7.7355 (3.97); 7.7315 (1.56); 7.7229 (0.91); 7.7176 (3.43); 7.7138 (2.37); 7.5689 (0.48); 7.5657 (0.33);

7.5574 (0.69); 7.5508 (2.02); 7.5452 (0.73); 7.5353 (1.52); 7.5323 (1.77); 7.5290 (1.92); 7.5233 (0.66); 7.5121 (0.51); 7.5020 (2.55); 7.4867

(1.60); 7.4829 (3.07); 7.4694 (0.48); 7.4653 (1.23); 7.4620 (0.70); 7.2632 (1.78); 7.2454 (1.72); 5.4248 (6.10); 3.3442 (100.27); 3.0943 (0.34);

3.0785 (16.00); 2.8913 (6.97); 2.7324 (5.33); 2.7317 (5.39); 2.5263 (0.62); 2.5215 (0.99); 2.5130 (11.94); 2.5085 (23.82); 2.5039 (31.41);

2.4993 (22.74); 2.4947 (10.77); −0.0002 (1.22)

›Example 203, Solvent: DMSO, Spectrometer: 400.13 MHz

12.4298 (2.41); 7.6250 (1.17); 7.6181 (1.35); 7.6141 (1.40); 7.6040 (1.01); 7.5940 (3.31); 7.5687 (0.82); 7.5546 (0.92); 7.5485 (1.27); 7.5342

(1.22); 7.5295 (0.81); 7.5134 (0.53); 7.4305 (0.62); 7.4278 (0.68); 7.4244 (0.64); 7.4217 (0.59); 7.4069 (1.11); 7.4027 (1.00); 7.3883 (0.52);

7.3828 (0.57); 7.3510 (0.51); 7.3468 (0.37); 7.3314 (3.65); 7.3262 (4.10); 7.3179 (13.37); 7.3034 (5.07); 7.2906 (0.37); 7.2780 (0.90); 7.2713

(0.94); 7.2689 (0.99); 7.2601 (0.81); 7.2565 (0.95); 7.2518 (0.68); 7.2465 (0.45); 7.2428 (0.47); 5.7615 (4.82); 5.3522 (6.66); 4.0419 (0.68);

4.0241 (0.70); 3.7558 (8.04); 3.4034 (3.90); 3.3532 (198.24); 3.3033 (2.75); 3.0161 (16.00); 2.5626 (0.48); 2.5580 (0.65); 2.5534 (0.51); 2.5488

(0.36); 2.5122 (27.53); 2.5078 (36.26); 2.5035 (26.37); 2.4625 (0.39); 2.4579 (0.46); 1.9936 (2.97); 1.2468 (0.42); 1.1964 (0.81); 1.1786 (1.57);

1.1608 (0.77); 0.8615 (0.51)

›Example 204, Solvent: DMSO, Spectrometer: 399.95 MHz

10.8413 (2.18); 8.0076 (1.27); 7.9870 (1.66); 7.9530 (0.92); 7.8670 (1.37); 7.8477 (1.84); 7.8274 (1.15); 7.7281 (2.70); 7.7243 (1.32); 7.7153

(0.79); 7.7103 (3.45); 7.7065 (2.42); 7.5697 (0.49); 7.5665 (0.32); 7.5576 (0.37); 7.5512 (1.66); 7.5456 (0.50); 7.5363 (0.87); 7.5330 (1.43);

7.5297 (0.74); 7.5012 (2.46); 7.4979 (1.09); 7.4857 (1.69); 7.4820 (3.19); 7.4718 (0.53); 7.4632 (4.80); 7.4577 (1.35); 7.4460 (1.27); 7.4405

(4.44); 7.4318 (0.38); 7.2020 (1.83); 7.1841 (1.73); 6.9056 (0.43); 6.8969 (4.17); 6.8914 (1.24); 6.8798 (1.20); 6.8743 (3.92); 6.8656 (0.33);

5.3842 (6.11); 5.0686 (1.07); 5.0521 (1.07); 3.3370 (109.15); 3.0613 (16.00); 2.8907 (7.63); 2.7313 (6.04); 2.5256 (0.74); 2.5123 (14.64);

2.5078 (29.08); 2.5032 (38.29); 2.4986 (27.75); 2.4941 (13.21); 1.5345 (5.46); 1.5181 (5.42); −0.0002 (2.46)

›Example 205, Solvent: DMSO, Spectrometer: 400.13 MHz

10.2539 (2.80); 7.8468 (0.61); 7.8258 (1.79); 7.8087 (2.72); 7.8062 (2.48); 7.8021 (2.53); 7.7850 (0.72); 7.7811 (0.46); 7.7309 (1.95); 7.7284

(2.59); 7.7246 (1.32); 7.7158 (0.79); 7.7106 (3.35); 7.7069 (2.41); 7.5683 (0.48); 7.5652 (0.33); 7.5565 (0.38); 7.5501 (1.60); 7.5444 (0.49);

7.5351 (0.88); 7.5318 (1.44); 7.5284 (0.76); 7.5012 (2.40); 7.4979 (1.11); 7.4858 (1.63); 7.4821 (3.03); 7.4685 (0.48); 7.4644 (1.19); 7.4612

(0.69); 7.1199 (1.35); 7.1161 (1.41); 7.1031 (1.29); 7.0993 (1.32); 5.7629 (5.65); 5.3423 (6.20); 4.1663 (1.39); 4.1503 (2.90); 4.1344 (1.43);

3.4009 (2.36); 3.3509 (182.55); 3.3235 (0.34); 3.3010 (1.74); 3.0681 (16.00); 2.5583 (0.34); 2.5307 (0.42); 2.5259 (0.71); 2.5173 (9.78); 2.5128

(20.52); 2.5083 (28.08); 2.5038 (20.19); 2.4994 (9.50); 2.4590 (0.42); 2.4316 (0.70); 2.4170 (0.49); 2.4119 (0.70); 2.4027 (0.88); 2.3911 (0.88);

2.3830 (0.71); 2.3742 (0.50); 2.3625 (0.76); 2.3340 (0.37); 1.8789 (0.44); 1.8630 (1.09); 1.8478 (0.92); 1.8426 (1.08); 1.8232 (1.04); 1.8071

(0.38)

›Example 206, Solvent: CDCl3, Spectrometer: 300.16 MHz

7.9142 (1.19); 7.8866 (1.56); 7.7097 (1.08); 7.6839 (1.47); 7.6570 (0.91); 7.4591 (0.71); 7.4531 (0.81); 7.4458 (0.66); 7.4349 (0.44); 7.4262

(0.66); 7.4204 (0.84); 7.4161 (0.95); 7.4092 (1.09); 7.3916 (0.96); 7.3833 (1.04); 7.3753 (1.26); 7.3697 (2.24); 7.3668 (2.31); 7.3494 (0.46);

7.3447 (0.58); 7.2622 (13.27); 7.2093 (0.48); 7.2037 (0.55); 7.2010 (0.58); 7.1959 (0.54); 7.1818 (1.16); 7.1740 (1.97); 7.1593 (0.69); 7.1505

(0.70); 7.1425 (0.38); 7.0029 (1.55); 6.9786 (1.46); 5.5854 (0.66); 5.3012 (2.73); 5.2941 (7.16); 3.1072 (0.41); 3.0941 (16.00); 1.5679 (0.47);

1.5257 (41.12); 1.4635 (0.34); 1.4433 (8.40); −0.0002 (7.32)

›Example 207, Solvent: DMSO, Spectrometer: 400.13 MHz

10.1215 (6.72); 7.8362 (1.44); 7.8152 (4.05); 7.7981 (5.62); 7.7940 (5.07); 7.7903 (5.55); 7.7730 (1.72); 7.7694 (1.12); 7.7248 (6.08); 7.7209

(3.06); 7.7121 (1.93); 7.7070 (7.83); 7.7033 (5.52); 7.5771 (0.61); 7.5741 (1.08); 7.5709 (0.73); 7.5623 (0.89); 7.5557 (3.78); 7.5500 (1.15);

7.5409 (2.15); 7.5376 (3.34); 7.5342 (1.75); 7.5100 (5.71); 7.4948 (3.76); 7.4909 (7.02); 7.4775 (1.12); 7.4734 (2.70); 7.4700 (1.55); 7.0981

(3.21); 7.0946 (3.22); 7.0812 (3.06); 7.0776 (2.98); 5.3434 (13.84); 4.8874 (0.98); 4.8720 (1.46); 4.8583 (1.41); 4.8547 (1.50); 4.8394 (1.01);

3.5303 (1.75); 3.5122 (6.02); 3.4940 (6.13); 3.4759 (1.90); 3.4628 (0.45); 3.4124 (8.00); 3.3926 (0.68); 3.3623 (579.30); 3.3382 (1.37); 3.3297

(0.78); 3.3253 (0.75); 3.3123 (6.40); 2.8081 (2.87); 2.8015 (6.71); 2.7949 (2.94); 2.6835 (0.34); 2.6790 (0.50); 2.6744 (0.35); 2.5689 (0.36);

2.5645 (0.75); 2.5600 (1.03); 2.5555 (0.74); 2.5509 (0.37); 2.5323 (1.30); 2.5275 (2.21); 2.5188 (29.41); 2.5144 (61.47); 2.5099 (83.77); 2.5054

(59.95); 2.5011 (27.90); 2.4691 (0.57); 2.4645 (0.81); 2.4600 (0.99); 2.4554 (0.72); 2.3414 (0.40); 2.3368 (0.55); 2.3323 (0.42); 2.2867 (1.91);

2.2801 (2.07); 2.2678 (4.04); 2.2614 (3.84); 2.2501 (2.37); 2.2436 (2.18); 1.7945 (0.62); 1.7773 (1.26); 1.7596 (2.65); 1.7510 (0.87); 1.7415

(2.98); 1.7241 (2.67); 1.7046 (1.15); 1.6904 (0.48); 1.3029 (0.41); 1.2929 (0.39); 1.2869 (0.52); 1.2585 (14.74); 1.2429 (15.24); 1.0647 (7.01);

1.0466 (16.00); 1.0284 (6.85); 0.8798 (0.69); 0.8630 (2.19); 0.8454 (0.86)

›Example 208, Solvent: DMSO, Spectrometer: 399.95 MHz

10.4914 (1.95); 8.0795 (1.27); 8.0589 (1.49); 7.9534 (0.57); 7.8298 (1.25); 7.8106 (1.73); 7.7902 (1.19); 7.7256 (1.98); 7.7230 (2.57); 7.7192

(1.25); 7.7104 (0.82); 7.7053 (3.47); 7.7015 (2.34); 7.5640 (0.49); 7.5521 (0.37); 7.5457 (1.63); 7.5400 (0.48); 7.5307 (0.88); 7.5274 (1.42);

7.5240 (0.70); 7.4961 (2.40); 7.4926 (1.00); 7.4807 (1.68); 7.4770 (3.06); 7.4634 (0.49); 7.4593 (1.23); 7.4561 (0.67); 7.1404 (1.73); 7.1230

(1.69); 5.3542 (6.07); 3.3300 (53.86); 3.0544 (16.00); 2.8910 (4.71); 2.7324 (3.77); 2.7313 (3.66); 2.5255 (0.57); 2.5206 (0.96); 2.5121 (10.93);

2.5076 (21.56); 2.5030 (28.24); 2.4984 (20.40); 2.4939 (9.59); 2.2748 (3.13); 2.2572 (3.26); 1.7590 (0.35); 1.7501 (0.45); 1.7418 (0.38); 1.7319

(0.32); 1.6732 (1.45); 1.6665 (1.45); 1.6415 (1.86); 1.5830 (0.45); 1.2343 (0.68); 1.2257 (0.72); 1.2014 (0.76); 1.1946 (0.91); 1.1636 (0.87);

1.1335 (0.51); 1.1032 (0.35); 1.0019 (0.38); 0.9960 (0.45); 0.9671 (0.99); 0.9405 (0.81); 0.8758 (0.44); −0.0002 (5.71)

›Example 210, Solvent: DMSO, Spectrometer: 399.95 MHz

10.2465 (2.58); 7.9533 (0.56); 7.8237 (0.58); 7.8067 (0.53); 7.8026 (1.81); 7.7856 (3.42); 7.7803 (2.40); 7.7634 (0.64); 7.7593 (0.35); 7.7305

(0.32); 7.7250 (1.97); 7.7223 (2.58); 7.7185 (1.27); 7.7098 (0.81); 7.7046 (3.42); 7.7009 (2.39); 7.5626 (0.48); 7.5507 (0.37); 7.5443 (1.63);

7.5386 (0.50); 7.5293 (0.88); 7.5260 (1.42); 7.5226 (0.73); 7.4951 (2.38); 7.4917 (1.04); 7.4798 (1.66); 7.4760 (3.07); 7.4624 (0.49); 7.4584

(1.23); 7.4551 (0.69); 7.2617 (1.60); 7.2454 (1.83); 7.2098 (0.33); 7.2040 (0.83); 7.1851 (2.07); 7.1664 (1.43); 7.1162 (1.95); 7.1055 (1.55);

7.1013 (1.67); 7.0928 (1.72); 7.0890 (2.12); 7.0848 (1.62); 7.0741 (0.95); 7.0387 (1.16); 7.0200 (0.90); 5.3317 (6.15); 4.4018 (0.68); 4.3848

(0.32); 4.2879 (1.61); 4.2705 (3.66); 4.2531 (1.67); 3.3314 (67.99); 3.0619 (16.00); 2.9517 (0.48); 2.9070 (1.42); 2.8902 (7.30); 2.8724 (1.34);

2.7321 (3.71); 2.7309 (3.66); 2.5250 (0.65); 2.5201 (1.10); 2.5117 (11.88); 2.5072 (23.41); 2.5025 (30.75); 2.4979 (22.38); 2.4934 (10.71);

2.2922 (1.58); 2.2788 (10.11); −0.0002 (6.38)

›Example 211, Solvent: DMSO, Spectrometer: 400.13 MHz

10.5300 (2.16); 8.0820 (1.25); 8.0613 (1.47); 7.8411 (1.22); 7.8217 (1.74); 7.8016 (1.11); 7.4233 (1.03); 7.4034 (2.19); 7.3833 (1.59); 7.2856

(1.43); 7.2833 (1.28); 7.2661 (1.17); 7.2639 (0.98); 7.2455 (1.54); 7.2396 (1.97); 7.2354 (1.37); 7.1463 (2.84); 7.1400 (1.14); 7.1382 (1.10);

7.1268 (2.18); 7.1193 (0.92); 5.3602 (5.94); 3.7893 (16.00); 3.3436 (40.59); 3.0438 (14.80); 2.5610 (0.36); 2.5321 (1.09); 2.5187 (16.41);

2.5143 (33.34); 2.5099 (45.01); 2.5054 (32.39); 2.5011 (15.25); 2.4608 (0.40); 2.3960 (1.63); 2.3776 (3.06); 2.3591 (1.76); 1.6129 (0.36);

1.5943 (1.09); 1.5759 (1.51); 1.5581 (1.05); 1.5397 (0.35); 1.3252 (0.38); 1.3092 (0.85); 1.2925 (1.70); 1.2850 (2.49); 1.2777 (2.12); 1.2677

(1.76); 1.2575 (1.37); 1.2472 (0.90); 0.8864 (2.49); 0.8694 (6.22); 0.8516 (2.57)

›Example 212, Solvent: DMSO, Spectrometer: 399.95 MHz

12.7329 (1.22); 7.9533 (1.66); 7.7494 (1.84); 7.7465 (2.48); 7.7425 (1.20); 7.7342 (0.74); 7.7290 (3.27); 7.7252 (2.24); 7.6770 (1.30); 7.6745

(1.29); 7.6713 (1.59); 7.6670 (1.88); 7.6652 (1.78); 7.6608 (2.96); 7.6587 (1.90); 7.5685 (0.44); 7.5502 (1.55); 7.5442 (0.47); 7.5356 (0.88);

7.5321 (1.45); 7.5286 (0.72); 7.5079 (2.34); 7.5045 (1.00); 7.4930 (1.48); 7.4889 (2.85); 7.4720 (2.20); 7.4678 (0.80); 7.4624 (0.34); 7.4520

(2.53); 7.4315 (1.35); 7.3830 (3.66); 7.2063 (0.90); 7.2041 (0.98); 7.2000 (0.92); 7.1978 (0.89); 7.1857 (0.79); 7.1832 (0.78); 7.1796 (0.81);

7.1771 (0.72); 5.3863 (5.28); 3.8427 (16.00); 3.3389 (84.95); 3.0183 (15.32); 2.8912 (13.52); 2.7326 (10.94); 2.7314 (10.57); 2.5260 (0.60);

2.5212 (0.97); 2.5126 (11.52); 2.5081 (22.90); 2.5035 (30.01); 2.4989 (21.67); 2.4943 (10.22); −0.0002 (5.68)

›Example 213, Solvent: DMSO, Spectrometer: 399.95 MHz

12.4033 (1.18); 7.9526 (1.06); 7.7378 (2.75); 7.7339 (1.35); 7.7253 (0.81); 7.7202 (3.49); 7.7164 (2.47); 7.5661 (0.49); 7.5629 (0.33); 7.5546

(0.35); 7.5477 (1.68); 7.5419 (0.51); 7.5330 (0.94); 7.5297 (1.52); 7.5262 (0.78); 7.5038 (2.55); 7.5006 (1.14); 7.4886 (1.66); 7.4848 (3.17);

7.4714 (0.50); 7.4673 (1.22); 7.4638 (0.70); 7.3316 (4.68); 7.1725 (1.12); 7.1543 (1.28); 7.1436 (0.59); 7.1407 (0.51); 7.1244 (1.16); 7.1045

(0.72); 7.1014 (0.62); 6.8819 (0.97); 6.8636 (1.65); 6.8466 (0.74); 6.8450 (0.74); 6.8173 (1.68); 6.7970 (1.50); 5.3395 (6.05); 4.8670 (7.56);

3.3370 (92.18); 3.0230 (16.00); 2.8901 (8.26); 2.7317 (6.57); 2.7308 (6.65); 2.5249 (0.64); 2.5115 (13.25); 2.5071 (26.45); 2.5025 (34.92);

2.4979 (25.57); 2.4934 (12.40); 2.2229 (10.86); −0.0002 (2.10)

›Example 214, Solvent: DMSO, Spectrometer: 300.16 MHz

9.8147 (0.73); 8.1638 (0.91); 7.8000 (0.36); 7.7861 (0.35); 7.7719 (0.62); 7.7626 (0.45); 7.7487 (0.78); 7.7326 (0.75); 7.7087 (0.33); 7.6790

(0.62); 7.6607 (0.76); 7.6492 (0.75); 7.6382 (0.36); 7.6311 (0.69); 7.3100 (0.73); 7.2803 (1.54); 7.2737 (2.64); 7.2706 (2.35); 7.2509 (0.63);

7.1221 (0.49); 7.1190 (0.49); 7.0993 (0.41); 5.2502 (1.74); 5.1466 (0.34); 4.0590 (0.32); 4.0353 (0.33); 2.5332 (0.71); 2.5274 (1.48); 2.5215

(2.02); 2.5155 (1.48); 2.5098 (0.72); 2.0079 (1.37); 1.4982 (1.79); 1.4791 (16.00); 1.3561 (0.34); 1.2163 (0.37); 1.1926 (0.73); 1.1688 (0.36)

›Example 215, Solvent: DMSO, Spectrometer: 400.13 MHz

10.2011 (3.15); 7.8365 (0.44); 7.8155 (2.34); 7.8071 (2.56); 7.8010 (5.59); 7.7862 (0.48); 7.5384 (2.33); 7.5234 (0.69); 7.5189 (0.59); 7.5143

(0.99); 7.5111 (1.03); 7.5017 (0.95); 7.3894 (0.34); 7.3699 (2.52); 7.3580 (3.35); 7.3560 (3.24); 7.0972 (1.36); 7.0908 (1.34); 7.0829 (1.18);

7.0765 (1.29); 5.7684 (0.63); 5.3282 (6.96); 4.1125 (2.20); 4.0959 (4.67); 4.0793 (2.24); 3.4034 (2.72); 3.3533 (187.35); 3.3261 (0.66); 3.3033

(2.15); 3.0728 (0.40); 3.0584 (16.00); 2.6788 (0.36); 2.5643 (0.55); 2.5598 (0.76); 2.5553 (0.54); 2.5320 (0.95); 2.5183 (21.78); 2.5142 (44.85);

2.5098 (60.71); 2.5054 (44.01); 2.4688 (0.41); 2.4643 (0.59); 2.4598 (0.70); 2.4552 (0.51); 2.3375 (11.57); 1.6317 (0.47); 1.6147 (1.51); 1.6083

(0.56); 1.5973 (1.94); 1.5776 (1.60); 1.5609 (0.66); 1.4187 (0.34); 1.4000 (1.17); 1.3810 (1.87); 1.3622 (1.88); 1.3440 (1.11); 1.3258 (0.33);

0.9317 (4.32); 0.9134 (8.71); 0.8949 (3.74)

›Example 216, Solvent: DMSO, Spectrometer: 399.95 MHz

12.5582 (1.05); 7.9544 (1.11); 7.7470 (0.32); 7.7413 (2.15); 7.7387 (2.76); 7.7347 (1.32); 7.7262 (0.86); 7.7210 (3.62); 7.7172 (2.52); 7.5674

(0.49); 7.5560 (0.36); 7.5491 (1.76); 7.5432 (0.51); 7.5344 (0.97); 7.5310 (1.57); 7.5275 (0.78); 7.5049 (2.60); 7.5016 (1.11); 7.4899 (1.71);

7.4859 (3.25); 7.4721 (0.83); 7.4683 (1.54); 7.4629 (4.55); 7.4574 (1.28); 7.4458 (1.34); 7.4403 (4.55); 7.4316 (0.41); 7.3404 (4.75); 6.9039

(0.43); 6.8952 (4.38); 6.8896 (1.27); 6.8781 (1.27); 6.8725 (4.02); 6.8638 (0.35); 5.3399 (5.85); 5.0656 (0.39); 5.0491 (1.47); 5.0325 (1.49);

5.0160 (0.40); 3.3352 (22.31); 3.0226 (16.00); 3.0128 (0.57); 2.8912 (8.97); 2.7333 (7.30); 2.5220 (0.50); 2.5135 (6.25); 2.5090 (12.45); 2.5044

(16.32); 2.4998 (11.74); 2.4953 (5.52); 1.5486 (5.61); 1.5321 (5.54); −0.0002 (6.50)

›Example 217, Solvent: DMSO, Spectrometer: 399.95 MHz

10.7035 (2.17); 8.1584 (1.52); 8.1385 (1.80); 8.0607 (0.41); 8.0534 (3.55); 8.0483 (1.09); 8.0362 (1.12); 8.0310 (3.79); 8.0237 (0.39); 7.9032

(2.27); 7.8982 (0.43); 7.8814 (2.19); 7.8633 (1.17); 7.7391 (1.86); 7.7365 (2.49); 7.7326 (1.22); 7.7239 (0.74); 7.7188 (3.28); 7.7150 (2.28);

7.5676 (0.47); 7.5558 (0.34); 7.5493 (1.59); 7.5436 (0.49); 7.5344 (0.85); 7.5310 (1.40); 7.5276 (0.72); 7.5015 (2.31); 7.4981 (1.00); 7.4862

(1.56); 7.4824 (2.94); 7.4689 (0.47); 7.4648 (1.19); 7.4615 (0.66); 7.3845 (0.61); 7.3625 (0.68); 7.2064 (1.66); 7.1889 (1.60); 7.0537 (0.41);

7.0465 (3.74); 7.0413 (1.12); 7.0350 (0.33); 7.0281 (2.08); 7.0241 (3.79); 7.0167 (0.40); 7.0109 (0.36); 7.0057 (1.09); 6.9765 (0.68); 6.9545

(0.58); 5.4143 (5.66); 3.8499 (0.99); 3.8405 (16.00); 3.8284 (0.59); 3.8236 (5.06); 3.7995 (0.60); 3.7894 (2.83); 3.3430 (69.40); 3.0831 (15.12);

2.9456 (2.95); 2.8910 (2.46); 2.7848 (0.45); 2.7498 (0.58); 2.7325 (1.96); 2.7313 (1.94); 2.5261 (0.61); 2.5213 (0.96); 2.5127 (12.40); 2.5082

(24.80); 2.5036 (32.75); 2.4990 (23.81); 2.4945 (11.31); −0.0002 (2.77)

›Example 218, Solvent: DMSO, Spectrometer: 399.95 MHz

10.4625 (2.01); 8.0034 (1.43); 7.9831 (1.88); 7.9533 (0.39); 7.8580 (1.31); 7.8387 (1.79); 7.8185 (1.11); 7.7185 (2.58); 7.7147 (1.24); 7.7058

(0.86); 7.7007 (3.40); 7.6969 (2.40); 7.5632 (0.49); 7.5511 (0.36); 7.5449 (1.63); 7.5393 (0.48); 7.5299 (0.86); 7.5266 (1.40); 7.5232 (0.72);

7.5071 (1.65); 7.5030 (2.25); 7.4932 (2.71); 7.4896 (2.35); 7.4861 (2.95); 7.4836 (2.50); 7.4778 (1.97); 7.4741 (3.20); 7.4605 (0.51); 7.4564

(1.26); 7.4533 (0.72); 7.3952 (0.80); 7.3909 (1.14); 7.3864 (0.48); 7.3738 (3.05); 7.3698 (1.30); 7.3554 (2.17); 7.3495 (0.42); 7.3454 (0.89);

7.3416 (1.60); 7.3378 (0.87); 7.3309 (0.47); 7.3241 (1.43); 7.3059 (0.37); 7.1874 (1.78); 7.1696 (1.70); 5.3745 (6.07); 5.0204 (3.59); 3.3353

(28.56); 3.3316 (77.85); 3.2150 (0.44); 3.0702 (0.39); 3.0548 (16.00); 2.8903 (3.14); 2.7319 (2.49); 2.7309 (2.46); 2.5251 (0.63); 2.5203 (1.02);

2.5118 (13.84); 2.5073 (27.81); 2.5027 (36.70); 2.4981 (26.57); 2.4935 (12.61); 0.0079 (0.46); −0.0002 (13.90); −0.0086 (0.42)

›Example 219, Solvent: DMSO, Spectrometer: 399.95 MHz

12.3592 (1.32); 7.9533 (0.68); 7.7409 (1.96); 7.7382 (2.70); 7.7343 (1.37); 7.7258 (0.85); 7.7206 (3.52); 7.7168 (2.52); 7.5664 (0.50); 7.5631

(0.33); 7.5549 (0.36); 7.5480 (1.71); 7.5422 (0.55); 7.5334 (0.96); 7.5299 (1.57); 7.5264 (0.83); 7.5038 (2.57); 7.5005 (1.17); 7.4888 (1.66);

7.4848 (3.19); 7.4714 (0.58); 7.4673 (1.33); 7.4638 (0.78); 7.3323 (4.48); 7.0164 (0.90); 7.0128 (1.01); 6.9962 (1.87); 6.9925 (1.84); 6.9649

(0.89); 6.9599 (1.00); 6.9477 (1.11); 6.9428 (1.33); 6.9275 (0.64); 6.9226 (0.78); 6.8840 (0.56); 6.8792 (0.83); 6.8640 (2.19); 6.8592 (1.79);

6.8513 (1.54); 6.8476 (1.51); 6.8341 (1.13); 6.8304 (1.24); 6.8141 (0.47); 6.8102 (0.46); 5.3384 (5.74); 4.9686 (0.39); 4.9521 (1.50); 4.9354

(1.53); 4.9188 (0.43); 3.7803 (15.50); 3.3322 (39.87); 3.0186 (16.00); 2.8903 (5.50); 2.7322 (4.29); 2.7310 (4.44); 2.5254 (0.43); 2.5206 (0.68);

2.5120 (8.09); 2.5075 (16.53); 2.5029 (22.20); 2.4983 (16.46); 2.4938 (8.35); 1.5410 (5.49); 1.5244 (5.58); −0.0002 (4.39)

›Example 220, Solvent: DMSO, Spectrometer: 400.13 MHz

7.7516 (2.80); 7.7338 (3.40); 7.7300 (2.55); 7.5760 (0.59); 7.5729 (0.47); 7.5645 (0.53); 7.5576 (1.83); 7.5519 (0.74); 7.5428 (1.18); 7.5396

(1.71); 7.5363 (1.09); 7.5131 (3.48); 7.5098 (2.53); 7.4980 (2.72); 7.4941 (4.04); 7.4868 (1.96); 7.4809 (1.58); 7.4765 (2.09); 7.4665 (2.66);

7.4470 (2.14); 7.3462 (2.33); 7.3286 (2.42); 5.7603 (5.19); 5.3835 (3.93); 4.0432 (0.38); 4.0253 (0.38); 3.3241 (11.73); 3.2913 (0.73); 3.0156

(16.00); 2.5157 (10.03); 2.5114 (19.41); 2.5069 (25.78); 2.5025 (18.91); 2.4982 (9.74); 1.9934 (1.62); 1.2390 (0.35); 1.1972 (0.47); 1.1794

(0.87); 1.1616 (0.44)

›Example 221, Solvent: DMSO, Spectrometer: 399.95 MHz

9.7726 (1.32); 8.0140 (1.09); 7.9940 (1.36); 7.8377 (0.93); 7.8186 (1.24); 7.7982 (0.83); 7.7246 (1.90); 7.7207 (0.96); 7.7120 (0.61); 7.7068

(2.55); 7.7030 (1.73); 7.5640 (0.34); 7.5457 (1.16); 7.5400 (0.39); 7.5308 (0.62); 7.5274 (1.00); 7.5241 (0.54); 7.4960 (1.77); 7.4927 (0.77);

7.4806 (1.22); 7.4769 (2.26); 7.4633 (0.36); 7.4592 (0.90); 7.4560 (0.51); 7.1523 (1.24); 7.1347 (1.19); 5.3791 (4.39); 3.3293 (39.08); 3.0881

(0.67); 3.0728 (10.99); 2.8909 (1.10); 2.7321 (0.82); 2.7314 (0.83); 2.5252 (0.36); 2.5204 (0.60); 2.5119 (7.76); 2.5074 (15.47); 2.5028 (20.42);

2.4982 (14.82); 2.4937 (7.08); 1.6926 (0.46); 1.6739 (1.57); 1.6552 (1.66); 1.6367 (0.54); 1.2342 (0.41); 1.1827 (16.00); 0.8759 (0.37); 0.7918

(1.95); 0.7734 (4.41); 0.7546 (1.80); −0.0002 (5.77)

›Example 222, Solvent: DMSO, Spectrometer: 399.95 MHz

8.5738 (2.41); 7.9525 (1.26); 7.9479 (1.67); 7.9270 (2.16); 7.8491 (1.43); 7.8301 (1.83); 7.8097 (1.07); 7.6954 (2.56); 7.6917 (1.25); 7.6822

(3.74); 7.6772 (5.94); 7.6741 (2.68); 7.6205 (2.37); 7.5997 (3.24); 7.5619 (0.50); 7.5497 (0.38); 7.5436 (1.66); 7.5380 (0.48); 7.5285 (0.88);

7.5252 (1.38); 7.5219 (0.68); 7.4951 (2.62); 7.4901 (3.70); 7.4744 (3.09); 7.4716 (3.48); 7.4692 (2.48); 7.4579 (0.52); 7.4539 (1.24); 7.4508

(0.69); 7.1560 (1.77); 7.1376 (1.72); 5.3008 (6.18); 3.3416 (164.31); 3.0054 (16.00); 2.8912 (9.12); 2.7323 (7.55); 2.5258 (0.81); 2.5209 (1.29);

2.5124 (15.83); 2.5079 (31.43); 2.5033 (41.17); 2.4987 (29.73); 2.4942 (14.01); 1.6912 (0.88); 1.6804 (2.43); 1.6730 (2.57); 1.6628 (0.91);

1.2167 (1.03); 1.2064 (2.45); 1.1990 (2.45); 1.1883 (0.87); −0.0002 (4.60)

›Example 223, Solvent: DMSO, Spectrometer: 400.13 MHz

10.0714 (2.63); 7.8267 (0.37); 7.8057 (2.13); 7.7975 (2.44); 7.7913 (5.42); 7.7766 (0.48); 7.5376 (2.16); 7.5222 (0.62); 7.5175 (0.54); 7.5136

(0.92); 7.5102 (0.98); 7.5046 (0.59); 7.5008 (0.90); 7.4962 (0.66); 7.3885 (0.33); 7.3694 (2.27); 7.3634 (1.53); 7.3575 (3.16); 7.3550 (3.12);

7.0922 (1.26); 7.0856 (1.22); 7.0779 (1.12); 7.0714 (1.20); 5.7640 (3.25); 5.3237 (6.55); 4.9274 (0.43); 4.9146 (0.58); 4.9121 (0.58); 4.9061

(0.55); 4.8993 (0.56); 4.8933 (0.59); 4.8780 (0.44); 3.3275 (11.77); 3.3047 (0.75); 3.0654 (16.00); 2.5322 (0.33); 2.5187 (7.70); 2.5143 (15.83);

2.5098 (21.48); 2.5053 (15.33); 2.5008 (7.18); 2.3394 (10.43); 1.6989 (0.49); 1.6803 (0.60); 1.6636 (0.57); 1.6472 (0.36); 1.5939 (0.54); 1.5791

(0.43); 1.5725 (0.56); 1.5592 (0.89); 1.5448 (0.60); 1.5382 (0.70); 1.5234 (0.54); 1.3592 (0.64); 1.3469 (0.71); 1.3391 (0.60); 1.3259 (0.94);

1.3126 (0.53); 1.3048 (0.55); 1.2923 (0.52); 1.2477 (0.81); 1.2371 (6.90); 1.2216 (6.73); 0.9042 (9.66); 0.9030 (9.64); 0.8876 (9.68); 0.8652

(0.97); 0.8475 (0.40)

›Example 224, Solvent: DMSO, Spectrometer: 400.13 MHz

10.1980 (3.39); 7.8358 (0.41); 7.8147 (2.34); 7.8062 (2.58); 7.8002 (5.62); 7.7854 (0.50); 7.5391 (2.45); 7.5237 (0.72); 7.5147 (1.02); 7.5115

(1.07); 7.5019 (1.01); 7.3891 (0.34); 7.3697 (2.62); 7.3573 (3.50); 7.0973 (1.39); 7.0910 (1.36); 7.0829 (1.22); 7.0766 (1.33); 5.7683 (4.33);

5.3284 (7.17); 4.1036 (2.10); 4.0868 (4.54); 4.0701 (2.17); 3.4000 (1.14); 3.3497 (84.51); 3.3260 (0.53); 3.2994 (1.10); 3.0734 (0.39); 3.0591

(16.00); 2.5646 (0.34); 2.5601 (0.45); 2.5319 (0.57); 2.5141 (30.36); 2.5097 (41.01); 2.5054 (29.94); 2.4686 (0.34); 2.4639 (0.48); 2.4595 (0.56);

2.4550 (0.38); 2.3375 (11.99); 1.9964 (0.43); 1.6310 (1.02); 1.6137 (1.65); 1.5967 (1.19); 1.5796 (0.38); 1.3485 (1.17); 1.3380 (2.06); 1.3307

(4.06); 1.3216 (3.23); 1.3127 (2.74); 1.2510 (0.54); 0.9036 (2.02); 0.8863 (5.30); 0.8686 (1.84); 0.8643 (1.22); 0.8462 (0.38)

›Example 225, Solvent: DMSO, Spectrometer: 399.95 MHz

10.1956 (2.22); 7.8322 (0.50); 7.8112 (1.95); 7.7954 (3.65); 7.7935 (3.12); 7.7773 (0.55); 7.7256 (2.01); 7.7229 (2.56); 7.7191 (1.23); 7.7104

(0.83); 7.7052 (3.34); 7.7015 (2.26); 7.5628 (0.49); 7.5510 (0.39); 7.5445 (1.63); 7.5387 (0.49); 7.5296 (0.90); 7.5262 (1.42); 7.5228 (0.72);

7.4959 (2.39); 7.4925 (1.00); 7.4806 (1.70); 7.4768 (3.04); 7.4633 (0.51); 7.4591 (1.21); 7.4559 (0.65); 7.1031 (1.30); 7.0981 (1.30); 7.0874

(1.19); 7.0824 (1.22); 5.3352 (6.27); 3.8862 (4.75); 3.8695 (4.79); 3.3373 (121.73); 3.0652 (16.00); 2.8909 (2.35); 2.7322 (1.87); 2.7312 (1.83);

2.5254 (0.77); 2.5121 (14.62); 2.5076 (29.05); 2.5030 (38.16); 2.4984 (27.63); 2.4938 (13.18); 1.9416 (0.40); 1.9248 (0.83); 1.9081 (1.06);

1.8913 (0.85); 1.8746 (0.43); 1.2347 (0.32); 0.9272 (14.67); 0.9104 (14.23); 0.8980 (0.66); −0.0002 (6.10)

›Example 226, Solvent: DMSO, Spectrometer: 400.13 MHz

10.2218 (3.02); 7.8377 (0.71); 7.8167 (1.86); 7.7995 (2.39); 7.7932 (2.26); 7.7901 (2.53); 7.7724 (0.83); 7.7692 (0.58); 7.7302 (2.78); 7.7171

(0.84); 7.7122 (3.46); 7.7085 (2.45); 7.5686 (0.50); 7.5656 (0.32); 7.5566 (0.40); 7.5503 (1.73); 7.5447 (0.53); 7.5353 (0.95); 7.5321 (1.45);

7.5289 (0.75); 7.5016 (2.50); 7.4859 (1.73); 7.4823 (3.19); 7.4686 (0.49); 7.4647 (1.20); 7.4616 (0.70); 7.1152 (1.49); 7.1120 (1.51); 7.0981

(1.44); 7.0949 (1.40); 5.7683 (0.91); 5.3344 (6.56); 4.9204 (0.64); 4.9051 (1.36); 4.8896 (1.37); 4.8743 (0.63); 3.4000 (1.26); 3.3505 (106.77);

3.3008 (1.03); 3.0791 (16.00); 2.9380 (1.30); 2.9314 (3.01); 2.9249 (1.33); 2.5636 (0.42); 2.5591 (0.59); 2.5546 (0.47); 2.5499 (0.35); 2.5375

(2.16); 2.5314 (2.82); 2.5183 (17.62); 2.5142 (34.59); 2.5097 (45.30); 2.5052 (32.26); 2.5009 (15.00); 2.4645 (0.37); 2.4599 (0.48); 2.4556

(0.38); 1.3707 (0.74); 1.3200 (6.79); 1.3042 (6.76)

›Example 227, Solvent: DMSO, Spectrometer: 399.95 MHz

10.3769 (2.12); 8.0203 (1.54); 8.0001 (2.07); 7.9530 (0.94); 7.8853 (1.40); 7.8659 (1.92); 7.8458 (1.15); 7.7280 (2.72); 7.7151 (0.85); 7.7101

(3.50); 7.7063 (2.50); 7.5663 (0.50); 7.5631 (0.33); 7.5543 (0.38); 7.5479 (1.73); 7.5423 (0.51); 7.5329 (0.91); 7.5297 (1.46); 7.5264 (0.77);

7.4980 (2.53); 7.4824 (1.75); 7.4788 (3.27); 7.4651 (0.54); 7.4611 (1.29); 7.4580 (0.74); 7.3286 (0.71); 7.3242 (0.87); 7.3064 (1.40); 7.2330

(0.75); 7.2286 (0.63); 7.2166 (2.17); 7.2123 (3.66); 7.2078 (2.41); 7.2021 (2.00); 7.1943 (3.30); 7.1863 (0.89); 7.1709 (0.38); 5.4621 (2.62);

5.3902 (6.51); 4.3243 (0.42); 4.3113 (0.77); 4.2972 (0.89); 4.2828 (0.88); 4.2702 (0.49); 3.9033 (0.48); 3.8924 (0.66); 3.8846 (0.59); 3.8744

(0.88); 3.8645 (0.55); 3.8567 (0.57); 3.8458 (0.46); 3.3316 (69.84); 3.0853 (0.63); 3.0755 (16.00); 2.9850 (0.34); 2.9798 (0.33); 2.9566 (0.44);

2.9434 (0.54); 2.9387 (0.53); 2.9261 (0.38); 2.8903 (7.59); 2.8083 (0.40); 2.7962 (0.71); 2.7836 (0.44); 2.7549 (0.48); 2.7313 (6.08); 2.5248

(0.66); 2.5115 (13.88); 2.5070 (27.45); 2.5024 (36.12); 2.4978 (26.26); 2.4934 (12.61); −0.0002 (8.08)

›Example 228, Solvent: DMSO, Spectrometer: 400.13 MHz

10.3312 (2.87); 7.8479 (0.61); 7.8269 (1.78); 7.8098 (2.61); 7.8066 (2.36); 7.8027 (2.46); 7.7855 (0.71); 7.7818 (0.44); 7.4213 (1.02); 7.4013

(2.19); 7.3813 (1.58); 7.2835 (1.46); 7.2813 (1.28); 7.2640 (1.21); 7.2619 (1.00); 7.2465 (1.57); 7.2407 (1.98); 7.2365 (1.36); 7.1432 (1.10);

7.1415 (1.15); 7.1369 (1.03); 7.1352 (0.99); 7.1227 (2.32); 7.1200 (2.09); 7.1060 (1.36); 7.1023 (1.31); 5.7685 (0.68); 5.3409 (5.98); 4.1955

(1.97); 4.1789 (4.28); 4.1622 (1.97); 3.7894 (16.00); 3.3943 (0.40); 3.3449 (25.89); 3.0753 (0.38); 3.0602 (14.66); 2.9234 (1.30); 2.9168 (2.93);

2.9102 (1.37); 2.5796 (1.18); 2.5729 (1.25); 2.5630 (2.80); 2.5563 (2.68); 2.5463 (1.26); 2.5396 (1.16); 2.5322 (0.65); 2.5186 (9.84); 2.5143

(19.78); 2.5099 (26.44); 2.5054 (18.87); 2.5011 (8.77); 2.4605 (0.33)

›Example 229, Solvent: DMSO, Spectrometer: 399.95 MHz

12.3982 (0.67); 7.9527 (0.74); 7.7410 (2.02); 7.7384 (2.73); 7.7344 (1.32); 7.7260 (0.80); 7.7208 (3.54); 7.7170 (2.45); 7.5667 (0.50); 7.5634

(0.33); 7.5553 (0.35); 7.5483 (1.74); 7.5425 (0.52); 7.5337 (0.95); 7.5303 (1.58); 7.5268 (0.78); 7.5048 (2.58); 7.5013 (1.09); 7.4897 (1.64);

7.4857 (3.18); 7.4724 (0.49); 7.4682 (1.26); 7.4647 (0.69); 7.3301 (4.81); 7.1016 (2.47); 7.0812 (2.92); 6.8624 (0.45); 6.8550 (3.93); 6.8498

(1.19); 6.8384 (1.10); 6.8334 (3.31); 5.3406 (5.96); 4.7940 (7.63); 3.6954 (0.43); 3.3486 (86.86); 3.0357 (0.38); 3.0206 (16.00); 3.0111 (0.61);

2.8904 (6.12); 2.7322 (4.75); 2.7312 (4.80); 2.5261 (0.45); 2.5213 (0.71); 2.5127 (8.80); 2.5082 (17.65); 2.5036 (23.41); 2.4990 (16.97); 2.4944

(8.04); 2.2230 (10.05); −0.0002 (1.03)

›Example 230, Solvent: DMSO, Spectrometer: 399.95 MHz

10.9090 (2.21); 8.0883 (1.25); 8.0676 (1.49); 7.8495 (1.30); 7.8301 (1.82); 7.8100 (1.21); 7.7200 (2.78); 7.7162 (1.39); 7.7070 (0.93); 7.7022

(3.52); 7.6984 (2.50); 7.5604 (0.50); 7.5573 (0.33); 7.5484 (0.38); 7.5419 (1.68); 7.5364 (0.51); 7.5271 (0.91); 7.5238 (1.45); 7.5205 (0.76);

7.4927 (2.53); 7.4772 (1.75); 7.4735 (3.21); 7.4599 (0.51); 7.4558 (1.25); 7.4527 (0.73); 7.3123 (1.16); 7.2942 (3.15); 7.2753 (2.45); 7.2162

(1.18); 7.2132 (0.91); 7.1978 (1.71); 7.1927 (0.63); 7.1817 (2.96); 7.1784 (3.48); 7.1607 (2.43); 7.1520 (2.10); 7.1328 (1.81); 5.3541 (6.10);

3.3297 (58.71); 3.0519 (16.00); 2.8903 (1.67); 2.7311 (1.34); 2.5248 (0.69); 2.5115 (12.61); 2.5070 (24.94); 2.5025 (32.88); 2.4979 (24.08);

2.4934 (11.66); 2.4261 (0.35); 2.4161 (0.60); 2.4105 (0.54); 2.4004 (0.80); 2.3935 (0.94); 2.3892 (0.84); 2.3775 (1.29); 2.3694 (0.71); 2.3565

(0.66); 1.5034 (0.51); 1.4929 (0.72); 1.4904 (0.69); 1.4804 (0.96); 1.4705 (0.67); 1.4678 (0.69); 1.4574 (0.52); 1.3763 (0.56); 1.3660 (0.62);

1.3602 (0.69); 1.3559 (0.80); 1.3502 (0.74); 1.3460 (0.60); 1.3399 (0.68); 1.3297 (0.48); 0.8756 (0.43); −0.0002 (6.50)

›Example 231, Solvent: DMSO, Spectrometer: 399.95 MHz

10.7963 (2.26); 8.0278 (1.31); 8.0071 (1.72); 7.9529 (0.79); 7.8784 (1.37); 7.8590 (1.92); 7.8389 (1.17); 7.7282 (2.93); 7.7245 (1.59); 7.7104

(3.62); 7.7067 (2.63); 7.5691 (0.52); 7.5660 (0.37); 7.5570 (0.41); 7.5505 (1.74); 7.5452 (0.57); 7.5357 (0.96); 7.5325 (1.52); 7.5293 (0.84);

7.5006 (2.64); 7.4851 (1.91); 7.4814 (3.34); 7.4613 (2.30); 7.4575 (1.90); 7.4416 (1.73); 7.4377 (1.73); 7.2908 (0.73); 7.2868 (0.73); 7.2700

(1.27); 7.2685 (1.29); 7.2663 (1.15); 7.2514 (0.99); 7.2474 (0.93); 7.2101 (1.99); 7.1916 (1.89); 7.0172 (1.50); 7.0144 (1.78); 6.9963 (1.41);

6.9935 (1.50); 6.9875 (1.16); 6.9843 (0.97); 6.9681 (1.66); 6.9652 (1.45); 6.9492 (0.86); 6.9460 (0.79); 5.3872 (6.51); 5.1665 (0.33); 5.1503

(1.11); 5.1337 (1.11); 5.1174 (0.35); 3.3803 (0.39); 3.3414 (130.53); 3.0658 (16.00); 3.0355 (0.46); 2.8907 (6.04); 2.7314 (5.07); 2.5258 (0.73);

2.5123 (14.56); 2.5080 (28.22); 2.5035 (36.82); 2.4989 (27.18); 2.4945 (13.39); 1.5828 (5.84); 1.5664 (5.80); −0.0002 (1.18)

›Example 232, Solvent: DMSO, Spectrometer: 399.95 MHz

10.7787 (1.95); 8.0189 (1.31); 7.9983 (1.69); 7.9532 (0.55); 7.8653 (1.35); 7.8461 (1.83); 7.8258 (1.16); 7.7272 (2.57); 7.7234 (1.25); 7.7145

(0.74); 7.7094 (3.36); 7.7057 (2.40); 7.5689 (0.48); 7.5569 (0.35); 7.5506 (1.66); 7.5449 (0.47); 7.5356 (0.85); 7.5323 (1.41); 7.5289 (0.72);

7.5003 (2.42); 7.4970 (1.03); 7.4848 (1.62); 7.4811 (3.12); 7.4675 (0.47); 7.4635 (1.23); 7.4603 (0.70); 7.2993 (1.74); 7.2941 (0.64); 7.2795

(2.38); 7.2775 (2.63); 7.2642 (0.73); 7.2592 (2.22); 7.1981 (1.82); 7.1803 (1.74); 6.9484 (0.98); 6.9463 (0.76); 6.9304 (2.22); 6.9270 (3.58);

6.9243 (3.02); 6.9093 (1.68); 6.9048 (3.02); 5.3845 (6.13); 5.0933 (0.33); 5.0770 (1.15); 5.0605 (1.16); 5.0441 (0.33); 3.3446 (117.32); 3.0603

(16.00); 2.8909 (4.49); 2.7323 (3.65); 2.7313 (3.50); 2.5261 (0.52); 2.5214 (0.82); 2.5128 (11.33); 2.5083 (23.02); 2.5037 (30.58); 2.4991

(22.28); 2.4946 (10.69); 1.5360 (5.77); 1.5196 (5.72); −0.0002 (0.43)

›Example 233, Solvent: DMSO, Spectrometer: 400.13 MHz

9.8433 (1.76); 7.8017 (0.42); 7.7807 (1.17); 7.7635 (1.52); 7.7578 (1.37); 7.7544 (1.57); 7.7368 (0.69); 7.7329 (1.58); 7.7303 (1.75); 7.7264

(0.84); 7.7177 (0.51); 7.7125 (2.21); 7.7088 (1.56); 7.5515 (1.08); 7.5458 (0.33); 7.5366 (0.58); 7.5332 (0.95); 7.5299 (0.48); 7.5030 (1.56);

7.4997 (0.69); 7.4876 (1.05); 7.4839 (1.99); 7.4662 (0.78); 7.4630 (0.45); 7.0807 (0.91); 7.0773 (0.93); 7.0637 (0.88); 7.0603 (0.87); 5.7638

(0.90); 5.3261 (4.14); 3.3823 (0.95); 3.3324 (57.48); 3.3086 (0.49); 3.2824 (0.64); 3.0700 (10.61); 2.5275 (0.43); 2.5189 (6.42); 2.5144 (13.43);

2.5099 (18.41); 2.5054 (13.05); 2.5009 (6.05); 1.7497 (0.75); 1.7375 (0.59); 1.7292 (0.73); 1.7186 (0.63); 1.7080 (0.96); 1.4418 (16.00); 1.4017

(0.48); 1.3916 (0.52); 1.3827 (0.66); 1.3716 (1.01); 1.3611 (0.63); 1.3542 (0.40); 1.3419 (0.43); 0.9098 (1.87); 0.8917 (3.99); 0.8732 (1.65)

›Example 234, Solvent: DMSO, Spectrometer: 400.13 MHz

12.5653 (1.63); 7.6272 (1.07); 7.6216 (1.06); 7.6183 (0.95); 7.6151 (1.26); 7.6116 (0.90); 7.6064 (0.94); 7.5956 (2.93); 7.5705 (0.78); 7.5564

(0.88); 7.5503 (1.17); 7.5360 (1.22); 7.5309 (0.70); 7.5152 (0.52); 7.4333 (0.58); 7.4306 (0.62); 7.4271 (0.56); 7.4243 (0.54); 7.4096 (1.04);

7.4050 (0.96); 7.3916 (4.93); 7.0153 (1.26); 6.9969 (1.68); 6.9946 (1.59); 6.9161 (0.66); 6.9085 (0.87); 6.9015 (0.93); 6.8938 (1.45); 6.8896

(0.57); 6.8817 (0.73); 6.8746 (1.81); 6.8634 (4.76); 6.8593 (2.94); 6.8484 (1.09); 6.8444 (0.87); 5.7631 (5.16); 5.3684 (5.98); 5.1570 (1.07);

5.1486 (1.99); 5.1388 (1.10); 4.4380 (2.18); 4.4330 (2.40); 4.4277 (2.64); 3.3982 (3.66); 3.3484 (263.44); 3.2987 (2.86); 3.0116 (16.00); 2.6771

(0.37); 2.5622 (0.63); 2.5578 (0.87); 2.5533 (0.67); 2.5486 (0.42); 2.5303 (1.19); 2.5168 (23.67); 2.5125 (47.68); 2.5081 (63.56); 2.5037 (45.37);

2.4994 (21.41); 2.4630 (0.55); 2.4585 (0.70); 2.4539 (0.50); 2.3350 (0.37)

›Example 235, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5169 (2.26); 8.0834 (1.34); 8.0627 (1.59); 7.8340 (1.29); 7.8147 (1.83); 7.7945 (1.19); 7.7230 (2.73); 7.7101 (0.89); 7.7051 (3.54); 7.7014

(2.49); 7.5638 (0.51); 7.5607 (0.33); 7.5519 (0.39); 7.5455 (1.69); 7.5399 (0.52); 7.5305 (0.92); 7.5272 (1.45); 7.5239 (0.75); 7.4957 (2.49);

7.4801 (1.78); 7.4765 (3.19); 7.4628 (0.52); 7.4588 (1.25); 7.4557 (0.72); 7.1443 (1.87); 7.1264 (1.80); 5.3554 (6.40); 5.0926 (0.44); 5.0895

(0.38); 5.0780 (0.74); 5.0747 (0.89); 5.0603 (0.39); 5.0572 (0.44); 3.3279 (52.28); 3.0528 (16.00); 2.5251 (0.72); 2.5118 (12.64); 2.5073 (24.46);

2.5028 (31.75); 2.4982 (23.07); 2.4937 (11.05); 2.3968 (0.66); 2.3814 (0.71); 2.3618 (0.95); 2.3463 (1.02); 2.2453 (0.94); 2.2253 (1.06); 2.2104

(0.64); 2.1902 (0.73); 1.9797 (0.75); 1.9619 (1.27); 1.9440 (1.28); 1.9270 (0.84); 1.9093 (0.43); 1.6557 (0.55); 1.6297 (6.45); 1.5525 (7.37);

1.3547 (0.33); 1.3376 (0.44); 1.3332 (0.36); 1.3208 (0.49); 1.3150 (0.44); 1.3068 (0.36); 1.2996 (0.41); 1.1983 (0.48); 1.1857 (0.51); 1.1785

(0.43); 1.1718 (0.32); 1.1637 (0.48); 0.9019 (5.82); 0.8853 (5.69); 0.0079 (0.36); −0.0002 (8.83)

›Example 236, Solvent: CDCl3, Spectrometer: 300.16 MHz

7.6688 (4.49); 7.6461 (5.37); 7.4378 (7.28); 7.4124 (7.11); 7.3906 (3.09); 7.2619 (12.61); 6.5633 (2.62); 6.5419 (2.50); 6.3065 (2.64); 6.2784

(2.51); 5.2285 (10.11); 4.4256 (1.25); 3.7686 (1.43); 3.1067 (16.00); 2.0868 (0.99); 1.7385 (3.38); 1.6955 (5.73); 1.6524 (4.11); 1.4633 (1.09);

1.4367 (2.16); 1.4101 (2.73); 1.3263 (1.92); 1.2933 (2.12); 1.2537 (2.36); 1.2075 (2.41); 1.1744 (12.09); 1.1557 (10.90); 0.9880 (0.76); 0.9493

(1.94); 0.9057 (2.30); 0.8694 (1.58); −0.0002 (8.47)

›Example 237, Solvent: DMSO, Spectrometer: 399.95 MHz

10.9450 (1.79); 8.0365 (0.79); 8.0157 (1.02); 7.9532 (0.86); 7.9012 (1.37); 7.8819 (1.86); 7.8617 (1.11); 7.7234 (2.67); 7.7197 (1.31); 7.7106

(0.79); 7.7056 (3.43); 7.7018 (2.42); 7.5661 (0.48); 7.5541 (0.35); 7.5477 (1.63); 7.5421 (0.49); 7.5327 (0.86); 7.5295 (1.40); 7.5261 (0.74);

7.4977 (2.43); 7.4822 (1.67); 7.4785 (3.12); 7.4649 (0.48); 7.4609 (1.21); 7.4578 (0.71); 7.2230 (1.81); 7.2048 (1.73); 5.3795 (6.53); 3.6620

(0.59); 3.6342 (1.83); 3.6063 (1.88); 3.5784 (0.64); 3.3291 (63.12); 3.0552 (16.00); 2.8907 (6.74); 2.7312 (5.41); 2.5251 (0.64); 2.5117 (12.44);

2.5072 (24.80); 2.5027 (32.66); 2.4981 (23.87); 2.4936 (11.50); 0.0080 (0.36); −0.0002 (10.95); −0.0085 (0.34)

›Example 238, Solvent: DMSO, Spectrometer: 399.95 MHz

10.2540 (2.69); 7.9534 (0.87); 7.8225 (0.71); 7.8015 (1.78); 7.7841 (2.12); 7.7740 (2.08); 7.7714 (2.26); 7.7533 (0.82); 7.7504 (0.62); 7.7227

(2.70); 7.7099 (0.85); 7.7049 (3.49); 7.7011 (2.48); 7.5631 (0.51); 7.5600 (0.33); 7.5513 (0.38); 7.5448 (1.71); 7.5392 (0.52); 7.5299 (1.01);

7.5266 (1.51); 7.5233 (0.77); 7.4991 (4.62); 7.4958 (3.54); 7.4781 (6.63); 7.4631 (0.53); 7.4590 (1.26); 7.4558 (0.73); 7.2932 (4.02); 7.2767

(1.37); 7.2722 (3.31); 7.2602 (0.56); 7.2438 (0.49); 7.1047 (1.54); 7.1018 (1.53); 7.0873 (1.51); 7.0844 (1.44); 5.3312 (6.46); 4.2908 (1.61);

4.2741 (3.64); 4.2575 (1.66); 3.3302 (61.62); 3.0610 (16.00); 2.9281 (1.43); 2.9115 (2.95); 2.8907 (7.28); 2.7320 (5.51); 2.5252 (0.69); 2.5203

(1.10); 2.5118 (13.33); 2.5073 (26.35); 2.5028 (34.64); 2.4982 (25.35); 2.4937 (12.29); 1.2348 (0.35); −0.0002 (7.26)

›Example 239, Solvent: DMSO, Spectrometer: 399.95 MHz

11.9040 (0.97); 7.9531 (0.94); 7.7274 (2.91); 7.7146 (0.91); 7.7096 (3.62); 7.7058 (2.54); 7.5600 (0.51); 7.5570 (0.33); 7.5486 (0.41); 7.5417

(1.78); 7.5360 (0.53); 7.5269 (1.04); 7.5237 (1.56); 7.5203 (0.80); 7.4973 (2.67); 7.4819 (1.89); 7.4781 (3.33); 7.4646 (0.59); 7.4606 (1.30);

7.4571 (0.81); 7.4380 (0.67); 7.4328 (1.09); 7.4264 (0.64); 7.4159 (4.82); 7.4127 (5.70); 7.3966 (3.78); 7.3915 (1.18); 7.3817 (1.87); 7.3773

(1.49); 7.3713 (1.12); 7.3661 (1.38); 7.3596 (0.79); 7.3494 (1.08); 7.2723 (4.67); 5.2853 (6.47); 5.2229 (8.16); 5.1615 (0.81); 3.3291 (51.70);

3.0358 (0.47); 3.0245 (16.00); 2.8903 (7.20); 2.7315 (5.92); 2.5245 (0.76); 2.5112 (13.86); 2.5068 (26.69); 2.5023 (34.48); 2.4977 (24.97);

2.4933 (11.96); 0.0078 (0.44); −0.0002 (11.95); −0.0085 (0.41)

›Example 240, Solvent: DMSO, Spectrometer: 399.95 MHz

9.9471 (2.07); 8.0542 (1.28); 8.0335 (1.59); 7.8817 (1.33); 7.8623 (1.94); 7.8422 (1.14); 7.7245 (2.73); 7.7067 (3.47); 7.7030 (2.51); 7.5643

(0.51); 7.5611 (0.34); 7.5523 (0.38); 7.5460 (1.68); 7.5403 (0.54); 7.5310 (0.95); 7.5277 (1.46); 7.5244 (0.79); 7.4962 (2.52); 7.4806 (1.84);

7.4770 (3.22); 7.4633 (0.54); 7.4593 (1.26); 7.4563 (0.76); 7.1912 (1.89); 7.1730 (1.82); 5.3689 (6.74); 4.0933 (8.50); 3.5200 (2.54); 3.5037

(5.27); 3.4873 (2.59); 3.3292 (45.74); 3.0719 (16.00); 2.5251 (0.59); 2.5117 (11.15); 2.5073 (21.82); 2.5028 (28.55); 2.4982 (21.20); 2.4939

(10.54); 1.5736 (0.45); 1.5563 (1.48); 1.5500 (0.55); 1.5397 (1.95); 1.5199 (1.60); 1.5036 (0.68); 1.3975 (0.36); 1.3791 (1.22); 1.3599 (1.86);

1.3410 (1.85); 1.3231 (1.07); 0.9122 (4.40); 0.8938 (8.76); 0.8753 (3.72); −0.0002 (6.95)

›Example 241, Solvent: DMSO, Spectrometer: 400.13 MHz

11.0140 (2.97); 7.8384 (4.05); 7.8278 (4.28); 7.7290 (2.77); 7.7111 (3.50); 7.7074 (2.47); 7.5694 (0.51); 7.5573 (0.43); 7.5511 (1.72); 7.5455

(0.54); 7.5360 (0.97); 7.5328 (1.47); 7.5013 (2.53); 7.4857 (1.86); 7.4822 (3.20); 7.4645 (1.38); 7.1630 (1.30); 7.1526 (2.13); 7.1421 (1.21);

5.3565 (6.72); 3.3941 (2.10); 3.3443 (171.35); 3.2941 (1.27); 3.0619 (16.00); 2.7990 (4.33); 2.7824 (4.46); 2.6813 (0.43); 2.6768 (0.57); 2.6724

(0.42); 2.5619 (0.91); 2.5575 (1.22); 2.5531 (0.95); 2.5300 (2.04); 2.5164 (37.35); 2.5122 (74.24); 2.5077 (98.29); 2.5033 (70.37); 2.4991

(33.42); 2.4575 (0.92); 2.3391 (0.46); 2.3346 (0.62); 2.3301 (0.45); 1.9948 (0.65); 1.8223 (0.43); 1.8056 (0.89); 1.7889 (1.12); 1.7723 (0.88);

1.7557 (0.46); 1.2508 (1.44); 1.1793 (0.36); 0.9545 (15.44); 0.9379 (14.90); 0.8796 (0.72); 0.8630 (2.05); 0.8454 (0.82)

›Example 242, Solvent: DMSO, Spectrometer: 400.13 MHz

10.3887 (3.15); 7.8550 (0.86); 7.8342 (1.87); 7.8162 (2.05); 7.7966 (2.48); 7.7948 (2.52); 7.7760 (1.23); 7.7282 (2.99); 7.7104 (3.74); 7.7067

(2.70); 7.5669 (0.57); 7.5639 (0.42); 7.5549 (0.54); 7.5487 (1.82); 7.5431 (0.67); 7.5336 (1.15); 7.5305 (1.62); 7.5272 (0.92); 7.5000 (2.72);

7.4843 (2.16); 7.4809 (3.42); 7.4670 (0.76); 7.4632 (1.41); 7.4601 (0.87); 7.1345 (1.79); 7.1168 (1.76); 5.4326 (0.42); 5.4274 (0.42); 5.4159

(1.21); 5.4107 (1.23); 5.3992 (1.28); 5.3939 (1.27); 5.3824 (0.50); 5.3771 (0.46); 5.3418 (6.76); 3.5850 (3.39); 3.5798 (3.32); 3.3971 (1.47);

3.3474 (119.76); 3.2970 (1.75); 3.0759 (16.00); 2.5573 (0.96); 2.5531 (0.92); 2.5160 (20.07); 2.5121 (37.07); 2.5077 (47.62); 2.5033 (34.71);

2.4669 (1.05); 2.4619 (1.10); 2.4575 (1.10); 1.4870 (7.01); 1.4702 (7.01)

›Example 243, Solvent: DMSO, Spectrometer: 399.95 MHz

11.0967 (2.79); 8.1639 (0.70); 8.1437 (0.81); 7.9529 (1.48); 7.9305 (1.31); 7.9110 (2.06); 7.8911 (1.16); 7.7277 (3.18); 7.7097 (3.91); 7.7062

(3.10); 7.6940 (1.91); 7.6920 (1.87); 7.6743 (2.06); 7.6722 (1.98); 7.5647 (0.57); 7.5464 (1.96); 7.5386 (1.44); 7.5335 (1.77); 7.5319 (1.78);

7.5283 (1.98); 7.5250 (1.41); 7.5197 (2.13); 7.5155 (2.11); 7.4974 (2.92); 7.4786 (4.49); 7.4634 (2.81); 7.4607 (3.30); 7.4449 (1.16); 7.4423

(1.04); 7.4186 (1.26); 7.4140 (1.24); 7.3991 (1.53); 7.3950 (1.49); 7.3804 (0.71); 7.3760 (0.64); 7.2413 (2.07); 7.2226 (1.98); 5.3754 (5.29);

3.3476 (114.40); 3.0811 (16.00); 2.8913 (9.58); 2.7324 (8.25); 2.5081 (34.57); 2.5037 (43.87); 2.4993 (33.49); 0.0004 (1.58)

›Example 244, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5103 (2.00); 8.0958 (1.42); 8.0752 (1.70); 7.8354 (1.27); 7.8162 (1.79); 7.7959 (1.18); 7.7275 (2.12); 7.7251 (2.63); 7.7214 (1.29); 7.7124

(0.85); 7.7073 (3.45); 7.7036 (2.42); 7.5647 (0.50); 7.5615 (0.32); 7.5527 (0.38); 7.5464 (1.68); 7.5407 (0.51); 7.5314 (0.91); 7.5281 (1.45);

7.5247 (0.74); 7.4967 (2.44); 7.4933 (1.08); 7.4812 (1.74); 7.4775 (3.16); 7.4639 (0.50); 7.4598 (1.26); 7.4566 (0.71); 7.1478 (1.80); 7.1293

(1.75); 5.3607 (6.17); 3.3304 (51.56); 3.0569 (16.00); 2.8913 (2.07); 2.7326 (1.71); 2.7316 (1.59); 2.6846 (0.33); 2.6713 (0.58); 2.6677 (0.64);

2.6491 (0.56); 2.6326 (0.37); 2.5256 (0.59); 2.5124 (10.74); 2.5079 (21.06); 2.5033 (27.53); 2.4987 (19.99); 2.4942 (9.54); 1.6099 (0.33);

1.5995 (0.35); 1.5872 (0.44); 1.5781 (0.42); 1.5653 (0.36); 1.3496 (0.35); 1.3367 (0.45); 1.3236 (0.56); 1.3051 (0.59); 1.2898 (0.92); 1.2785

(0.91); 1.2718 (1.20); 1.2549 (1.30); 1.2459 (1.04); 1.2354 (1.03); 1.2217 (0.82); 1.2152 (0.61); 1.2044 (0.54); 1.1962 (0.43); 1.1881 (0.47);

1.1733 (0.35); 1.0670 (5.83); 1.0500 (5.71); 0.8578 (2.10); 0.8528 (1.20); 0.8406 (4.59); 0.8225 (2.41); −0.0002 (8.32)

›Example 245, Solvent: DMSO, Spectrometer: 400.13 MHz

10.9988 (2.86); 8.1622 (1.92); 8.1415 (2.35); 8.0503 (4.12); 8.0457 (1.56); 8.0332 (1.65); 8.0288 (4.52); 7.9336 (1.40); 7.9142 (2.11); 7.8942

(1.28); 7.7393 (2.94); 7.7213 (3.60); 7.7176 (2.71); 7.5949 (4.60); 7.5904 (1.65); 7.5734 (4.59); 7.5601 (0.66); 7.5536 (1.93); 7.5480 (0.76);

7.5353 (1.64); 7.5054 (2.70); 7.4861 (3.43); 7.4684 (1.34); 7.2443 (2.11); 7.2257 (2.05); 5.7612 (6.52); 5.4213 (7.01); 4.0422 (0.33); 4.0246

(0.35); 3.3685 (1.08); 3.3365 (221.52); 3.2583 (0.71); 3.0816 (16.00); 2.6758 (0.34); 2.5112 (43.36); 2.5068 (57.28); 2.5025 (42.19); 2.3337

(0.39); 1.9934 (1.44); 1.2382 (0.42); 1.1967 (0.40); 1.1790 (0.76); 1.1612 (0.40)

›Example 246, Solvent: DMSO, Spectrometer: 400.13 MHz

9.8610 (1.10); 7.8194 (0.75); 7.8141 (0.34); 7.8059 (0.88); 7.7970 (0.84); 7.7887 (0.44); 7.7831 (1.42); 7.7696 (1.10); 7.7668 (1.53); 7.3587

(0.78); 7.3366 (1.43); 7.3144 (0.71); 7.0800 (0.51); 7.0749 (0.51); 7.0645 (0.49); 7.0594 (0.49); 5.3185 (2.53); 3.5596 (0.87); 3.4011 (0.37);

3.3516 (32.11); 3.0680 (5.99); 2.5186 (2.03); 2.5142 (4.23); 2.5098 (5.74); 2.5053 (4.09); 2.5009 (1.88); 1.9957 (0.47); 1.5107 (1.98); 1.4682

(16.00); 1.3330 (0.37)

›Example 247, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5085 (0.85); 8.0766 (0.49); 8.0559 (0.58); 7.8330 (0.50); 7.8136 (0.70); 7.7935 (0.46); 7.7240 (1.04); 7.7111 (0.35); 7.7061 (1.35); 7.7024

(0.95); 7.5458 (0.66); 7.5308 (0.35); 7.5275 (0.56); 7.4964 (0.97); 7.4809 (0.68); 7.4772 (1.23); 7.4595 (0.48); 7.1416 (0.72); 7.1235 (0.69);

5.3540 (2.48); 3.3285 (24.24); 3.0542 (6.16); 2.8910 (1.65); 2.7320 (1.33); 2.5118 (4.89); 2.5074 (9.68); 2.5028 (12.76); 2.4982 (9.38); 2.4938

(4.60); 2.3677 (0.59); 2.3494 (1.23); 2.3308 (0.71); 1.5627 (0.37); 1.5435 (0.40); 1.5403 (0.41); 1.5309 (0.33); 1.5206 (0.40); 1.1837 (0.76);

1.1733 (0.44); 1.1633 (0.44); 1.1604 (0.45); 1.1525 (0.41); 1.1410 (0.61); 0.8623 (16.00); −0.0002 (3.48)

›Example 248, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5134 (2.17); 8.0921 (1.60); 8.0715 (1.88); 7.8348 (1.33); 7.8153 (1.96); 7.7952 (1.26); 7.7243 (2.91); 7.7114 (0.95); 7.7064 (3.73); 7.7028

(2.63); 7.5650 (0.51); 7.5619 (0.36); 7.5529 (0.40); 7.5466 (1.72); 7.5410 (0.57); 7.5316 (0.94); 7.5284 (1.48); 7.5252 (0.83); 7.4972 (2.69);

7.4815 (1.85); 7.4779 (3.35); 7.4642 (0.53); 7.4603 (1.27); 7.4573 (0.78); 7.1461 (2.00); 7.1276 (1.90); 5.3601 (6.80); 3.3344 (89.79); 3.0882

(0.49); 3.0572 (16.00); 2.8911 (1.68); 2.7316 (1.43); 2.7087 (0.35); 2.6892 (0.60); 2.6725 (0.79); 2.6579 (0.40); 2.5121 (13.08); 2.5078 (25.41);

2.5033 (33.14); 2.4987 (24.36); 2.4944 (11.93); 1.5898 (0.51); 1.5852 (0.43); 1.5755 (0.53); 1.5692 (0.61); 1.5639 (0.43); 1.5543 (0.60); 1.3273

(0.48); 1.3148 (0.63); 1.3019 (0.92); 1.2826 (1.32); 1.2684 (1.74); 1.2577 (0.88); 1.2491 (1.38); 1.2339 (1.28); 1.2207 (0.45); 1.2161 (0.50);

1.2088 (0.34); 1.0653 (6.44); 1.0483 (6.34); 0.8939 (0.36); 0.8785 (3.29); 0.8607 (6.20); 0.8428 (2.44); −0.0002 (5.41)

›Example 249, Solvent: DMSO, Spectrometer: 400.13 MHz

9.8213 (1.22); 7.7724 (0.82); 7.7568 (1.83); 7.6494 (0.32); 7.3888 (0.69); 7.3835 (0.80); 7.3760 (1.13); 7.3667 (0.78); 7.0218 (0.59); 7.0175

(0.58); 7.0059 (0.55); 7.0015 (0.55); 5.7640 (2.62); 5.3195 (2.87); 3.3401 (6.83); 3.3237 (6.22); 2.5124 (0.98); 2.5081 (1.27); 2.5039 (0.93);

1.4639 (16.00)

›Example 250, Solvent: DMSO, Spectrometer: 400.13 MHz

10.0917 (2.65); 7.8295 (0.49); 7.8085 (1.97); 7.7927 (4.08); 7.7746 (0.63); 7.5387 (2.38); 7.5231 (0.70); 7.5145 (1.00); 7.5110 (1.06); 7.5015

(1.00); 7.4972 (0.75); 7.3893 (0.36); 7.3701 (2.46); 7.3640 (1.77); 7.3580 (3.41); 7.3557 (3.30); 7.0915 (1.40); 7.0866 (1.35); 7.0759 (1.29);

7.0710 (1.30); 5.7642 (4.65); 5.3254 (6.89); 4.6816 (0.44); 4.6690 (0.53); 4.6590 (0.83); 4.6495 (0.61); 4.6366 (0.41); 3.3277 (10.72); 3.3053

(0.96); 3.0626 (16.00); 2.5185 (9.24); 2.5142 (18.30); 2.5098 (24.34); 2.5054 (17.56); 2.5012 (8.48); 2.3398 (11.18); 1.8755 (0.86); 1.8628

(0.98); 1.8494 (1.02); 1.7352 (0.85); 1.7269 (0.92); 1.7121 (1.00); 1.5277 (0.44); 1.5175 (0.47); 1.4974 (0.52); 1.4711 (0.43); 1.4632 (0.40);

1.4391 (1.00); 1.4143 (1.27); 1.3887 (1.27); 1.3616 (1.14); 1.3359 (0.90); 1.3296 (0.97); 1.3116 (0.40); 1.3038 (0.53); 1.2830 (0.47); 1.2533

(0.80); 0.8655 (0.36)

›Example 251, Solvent: DMSO, Spectrometer: 399.95 MHz

12.7560 (0.76); 8.1825 (1.92); 8.1772 (0.82); 8.1689 (2.16); 8.1656 (1.14); 8.1602 (2.17); 8.1521 (0.87); 8.1466 (1.97); 7.9535 (1.88); 7.7488

(2.02); 7.7462 (2.70); 7.7422 (1.34); 7.7338 (0.84); 7.7286 (3.47); 7.7247 (2.44); 7.5689 (0.47); 7.5576 (0.34); 7.5505 (1.66); 7.5446 (0.52);

7.5359 (0.94); 7.5325 (1.53); 7.5290 (0.79); 7.5082 (2.52); 7.5048 (1.13); 7.4932 (1.63); 7.4892 (3.11); 7.4759 (0.52); 7.4717 (1.23); 7.4681

(0.73); 7.4076 (1.98); 7.4024 (0.69); 7.3849 (5.55); 7.3684 (0.71); 7.3632 (1.90); 5.3844 (5.92); 3.3476 (122.79); 3.0193 (16.00); 2.8918 (14.81);

2.7330 (11.98); 2.5269 (0.67); 2.5136 (12.10); 2.5091 (23.58); 2.5045 (30.73); 2.4999 (22.31); 2.4954 (10.72); −0.0002 (1.49)

›Example 252, Solvent: DMSO, Spectrometer: 400.13 MHz

12.4342 (2.00); 7.6225 (3.81); 7.6020 (4.37); 7.3495 (0.58); 7.3451 (0.47); 7.3298 (4.03); 7.3240 (4.71); 7.3162 (14.21); 7.3074 (5.07); 7.2870

(3.71); 7.2772 (1.63); 7.2672 (6.35); 7.2557 (1.44); 7.2512 (1.07); 7.2419 (0.83); 7.2344 (0.41); 5.3051 (7.02); 3.7517 (8.42); 3.5607 (1.00);

3.4211 (3.15); 3.3715 (269.39); 3.3219 (2.90); 3.0017 (16.00); 2.5572 (0.56); 2.5120 (34.30); 2.5077 (43.77); 2.5036 (32.56); 2.4582 (0.55);

2.3524 (11.36); 1.9931 (0.71); 1.2476 (0.82); 1.1775 (0.37); 0.8772 (0.35); 0.8606 (0.95); 0.8429 (0.40)

›Example 253, Solvent: DMSO, Spectrometer: 400.13 MHz

7.7389 (2.92); 7.7211 (3.54); 7.7173 (2.65); 7.5620 (0.56); 7.5588 (0.43); 7.5503 (0.49); 7.5436 (1.77); 7.5379 (0.68); 7.5288 (1.08); 7.5255

(1.60); 7.4986 (2.75); 7.4832 (1.93); 7.4795 (3.36); 7.4659 (0.69); 7.4619 (1.34); 7.4586 (0.89); 7.3839 (1.23); 7.3657 (1.59); 7.3632 (1.60);

7.3451 (1.37); 6.5154 (0.75); 6.5021 (1.44); 6.4870 (2.65); 6.4691 (2.05); 6.3994 (2.02); 6.3787 (1.97); 5.7616 (1.11); 5.1994 (6.87); 3.3396

(118.89); 3.2708 (0.67); 3.2506 (0.44); 3.2314 (1.07); 3.2146 (1.87); 3.1992 (1.83); 3.1821 (1.04); 3.0738 (16.00); 3.0481 (0.42); 2.5158 (11.06);

2.5116 (21.74); 2.5072 (29.16); 2.5028 (21.84); 1.7043 (1.28); 1.6690 (1.94); 1.6248 (1.72); 1.5917 (0.78); 1.4442 (0.43); 1.4240 (0.81); 1.4072

(1.97); 1.3886 (2.16); 1.3716 (1.33); 1.3634 (0.65); 1.3410 (0.49); 1.3329 (0.58); 1.3253 (0.56); 1.3162 (0.61); 1.3073 (0.56); 1.2990 (0.49);

1.2898 (0.44); 1.2803 (0.33); 1.2390 (0.50); 1.2303 (0.43); 1.1985 (0.95); 1.1688 (1.44); 1.1466 (1.69); 1.1261 (0.88); 1.0957 (0.50); 0.9179

(0.61); 0.8891 (1.28); 0.8609 (1.22); 0.8373 (0.49)

›Example 254, Solvent: DMSO, Spectrometer: 400.13 MHz

9.8576 (1.05); 7.7899 (0.86); 7.7808 (0.98); 7.7751 (2.20); 7.5367 (0.39); 7.5328 (0.43); 7.0999 (0.53); 7.0938 (0.54); 7.0854 (0.48); 7.0792

(0.54); 5.7642 (3.14); 5.3711 (2.61); 3.3398 (7.33); 3.1915 (6.87); 2.5176 (0.35); 2.5131 (0.76); 2.5086 (1.07); 2.5041 (0.79); 2.4996 (0.40);

1.4703 (16.00)

›Example 255, Solvent: DMSO, Spectrometer: 399.95 MHz

10.8720 (1.81); 8.0114 (0.77); 7.9907 (0.97); 7.9537 (0.52); 7.8515 (1.29); 7.8323 (1.71); 7.8119 (1.13); 7.7329 (1.93); 7.7301 (2.57); 7.7262

(1.29); 7.7176 (0.83); 7.7124 (3.41); 7.7087 (2.43); 7.5678 (0.49); 7.5646 (0.32); 7.5559 (0.36); 7.5495 (1.61); 7.5437 (0.51); 7.5346 (0.86);

7.5312 (1.42); 7.5278 (0.74); 7.5005 (2.37); 7.4971 (1.10); 7.4852 (1.60); 7.4814 (3.01); 7.4679 (0.47); 7.4638 (1.21); 7.4605 (0.69); 7.2920

(0.46); 7.2840 (0.55); 7.2776 (0.56); 7.2695 (0.98); 7.2615 (0.63); 7.2559 (0.88); 7.2455 (0.79); 7.2339 (1.15); 7.2222 (1.13); 7.2112 (0.77);

7.1995 (0.76); 7.1839 (0.60); 7.1761 (2.23); 7.1640 (0.82); 7.1590 (1.89); 7.1574 (1.95); 7.1457 (0.48); 5.3814 (5.89); 4.1094 (0.35); 4.0916

(0.35); 3.8350 (3.84); 3.7363 (0.35); 3.7328 (0.35); 3.3305 (59.82); 3.2301 (0.36); 3.0667 (16.00); 3.0574 (0.36); 2.8909 (4.28); 2.7325 (3.42);

2.7312 (3.33); 2.5256 (0.69); 2.5208 (1.11); 2.5123 (11.54); 2.5078 (22.78); 2.5031 (29.97); 2.4985 (21.65); 2.4940 (10.19); 1.2029 (0.40);

1.1851 (0.83); 1.1673 (0.39); 0.8761 (0.50); −0.0002 (7.11)

›Example 256, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5588 (1.92); 8.0692 (1.21); 8.0485 (1.45); 7.8364 (1.30); 7.8171 (1.80); 7.7969 (1.20); 7.7262 (2.15); 7.7241 (2.67); 7.7112 (0.85); 7.7062

(3.58); 7.7024 (2.41); 7.5647 (0.49); 7.5528 (0.37); 7.5464 (1.67); 7.5406 (0.51); 7.5314 (0.91); 7.5281 (1.42); 7.5248 (0.73); 7.4973 (2.50);

7.4819 (1.74); 7.4782 (3.15); 7.4646 (0.50); 7.4605 (1.24); 7.4573 (0.68); 7.1464 (1.79); 7.1280 (1.75); 5.8644 (0.63); 5.8549 (0.33); 5.8485

(0.32); 5.8386 (0.87); 5.8217 (0.87); 5.8119 (0.36); 5.8055 (0.37); 5.7959 (0.74); 5.7799 (0.35); 5.3561 (6.42); 5.0796 (0.48); 5.0755 (1.20);

5.0709 (1.22); 5.0668 (0.48); 5.0366 (0.43); 5.0325 (1.08); 5.0279 (1.09); 5.0238 (0.43); 4.9832 (0.55); 4.9801 (1.14); 4.9779 (0.90); 4.9753

(1.00); 4.9723 (0.46); 4.9576 (0.52); 4.9545 (1.08); 4.9523 (0.85); 4.9498 (0.95); 4.9467 (0.42); 3.3290 (56.17); 3.2234 (0.36); 3.0878 (0.60);

3.0535 (16.00); 2.8908 (0.51); 2.7320 (0.42); 2.5252 (0.64); 2.5118 (12.37); 2.5073 (22.99); 2.5027 (29.47); 2.4981 (21.39); 2.4934 (12.11);

2.4732 (2.16); 2.3493 (0.70); 2.3335 (1.76); 2.3301 (1.78); 2.3172 (1.20); 2.3140 (1.54); 2.2975 (0.45); 0.8758 (0.48); −0.0002 (4.83)

›Example 257, Solvent: DMSO, Spectrometer: 399.95 MHz

12.7279 (1.12); 8.0919 (2.68); 8.0786 (0.91); 8.0740 (3.13); 8.0705 (2.35); 7.9533 (1.19); 7.7499 (2.15); 7.7474 (2.71); 7.7434 (1.32); 7.7349

(0.91); 7.7297 (3.52); 7.7259 (2.47); 7.6618 (0.34); 7.6589 (0.57); 7.6559 (0.35); 7.6454 (0.48); 7.6406 (1.62); 7.6357 (0.53); 7.6250 (0.78);

7.6220 (1.22); 7.6189 (0.67); 7.5652 (2.44); 7.5580 (0.66); 7.5499 (2.75); 7.5453 (3.65); 7.5360 (1.22); 7.5324 (1.96); 7.5275 (1.71); 7.5086

(2.58); 7.5053 (1.14); 7.4937 (1.71); 7.4896 (3.16); 7.4763 (0.54); 7.4721 (1.26); 7.4685 (0.76); 7.3803 (4.21); 5.3865 (6.20); 3.3487 (150.38);

3.3096 (0.39); 3.0226 (16.00); 2.8916 (9.19); 2.7329 (7.61); 2.5267 (0.71); 2.5133 (12.92); 2.5089 (24.83); 2.5043 (31.99); 2.4997 (23.15);

2.4953 (11.06); −0.0002 (0.54)

›Example 258, Solvent: CDCl3, Spectrometer: 300.16 MHz

7.9129 (1.78); 7.8851 (2.27); 7.7253 (1.47); 7.6987 (2.54); 7.6693 (3.25); 7.6447 (3.33); 7.6240 (2.67); 7.3467 (4.08); 7.3191 (3.66); 7.2968

(4.19); 7.2573 (12.26); 7.2301 (3.45); 7.1347 (2.37); 7.1087 (4.54); 7.0814 (2.29); 7.0233 (2.66); 6.9986 (2.51); 5.2777 (10.06); 4.4296 (2.48);

4.4069 (5.17); 4.3840 (2.68); 3.0953 (16.00); 3.0239 (2.57); 3.0012 (4.99); 2.9786 (2.43); 2.0084 (2.01); 1.6038 (6.29); 1.2541 (0.52); −0.0002

(3.01)

›Example 259, Solvent: DMSO, Spectrometer: 400.13 MHz

7.8120 (1.89); 7.8066 (0.85); 7.7985 (2.10); 7.7932 (1.15); 7.7895 (2.11); 7.7815 (0.87); 7.7761 (1.92); 7.3987 (1.28); 7.3804 (1.66); 7.3783

(1.62); 7.3599 (1.42); 7.3477 (2.07); 7.3424 (0.74); 7.3255 (3.68); 7.3207 (0.88); 7.3086 (0.65); 7.3033 (1.83); 6.5061 (1.83); 6.4886 (1.76);

6.3893 (1.87); 6.3693 (1.81); 6.0030 (2.81); 5.7558 (11.12); 5.1716 (6.65); 4.9644 (0.41); 3.4636 (2.31); 3.3258 (9.38); 3.3020 (0.35); 3.1338

(0.43); 3.0837 (16.00); 3.0284 (0.43); 2.5097 (1.31); 2.5053 (2.76); 2.5007 (3.79); 2.4963 (2.70); 2.4919 (1.26); 1.5326 (2.59)

›Example 260, Solvent: DMSO, Spectrometer: 399.95 MHz

10.8357 (2.17); 8.0093 (1.23); 7.9887 (1.63); 7.9531 (0.80); 7.8678 (1.35); 7.8486 (1.80); 7.8283 (1.14); 7.7300 (1.97); 7.7275 (2.60); 7.7237

(1.26); 7.7149 (0.79); 7.7098 (3.45); 7.7060 (2.40); 7.5698 (0.49); 7.5579 (0.36); 7.5515 (1.65); 7.5459 (0.49); 7.5365 (0.87); 7.5332 (1.42);

7.5299 (0.73); 7.5015 (2.40); 7.4980 (1.01); 7.4860 (1.69); 7.4823 (3.10); 7.4687 (0.50); 7.4646 (1.24); 7.4614 (0.70); 7.3514 (0.36); 7.3425

(4.16); 7.3369 (1.23); 7.3255 (1.31); 7.3199 (4.66); 7.3109 (0.40); 7.2029 (1.76); 7.1852 (1.71); 6.9558 (0.42); 6.9469 (4.37); 6.9413 (1.26);

6.9299 (1.19); 6.9243 (3.92); 6.9154 (0.32); 5.3843 (5.98); 5.0701 (1.07); 5.0536 (1.08); 3.3514 (102.16); 3.3486 (139.13); 3.0611 (16.00);

2.8914 (6.58); 2.7327 (5.16); 2.7319 (5.05); 2.5266 (0.64); 2.5133 (13.11); 2.5088 (25.99); 2.5042 (34.16); 2.4996 (24.71); 2.4951 (11.70);

1.5354 (5.41); 1.5190 (5.40); −0.0002 (0.56)

›Example 261, Solvent: DMSO, Spectrometer: 400.13 MHz

8.0043 (0.53); 7.9848 (0.33); 7.6324 (0.57); 7.4997 (0.41); 7.4808 (0.48); 7.4447 (0.51); 7.4255 (0.41); 5.8276 (1.62); 5.5018 (1.32); 3.4021

(1.07); 3.1184 (3.35); 2.5758 (4.24); 2.5714 (8.61); 2.5669 (11.56); 2.5624 (8.20); 2.5580 (3.77); 1.5267 (0.57); 1.4096 (16.00)

›Example 262, Solvent: DMSO, Spectrometer: 399.95 MHz

12.8129 (1.57); 7.9526 (1.61); 7.7914 (2.80); 7.7865 (2.81); 7.7412 (2.05); 7.7386 (2.70); 7.7346 (1.31); 7.7262 (0.93); 7.7210 (3.51); 7.7171

(2.39); 7.6968 (2.46); 7.6761 (3.42); 7.5797 (2.16); 7.5747 (2.02); 7.5684 (0.38); 7.5651 (0.59); 7.5590 (1.64); 7.5539 (1.85); 7.5468 (1.72);

7.5410 (0.51); 7.5321 (0.98); 7.5288 (1.53); 7.5253 (0.77); 7.5030 (2.53); 7.4996 (1.07); 7.4879 (1.74); 7.4840 (3.13); 7.4705 (0.54); 7.4664

(1.28); 7.4629 (0.75); 7.4112 (4.10); 5.3639 (5.70); 3.3327 (57.92); 3.3298 (86.16); 3.0374 (16.00); 3.0161 (0.56); 2.8905 (13.13); 2.7315

(10.22); 2.7308 (10.22); 2.5246 (0.96); 2.5198 (1.45); 2.5113 (18.55); 2.5068 (36.83); 2.5022 (48.25); 2.4976 (34.97); 2.4930 (16.60); 0.0079

(0.40); −0.0002 (12.51); −0.0085 (0.40)

›Example 263, Solvent: DMSO, Spectrometer: 399.95 MHz

12.8993 (0.93); 7.8246 (1.47); 7.8192 (1.89); 7.8040 (1.90); 7.7986 (1.52); 7.7462 (2.83); 7.7423 (1.48); 7.7336 (0.90); 7.7285 (3.53); 7.7247

(2.56); 7.6126 (0.33); 7.6068 (0.54); 7.5898 (0.68); 7.5841 (1.07); 7.5785 (0.62); 7.5691 (0.71); 7.5613 (0.67); 7.5582 (0.61); 7.5510 (1.79);

7.5452 (0.57); 7.5363 (0.99); 7.5330 (1.58); 7.5295 (0.87); 7.5083 (2.63); 7.4932 (1.69); 7.4893 (3.22); 7.4759 (0.55); 7.4718 (1.26); 7.4683

(0.75); 7.4245 (3.48); 5.3912 (6.09); 3.3462 (66.87); 3.3416 (98.96); 3.0178 (16.00); 2.8915 (0.44); 2.7322 (0.36); 2.5263 (0.57); 2.5129 (12.95);

2.5085 (25.78); 2.5040 (34.03); 2.4994 (25.26); 2.4950 (12.64); −0.0002 (8.68); −0.0085 (0.33)

›Example 264, Solvent: DMSO, Spectrometer: 399.95 MHz

10.8225 (1.89); 8.0438 (1.01); 8.0231 (1.23); 7.9530 (0.55); 7.8547 (1.32); 7.8354 (1.82); 7.8152 (1.18); 7.7230 (2.64); 7.7192 (1.31); 7.7103

(0.83); 7.7052 (3.52); 7.7015 (2.39); 7.5641 (0.49); 7.5609 (0.32); 7.5522 (0.37); 7.5458 (1.67); 7.5401 (0.50); 7.5308 (0.88); 7.5275 (1.43);

7.5242 (0.73); 7.4962 (2.50); 7.4929 (1.11); 7.4808 (1.67); 7.4770 (3.13); 7.4634 (0.49); 7.4594 (1.24); 7.4562 (0.69); 7.3918 (1.71); 7.3881

(1.77); 7.3794 (1.79); 7.3757 (1.82); 7.1740 (1.80); 7.1560 (1.78); 6.9915 (0.93); 6.9864 (2.04); 6.9830 (1.86); 6.9796 (3.14); 6.9708 (1.01);

6.9671 (2.25); 6.9585 (1.10); 5.3715 (6.28); 3.9564 (5.70); 3.3300 (63.32); 3.2185 (0.68); 3.0543 (16.00); 2.8902 (4.49); 2.7317 (3.51); 2.7309

(3.56); 2.5249 (0.63); 2.5201 (0.99); 2.5116 (11.97); 2.5071 (23.85); 2.5025 (31.51); 2.4979 (22.91); 2.4934 (10.95); 0.8757 (0.44); −0.0002

(7.55)

›Example 265, Solvent: DMSO, Spectrometer: 399.95 MHz

11.7658 (1.42); 7.9531 (0.62); 7.7302 (2.85); 7.7263 (1.44); 7.7174 (1.11); 7.7126 (3.67); 7.7088 (2.49); 7.5624 (0.53); 7.5592 (0.37); 7.5508

(0.42); 7.5440 (1.76); 7.5382 (0.58); 7.5292 (1.07); 7.5259 (1.61); 7.5225 (0.86); 7.5000 (2.80); 7.4848 (1.93); 7.4810 (3.48); 7.4676 (0.62);

7.4634 (1.37); 7.4599 (0.85); 7.2523 (4.15); 5.3572 (0.43); 5.2833 (6.24); 4.1472 (0.63); 4.1312 (0.39); 4.1221 (2.32); 4.1053 (4.91); 4.0886

(2.37); 3.3301 (65.71); 3.0486 (0.70); 3.0299 (16.00); 2.9910 (0.99); 2.8907 (4.72); 2.7321 (3.83); 2.7311 (3.80); 2.5250 (0.70); 2.5117 (13.28);

2.5072 (26.01); 2.5026 (34.09); 2.4981 (24.95); 2.4936 (12.17); 1.6644 (1.22); 1.6472 (2.50); 1.6289 (2.58); 1.6117 (1.30); 1.5937 (0.32);

1.2349 (0.38); 1.1211 (0.61); 1.1058 (0.60); 0.9307 (4.55); 0.9123 (8.73); 0.8937 (3.88); 0.8028 (0.50); 0.7844 (1.04); 0.7658 (0.45); 0.0080

(0.38); −0.0002 (9.93); −0.0085 (0.33)

›Example 266, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5110 (1.78); 8.0783 (1.26); 8.0577 (1.49); 7.8342 (1.26); 7.8150 (1.72); 7.7947 (1.16); 7.7263 (1.91); 7.7238 (2.51); 7.7199 (1.21); 7.7112

(0.74); 7.7060 (3.33); 7.7023 (2.30); 7.5647 (0.47); 7.5528 (0.35); 7.5463 (1.60); 7.5406 (0.47); 7.5314 (0.85); 7.5281 (1.39); 7.5246 (0.70);

7.4973 (2.34); 7.4938 (1.00); 7.4819 (1.59); 7.4781 (3.01); 7.4646 (0.46); 7.4605 (1.20); 7.4573 (0.66); 7.1409 (1.74); 7.1235 (1.68); 5.3553

(6.25); 3.3290 (47.50); 3.0544 (16.00); 2.8908 (0.96); 2.7321 (0.75); 2.7311 (0.74); 2.5252 (0.56); 2.5204 (0.88); 2.5119 (10.17); 2.5074 (20.26);

2.5028 (26.71); 2.4982 (19.34); 2.4937 (9.17); 2.3781 (1.98); 2.3599 (3.85); 2.3416 (2.19); 1.6185 (1.28); 1.6001 (2.48); 1.5817 (2.46); 1.5634

(1.29); 0.9106 (4.18); 0.8922 (8.59); 0.8736 (3.79); −0.0002 (7.17)

›Example 267, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5028 (2.08); 8.0700 (1.21); 8.0493 (1.45); 7.9534 (0.39); 7.8304 (1.26); 7.8112 (1.73); 7.7909 (1.16); 7.7314 (0.32); 7.7257 (1.96); 7.7232

(2.58); 7.7194 (1.25); 7.7106 (0.80); 7.7055 (3.40); 7.7017 (2.36); 7.5637 (0.48); 7.5518 (0.36); 7.5454 (1.62); 7.5397 (0.49); 7.5305 (0.87);

7.5272 (1.41); 7.5237 (0.72); 7.4958 (2.39); 7.4924 (1.03); 7.4804 (1.65); 7.4766 (3.07); 7.4631 (0.48); 7.4590 (1.22); 7.4558 (0.68); 7.1392

(1.76); 7.1215 (1.69); 5.3524 (6.09); 3.3277 (54.17); 3.0520 (16.00); 2.8908 (3.16); 2.7321 (2.47); 2.7311 (2.47); 2.5250 (0.71); 2.5117 (12.59);

2.5072 (24.78); 2.5026 (32.57); 2.4980 (23.61); 2.4935 (11.26); 2.3682 (1.40); 2.3498 (2.77); 2.3311 (1.64); 1.6865 (0.99); 1.6576 (1.98);

1.6362 (0.94); 1.6282 (1.15); 1.6127 (1.04); 1.5935 (1.32); 1.5746 (1.54); 1.5557 (0.98); 1.5369 (0.37); 1.2339 (0.58); 1.2191 (0.45); 1.2073

(0.81); 1.1991 (1.06); 1.1871 (1.49); 1.1753 (1.92); 1.1682 (2.47); 1.1488 (1.75); 1.1384 (1.38); 1.1225 (0.41); 1.1160 (0.56); 1.1098 (0.41);

1.0854 (0.37); 0.8776 (0.44); 0.8487 (0.88); 0.8221 (0.82); 0.0080 (0.35); −0.0002 (9.29)

›Example 268, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5090 (1.95); 8.0719 (1.29); 8.0512 (1.54); 7.8323 (1.29); 7.8129 (1.81); 7.7928 (1.20); 7.7231 (2.74); 7.7194 (1.36); 7.7105 (0.83); 7.7054

(3.62); 7.7016 (2.45); 7.5642 (0.50); 7.5610 (0.32); 7.5523 (0.38); 7.5458 (1.70); 7.5403 (0.50); 7.5310 (0.89); 7.5276 (1.46); 7.5243 (0.75);

7.4964 (2.54); 7.4931 (1.07); 7.4809 (1.71); 7.4772 (3.21); 7.4636 (0.49); 7.4596 (1.26); 7.4564 (0.71); 7.1407 (1.86); 7.1225 (1.78); 5.4108

(0.42); 5.3970 (0.36); 5.3722 (1.59); 5.3543 (6.98); 5.3425 (1.86); 5.3275 (0.64); 5.3037 (0.40); 3.3309 (61.84); 3.0544 (15.69); 2.5257 (0.52);

2.5123 (9.90); 2.5078 (19.67); 2.5032 (25.99); 2.4986 (18.86); 2.4941 (8.99); 2.3961 (1.36); 2.3881 (0.66); 2.3779 (2.62); 2.3594 (1.42); 2.2293

(0.47); 2.2126 (0.72); 2.1962 (0.66); 2.1803 (0.40); 1.9840 (0.57); 1.9671 (1.27); 1.9514 (1.43); 1.9333 (0.76); 1.5991 (0.43); 1.5809 (1.05);

1.5620 (1.35); 1.5431 (1.03); 1.5245 (0.40); 1.3616 (0.47); 1.3423 (1.15); 1.3304 (0.77); 1.3239 (1.47); 1.3046 (0.97); 1.2858 (0.52); 0.9309

(16.00); 0.9140 (15.65); 0.8974 (2.18); 0.8808 (2.11); 0.8758 (0.68); 0.8623 (0.34); −0.0002 (4.98)

›Example 269, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5931 (2.29); 8.0375 (0.71); 8.0168 (0.91); 7.8905 (1.34); 7.8712 (1.86); 7.8510 (1.15); 7.7298 (2.70); 7.7260 (1.34); 7.7170 (0.83); 7.7120

(3.50); 7.7082 (2.49); 7.6176 (1.63); 7.6137 (1.68); 7.5979 (1.77); 7.5940 (1.73); 7.5684 (0.50); 7.5564 (0.37); 7.5500 (1.70); 7.5444 (0.50);

7.5351 (0.92); 7.5318 (1.47); 7.5284 (0.75); 7.5010 (2.47); 7.4976 (1.08); 7.4855 (1.75); 7.4818 (3.20); 7.4681 (0.52); 7.4641 (1.27); 7.4609

(0.72); 7.3529 (0.73); 7.3489 (0.73); 7.3341 (1.08); 7.3319 (1.25); 7.3284 (1.04); 7.3137 (0.96); 7.3097 (0.90); 7.2140 (1.82); 7.1956 (1.75);

7.0479 (1.50); 7.0448 (1.61); 7.0271 (1.37); 7.0240 (1.34); 6.9440 (1.01); 6.9407 (0.92); 6.9248 (1.54); 6.9218 (1.48); 6.9058 (0.86); 6.9025

(0.78); 5.3871 (6.33); 4.9188 (5.58); 3.3532 (60.00); 3.3473 (97.95); 3.0723 (16.00); 2.8909 (0.53); 2.7323 (0.35); 2.5261 (0.64); 2.5128 (12.51);

2.5083 (24.48); 2.5038 (31.93); 2.4992 (23.20); 2.4947 (11.08); −0.0002 (2.55)

›Example 270, Solvent: DMSO, Spectrometer: 400.13 MHz

10.2536 (4.91); 7.8306 (1.24); 7.8097 (2.96); 7.7922 (3.54); 7.7818 (3.38); 7.7790 (3.75); 7.7611 (1.42); 7.7581 (1.12); 7.7247 (4.46); 7.7208

(2.20); 7.7120 (1.48); 7.7069 (5.89); 7.7032 (4.08); 7.5784 (0.45); 7.5752 (0.81); 7.5720 (0.55); 7.5635 (0.64); 7.5569 (2.82); 7.5511 (0.86);

7.5421 (1.61); 7.5387 (2.50); 7.5353 (1.30); 7.5105 (4.22); 7.4952 (2.79); 7.4914 (5.22); 7.4779 (0.82); 7.4738 (2.04); 7.4704 (1.14); 7.3147

(16.00); 7.3037 (15.02); 7.2946 (0.69); 7.2901 (0.42); 7.2849 (0.47); 7.2820 (0.53); 7.2560 (0.44); 7.2465 (1.26); 7.2360 (1.87); 7.2252 (1.99);

7.2149 (1.08); 7.2034 (0.48); 7.1002 (2.50); 7.0973 (2.55); 7.0828 (2.42); 7.0799 (2.35); 5.3435 (10.41); 4.3087 (2.93); 4.2915 (6.69); 4.2743

(3.04); 4.0612 (0.38); 4.0434 (1.16); 4.0256 (1.17); 4.0078 (0.39); 3.5201 (1.32); 3.5020 (4.61); 3.4839 (4.65); 3.4655 (1.48); 3.4124 (9.03);

3.4045 (0.68); 3.3977 (0.59); 3.3625 (697.57); 3.3126 (8.07); 3.3005 (0.40); 3.2629 (0.33); 2.9537 (2.84); 2.9365 (6.03); 2.9193 (2.75); 2.6835

(0.42); 2.6789 (0.57); 2.6744 (0.42); 2.5688 (0.33); 2.5643 (0.78); 2.5597 (1.16); 2.5552 (0.87); 2.5509 (0.49); 2.5323 (1.56); 2.5275 (2.67);

2.5189 (34.24); 2.5144 (71.95); 2.5099 (98.33); 2.5054 (69.91); 2.5009 (32.16); 2.4691 (0.51); 2.4645 (0.86); 2.4599 (1.17); 2.4555 (0.90);

2.4509 (0.51); 2.3413 (0.45); 2.3368 (0.62); 2.3321 (0.45); 1.9958 (5.24); 1.3701 (0.42); 1.2841 (0.40); 1.2510 (1.87); 1.1982 (1.46); 1.1804

(2.85); 1.1626 (1.39); 1.0513 (5.25); 1.0332 (12.20); 1.0150 (5.20); 0.8804 (0.89); 0.8637 (2.97); 0.8461 (1.12)

›Example 271, Solvent: DMSO, Spectrometer: 399.95 MHz

12.1189 (1.60); 7.9530 (0.48); 7.7432 (0.33); 7.7374 (2.09); 7.7347 (2.76); 7.7306 (1.39); 7.7223 (0.86); 7.7171 (3.63); 7.7132 (2.53); 7.5640

(0.50); 7.5607 (0.35); 7.5526 (0.36); 7.5456 (1.68); 7.5398 (0.56); 7.5310 (0.95); 7.5276 (1.58); 7.5240 (0.88); 7.5021 (2.62); 7.4988 (1.18);

7.4871 (1.68); 7.4831 (3.19); 7.4698 (0.52); 7.4657 (1.27); 7.4621 (0.72); 7.2601 (3.80); 5.3202 (5.95); 5.1159 (0.52); 3.3307 (65.87); 3.0484

(1.43); 3.0298 (0.62); 3.0139 (16.00); 2.8907 (3.98); 2.7320 (3.13); 2.7310 (3.10); 2.5251 (0.64); 2.5202 (1.04); 2.5118 (12.70); 2.5073 (25.38);

2.5026 (33.45); 2.4980 (24.20); 2.4935 (11.50); 2.4042 (2.10); 2.3859 (4.07); 2.3764 (0.36); 2.3675 (2.31); 2.1760 (0.67); 2.1579 (0.36); 1.6315

(1.32); 1.6130 (2.55); 1.5946 (2.52); 1.5762 (1.32); 1.5169 (0.35); 1.4985 (0.35); 1.2350 (0.41); 1.1237 (0.50); 1.1084 (0.49); 0.9055 (4.24);

0.8940 (0.95); 0.8870 (8.75); 0.8758 (1.29); 0.8685 (3.89); 0.8573 (0.53); 0.0080 (0.38); −0.0002 (11.42); −0.0085 (0.35)

›Example 272, Solvent: DMSO, Spectrometer: 400.13 MHz

10.2748 (3.08); 7.8288 (0.62); 7.8077 (1.84); 7.7907 (2.76); 7.7879 (2.33); 7.7839 (2.42); 7.7666 (0.68); 7.7630 (0.42); 7.5396 (2.16); 7.5241

(0.64); 7.5201 (0.56); 7.5152 (0.95); 7.5119 (1.00); 7.5065 (0.59); 7.5024 (0.90); 7.4979 (0.69); 7.3698 (2.38); 7.3642 (1.56); 7.3581 (3.33);

7.3557 (3.19); 7.3182 (9.42); 7.3072 (10.44); 7.2977 (0.47); 7.2484 (0.79); 7.2382 (1.13); 7.2271 (1.24); 7.2169 (0.59); 7.2151 (0.59); 7.1003

(1.43); 7.0967 (1.44); 7.0835 (1.36); 7.0798 (1.36); 5.7683 (4.36); 5.3294 (6.25); 4.3091 (1.77); 4.2919 (3.97); 4.2746 (1.82); 3.4037 (0.97);

3.3535 (85.62); 3.3034 (0.84); 3.0561 (16.00); 2.9567 (1.70); 2.9394 (3.60); 2.9223 (1.63); 2.5598 (0.36); 2.5321 (0.51); 2.5273 (0.83); 2.5186

(10.78); 2.5142 (22.44); 2.5097 (30.45); 2.5052 (21.69); 2.5008 (10.00); 2.3376 (10.61); 1.9962 (0.32); 0.8633 (0.38)

›Example 273, Solvent: DMSO, Spectrometer: 400.13 MHz

10.0964 (3.37); 7.8268 (0.34); 7.8057 (2.55); 7.7996 (2.71); 7.7923 (5.67); 7.7786 (0.49); 7.7281 (2.96); 7.7102 (3.59); 7.7066 (2.67); 7.5665

(0.51); 7.5545 (0.42); 7.5481 (1.76); 7.5427 (0.58); 7.5330 (1.00); 7.5300 (1.53); 7.4993 (2.67); 7.4801 (3.37); 7.4663 (0.60); 7.4624 (1.28);

7.0999 (1.37); 7.0926 (1.37); 7.0866 (1.21); 7.0792 (1.31); 5.7660 (9.16); 5.3293 (7.08); 4.9239 (0.48); 4.9086 (0.67); 4.9026 (0.63); 4.8958

(0.64); 4.8896 (0.68); 4.8744 (0.48); 3.3938 (0.69); 3.3441 (47.37); 3.2945 (0.46); 3.0757 (16.00); 2.5620 (0.35); 2.5575 (0.45); 2.5530 (0.33);

2.5121 (25.17); 2.5077 (33.19); 2.5034 (24.22); 2.4584 (0.34); 1.6934 (0.55); 1.6756 (0.68); 1.6582 (0.64); 1.6419 (0.40); 1.5897 (0.56); 1.5748

(0.46); 1.5682 (0.60); 1.5549 (0.96); 1.5406 (0.64); 1.5340 (0.74); 1.5192 (0.57); 1.3542 (0.67); 1.3419 (0.75); 1.3341 (0.65); 1.3209 (1.04);

1.3076 (0.57); 1.2998 (0.59); 1.2872 (0.57); 1.2329 (7.05); 1.2174 (6.90); 0.8989 (10.42); 0.8828 (10.36); 0.8617 (0.94); 0.8441 (0.40)

›Example 274, Solvent: DMSO, Spectrometer: 399.95 MHz

10.7019 (2.04); 8.0143 (0.53); 7.9939 (0.68); 7.9532 (0.96); 7.8834 (1.41); 7.8645 (1.82); 7.8439 (1.19); 7.7312 (1.94); 7.7285 (2.56); 7.7247

(1.23); 7.7160 (0.76); 7.7108 (3.44); 7.7071 (2.38); 7.6072 (3.15); 7.6007 (3.32); 7.5674 (0.48); 7.5555 (0.35); 7.5491 (1.63); 7.5434 (0.48);

7.5342 (0.87); 7.5308 (1.41); 7.5274 (0.72); 7.4996 (2.34); 7.4962 (0.99); 7.4842 (1.60); 7.4805 (3.04); 7.4669 (0.47); 7.4628 (1.22); 7.4596

(0.67); 7.3777 (1.54); 7.3713 (1.43); 7.3555 (1.80); 7.3490 (1.73); 7.2103 (1.70); 7.1917 (1.63); 7.1000 (2.67); 7.0776 (2.29); 5.3832 (5.95);

4.9497 (4.55); 3.3282 (37.74); 3.0682 (16.00); 2.8906 (7.85); 2.7319 (6.15); 2.7310 (6.09); 2.5250 (0.63); 2.5202 (0.97); 2.5117 (12.73); 2.5071

(25.54); 2.5025 (33.71); 2.4979 (24.41); 2.4934 (11.58); −0.0002 (8.34)

›Example 275, Solvent: DMSO, Spectrometer: 399.95 MHz

10.7688 (2.18); 8.0309 (1.21); 8.0102 (1.60); 7.9528 (0.76); 7.8802 (1.31); 7.8607 (1.81); 7.8406 (1.14); 7.7282 (2.70); 7.7246 (1.38); 7.7156

(0.77); 7.7105 (3.43); 7.7068 (2.51); 7.6133 (1.57); 7.6094 (1.68); 7.5936 (1.72); 7.5896 (1.73); 7.5690 (0.50); 7.5659 (0.34); 7.5570 (0.36);

7.5507 (1.64); 7.5451 (0.50); 7.5357 (0.86); 7.5324 (1.44); 7.5291 (0.78); 7.5005 (2.47); 7.4851 (1.65); 7.4813 (3.15); 7.4677 (0.49); 7.4637

(1.25); 7.4606 (0.76); 7.3333 (0.70); 7.3293 (0.73); 7.3145 (1.01); 7.3125 (1.22); 7.3109 (1.23); 7.3088 (1.10); 7.2941 (0.92); 7.2901 (0.90);

7.2107 (1.86); 7.1920 (1.77); 6.9906 (1.36); 6.9877 (1.60); 6.9697 (1.29); 6.9668 (1.36); 6.9256 (0.92); 6.9223 (0.90); 6.9062 (1.47); 6.9035

(1.44); 6.8874 (0.84); 6.8841 (0.79); 5.3872 (6.09); 5.1467 (1.03); 5.1302 (1.04); 3.3399 (123.75); 3.0660 (16.00); 2.8908 (5.95); 2.7322 (4.63);

2.7311 (4.93); 2.5258 (0.64); 2.5210 (1.07); 2.5124 (13.90); 2.5079 (28.05); 2.5033 (37.22); 2.4987 (27.34); 2.4942 (13.33); 1.5824 (5.61);

1.5660 (5.59); −0.0002 (1.61)

›Example 276, Solvent: DMSO, Spectrometer: 399.95 MHz

12.5560 (0.64); 7.9537 (0.82); 7.7374 (2.70); 7.7335 (1.28); 7.7249 (0.79); 7.7197 (3.48); 7.7159 (2.39); 7.5677 (0.48); 7.5562 (0.35); 7.5493

(1.71); 7.5435 (0.50); 7.5346 (0.94); 7.5312 (1.53); 7.5277 (0.77); 7.5050 (2.54); 7.5016 (1.06); 7.4899 (1.64); 7.4859 (3.15); 7.4725 (0.49);

7.4684 (1.25); 7.4649 (0.68); 7.3508 (0.43); 7.3414 (6.02); 7.3404 (5.91); 7.3249 (1.35); 7.3193 (4.72); 7.3104 (0.42); 6.9532 (0.42); 6.9443

(4.51); 6.9387 (1.29); 6.9273 (1.23); 6.9217 (4.04); 6.9127 (0.34); 5.3386 (5.77); 5.0657 (0.38); 5.0492 (1.46); 5.0326 (1.48); 5.0161 (0.39);

3.3457 (65.65); 3.0206 (16.00); 2.8912 (6.84); 2.7330 (5.35); 2.7321 (5.33); 2.5269 (0.41); 2.5221 (0.63); 2.5136 (7.99); 2.5091 (16.01); 2.5045

(21.12); 2.4999 (15.25); 2.4953 (7.19); 1.5480 (5.56); 1.5314 (5.56); −0.0002 (1.60)

›Example 277, Solvent: DMSO, Spectrometer: 399.95 MHz

10.6096 (2.19); 8.0826 (1.14); 8.0618 (1.37); 7.9528 (0.54); 7.8409 (1.25); 7.8215 (1.73); 7.8013 (1.16); 7.7213 (2.00); 7.7189 (2.60); 7.7151

(1.25); 7.7062 (0.86); 7.7011 (3.43); 7.6974 (2.44); 7.5647 (0.49); 7.5527 (0.37); 7.5464 (1.64); 7.5407 (0.51); 7.5314 (0.87); 7.5281 (1.42);

7.5247 (0.72); 7.4962 (2.43); 7.4929 (1.04); 7.4808 (1.67); 7.4770 (3.10); 7.4634 (0.49); 7.4594 (1.23); 7.4562 (0.68); 7.1677 (3.79); 7.1664

(3.80); 7.1476 (2.84); 7.1283 (1.73); 6.9328 (1.44); 6.9284 (1.09); 6.9099 (1.23); 5.3488 (6.06); 4.0675 (0.65); 4.0497 (0.65); 4.0080 (1.45);

3.9927 (3.37); 3.9776 (2.00); 3.9627 (0.33); 3.3890 (0.38); 3.3452 (212.55); 3.3105 (0.40); 3.0430 (16.00); 2.8912 (4.40); 2.7324 (3.41); 2.7316

(3.45); 2.6095 (1.27); 2.5913 (2.79); 2.5733 (1.45); 2.5261 (0.99); 2.5213 (1.58); 2.5128 (17.45); 2.5083 (34.25); 2.5037 (44.75); 2.4991 (32.26);

2.4946 (15.19); 2.4704 (0.69); 2.4523 (0.36); 2.1263 (1.67); 2.1070 (10.62); 2.0661 (0.37); 2.0495 (1.13); 2.0329 (1.74); 2.0160 (1.10); 1.9995

(0.51); 1.9820 (0.35); 1.1884 (0.73); 1.1706 (1.50); 1.1528 (0.72); −0.0002 (3.49)

›Example 278, Solvent: DMSO, Spectrometer: 399.95 MHz

10.1336 (1.96); 8.0664 (1.00); 8.0457 (1.26); 7.9513 (0.33); 7.8853 (1.24); 7.8659 (1.71); 7.8459 (1.15); 7.7246 (2.19); 7.7221 (2.73); 7.7180

(1.51); 7.7142 (0.65); 7.7089 (1.35); 7.7043 (3.69); 7.7005 (2.37); 7.5649 (0.50); 7.5616 (0.33); 7.5528 (0.42); 7.5466 (1.70); 7.5408 (0.57);

7.5315 (1.18); 7.5282 (1.48); 7.5249 (0.82); 7.4962 (2.41); 7.4927 (1.05); 7.4808 (1.86); 7.4770 (3.30); 7.4635 (0.63); 7.4593 (1.50); 7.4559

(1.13); 7.4002 (0.58); 7.3855 (7.73); 7.3797 (3.53); 7.3714 (2.95); 7.3696 (3.46); 7.3640 (0.65); 7.3553 (0.54); 7.3520 (0.70); 7.3498 (0.81);

7.3310 (0.68); 7.3248 (0.93); 7.3179 (0.78); 7.3090 (0.84); 7.3001 (0.46); 7.2945 (0.34); 7.1994 (0.35); 7.1902 (1.72); 7.1726 (1.65); 7.1104

(0.40); 5.4143 (0.33); 5.3643 (6.06); 5.3563 (1.29); 5.2003 (0.33); 4.6039 (8.29); 4.1870 (7.38); 3.3359 (181.12); 3.3008 (0.45); 3.0859 (0.55);

3.0808 (1.06); 3.0716 (2.84); 3.0582 (16.00); 2.9841 (0.85); 2.8906 (2.19); 2.7318 (1.71); 2.7307 (1.65); 2.6762 (0.32); 2.6716 (0.45); 2.6670

(0.33); 2.5484 (0.34); 2.5343 (0.39); 2.5250 (1.32); 2.5201 (2.11); 2.5117 (26.87); 2.5071 (53.88); 2.5025 (71.21); 2.4979 (51.70); 2.4934

(24.61); 2.3822 (0.50); 2.3338 (0.35); 2.3292 (0.47); 2.3247 (0.34); 1.2349 (0.42); 0.0079 (0.69); −0.0002 (21.52); −0.0085 (0.66)

›Example 280, Solvent: DMSO, Spectrometer: 400.13 MHz

10.5230 (2.44); 8.0938 (1.50); 8.0731 (1.78); 7.8439 (1.38); 7.8244 (2.03); 7.8043 (1.29); 7.7289 (2.98); 7.7111 (3.71); 7.7074 (2.72); 7.5768

(0.52); 7.5738 (0.37); 7.5651 (0.44); 7.5585 (1.80); 7.5529 (0.59); 7.5435 (1.08); 7.5404 (1.59); 7.5119 (2.76); 7.4963 (1.92); 7.4927 (3.41);

7.4791 (0.59); 7.4751 (1.29); 7.4720 (0.80); 7.1436 (2.08); 7.1254 (1.99); 5.3696 (7.11); 3.5033 (0.91); 3.4852 (3.04); 3.4670 (3.10); 3.4489

(0.96); 3.3413 (12.46); 2.5602 (0.35); 2.5324 (0.52); 2.5186 (11.43); 2.5145 (23.19); 2.5101 (31.21); 2.5057 (22.84); 2.4646 (0.39); 2.4601

(0.46); 2.4556 (0.33); 2.2822 (3.82); 2.2643 (4.64); 2.1022 (0.46); 2.0853 (0.83); 2.0684 (0.98); 2.0513 (0.77); 2.0341 (0.41); 1.0578 (3.39);

1.0397 (7.59); 1.0215 (3.33); 0.9258 (16.00); 0.9091 (15.75); 0.8953 (0.76); 0.8759 (0.34)

›Example 281, Solvent: DMSO, Spectrometer: 399.95 MHz

11.0200 (2.46); 8.3677 (1.55); 8.3636 (2.85); 8.3595 (1.59); 8.1509 (1.72); 8.1305 (2.07); 8.0224 (0.91); 8.0198 (1.25); 8.0161 (0.96); 8.0028

(1.00); 8.0000 (1.28); 7.9965 (0.99); 7.9676 (1.01); 7.9649 (1.26); 7.9612 (1.03); 7.9533 (1.19); 7.9482 (1.33); 7.9443 (1.35); 7.9417 (0.99);

7.9289 (1.34); 7.9095 (1.89); 7.8893 (1.20); 7.7370 (2.65); 7.7242 (0.78); 7.7191 (3.38); 7.7153 (2.38); 7.5677 (0.48); 7.5559 (0.35); 7.5493

(1.69); 7.5437 (0.48); 7.5344 (0.88); 7.5312 (1.44); 7.5278 (0.73); 7.5015 (2.46); 7.4861 (1.65); 7.4823 (3.14); 7.4688 (0.48); 7.4647 (1.22);

7.4615 (0.68); 7.3370 (1.49); 7.3174 (2.77); 7.2978 (1.35); 7.2416 (1.89); 7.2232 (1.81); 5.4172 (6.36); 3.3294 (54.36); 3.0805 (16.00); 2.8908

(8.70); 2.7319 (7.06); 2.5250 (0.74); 2.5118 (13.92); 2.5073 (27.85); 2.5027 (36.77); 2.4981 (26.76); 2.4936 (12.83); 0.0080 (0.38); −0.0002

(11.62); −0.0085 (0.35)

›Example 282, Solvent: DMSO, Spectrometer: 400.13 MHz

10.0952 (3.12); 7.8296 (0.38); 7.8084 (2.33); 7.8011 (2.52); 7.7944 (5.57); 7.7801 (0.48); 7.7305 (2.80); 7.7175 (0.87); 7.7126 (3.46); 7.7089

(2.53); 7.5694 (0.50); 7.5664 (0.34); 7.5575 (0.38); 7.5511 (1.71); 7.5456 (0.52); 7.5360 (0.93); 7.5329 (1.47); 7.5024 (2.53); 7.4867 (1.76);

7.4832 (3.22); 7.4695 (0.51); 7.4655 (1.21); 7.4625 (0.73); 7.1017 (1.33); 7.0949 (1.30); 7.0877 (1.16); 7.0810 (1.27); 5.7679 (0.50); 5.3323

(6.88); 4.8468 (0.51); 4.8312 (0.81); 4.8146 (0.82); 4.7991 (0.52); 3.4002 (1.35); 3.3506 (114.16); 3.3011 (1.16); 3.0779 (16.00); 2.5599 (0.44);

2.5554 (0.36); 2.5327 (0.62); 2.5190 (13.97); 2.5148 (28.89); 2.5104 (39.28); 2.5060 (28.69); 2.5019 (13.86); 2.4655 (0.34); 2.4610 (0.45);

2.4565 (0.37); 1.9969 (0.77); 1.5931 (0.52); 1.5889 (0.34); 1.5787 (0.44); 1.5745 (0.45); 1.5693 (0.69); 1.5603 (0.45); 1.5550 (0.54); 1.5507

(0.51); 1.5361 (0.69); 1.5193 (0.54); 1.5130 (0.44); 1.5053 (0.52); 1.4993 (0.65); 1.4835 (0.66); 1.4633 (0.34); 1.3874 (0.66); 1.3708 (0.99);

1.3540 (1.17); 1.3476 (0.93); 1.3362 (0.80); 1.3311 (0.84); 1.3193 (0.34); 1.3133 (0.54); 1.2355 (7.10); 1.2198 (7.05); 1.1814 (0.45); 0.9132

(3.75); 0.8949 (7.77); 0.8766 (3.27)

›Example 283, Solvent: DMSO, Spectrometer: 400.13 MHz

11.4597 (1.60); 7.9113 (0.78); 7.8913 (1.69); 7.8723 (1.17); 7.7326 (2.70); 7.7198 (0.86); 7.7148 (3.40); 7.7111 (2.45); 7.5694 (0.49); 7.5663

(0.33); 7.5574 (0.38); 7.5511 (1.66); 7.5455 (0.51); 7.5360 (0.89); 7.5328 (1.43); 7.5296 (0.77); 7.5009 (2.42); 7.4854 (1.71); 7.4818 (3.12);

7.4681 (0.50); 7.4641 (1.21); 7.4610 (0.72); 7.2536 (1.56); 7.2332 (1.50); 5.7642 (6.38); 5.3885 (6.64); 4.4197 (2.03); 4.4033 (4.31); 4.3868

(2.06); 3.3963 (1.56); 3.3463 (92.86); 3.2958 (0.99); 3.0685 (16.00); 2.5577 (0.46); 2.5532 (0.38); 2.5301 (0.55); 2.5166 (10.67); 2.5122 (21.77);

2.5077 (29.27); 2.5033 (20.86); 2.4990 (9.75); 1.7398 (1.09); 1.7229 (2.25); 1.7047 (2.31); 1.6877 (1.16); 0.9557 (3.48); 0.9373 (7.16); 0.9187

(3.18)

›Example 284, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5363 (2.05); 8.1219 (1.42); 8.1013 (1.65); 7.8375 (1.30); 7.8182 (1.79); 7.7979 (1.24); 7.7335 (0.33); 7.7254 (2.71); 7.7216 (1.38); 7.7128

(0.87); 7.7076 (3.63); 7.7039 (2.48); 7.5641 (0.50); 7.5609 (0.33); 7.5521 (0.38); 7.5457 (1.68); 7.5401 (0.52); 7.5307 (0.88); 7.5274 (1.43);

7.5241 (0.75); 7.4955 (2.51); 7.4920 (1.10); 7.4800 (1.70); 7.4762 (3.21); 7.4626 (0.49); 7.4586 (1.26); 7.4554 (0.71); 7.1502 (1.83); 7.1323

(1.77); 5.3644 (6.20); 3.3298 (63.56); 3.2303 (0.37); 3.0552 (16.00); 2.8911 (1.33); 2.7316 (1.05); 2.5431 (0.40); 2.5316 (0.63); 2.5254 (0.90);

2.5205 (1.60); 2.5122 (12.11); 2.5078 (23.99); 2.5032 (31.50); 2.4985 (23.15); 2.4940 (11.22); 1.5746 (0.50); 1.5575 (0.66); 1.5519 (0.59);

1.5413 (0.89); 1.5347 (0.68); 1.5233 (0.78); 1.5194 (0.75); 1.5010 (0.54); 1.4484 (0.42); 1.4353 (0.52); 1.4299 (0.50); 1.4164 (0.65); 1.4019

(0.51); 1.3969 (0.51); 1.3892 (0.49); 1.3835 (0.47); 1.3770 (0.52); 1.3645 (0.60); 1.3523 (0.52); 1.3436 (0.37); 1.3317 (0.46); 1.3193 (0.32);

1.3068 (0.41); 1.3001 (0.47); 1.2817 (1.02); 1.2632 (1.34); 1.2451 (1.38); 1.2287 (1.07); 1.2220 (0.79); 1.2059 (0.95); 1.1933 (0.56); 1.1888

(0.51); 1.1739 (0.49); 1.1624 (0.36); 0.8759 (0.71); 0.8624 (0.55); 0.8568 (0.68); 0.8470 (4.95); 0.8291 (10.76); 0.8108 (5.01); −0.0002 (5.59)

›Example 285, Solvent: DMSO, Spectrometer: 399.95 MHz

10.0705 (2.77); 7.9536 (0.36); 7.8216 (0.41); 7.8005 (2.24); 7.7921 (2.44); 7.7860 (5.46); 7.7711 (0.49); 7.7226 (2.67); 7.7187 (1.30); 7.7098

(0.84); 7.7048 (3.49); 7.7010 (2.43); 7.5621 (0.50); 7.5503 (0.37); 7.5438 (1.67); 7.5381 (0.49); 7.5289 (0.91); 7.5256 (1.45); 7.5222 (0.74);

7.4951 (2.47); 7.4919 (1.05); 7.4797 (1.72); 7.4760 (3.15); 7.4624 (0.51); 7.4583 (1.24); 7.4551 (0.70); 7.0950 (1.33); 7.0886 (1.32); 7.0806

(1.15); 7.0742 (1.26); 5.3254 (6.53); 4.8215 (0.47); 4.8062 (0.78); 4.7893 (0.78); 4.7738 (0.48); 3.3407 (96.03); 3.0703 (16.00); 2.8915 (2.89);

2.7327 (2.25); 2.7320 (2.25); 2.5262 (0.53); 2.5213 (0.88); 2.5129 (10.07); 2.5085 (19.85); 2.5039 (26.06); 2.4993 (18.98); 2.4948 (9.12);

1.5881 (0.36); 1.5747 (0.42); 1.5658 (0.48); 1.5564 (0.42); 1.5509 (0.51); 1.5322 (0.59); 1.5152 (0.44); 1.5066 (0.54); 1.4929 (0.46); 1.3536

(0.50); 1.3363 (0.71); 1.3321 (0.72); 1.3193 (0.78); 1.3149 (0.81); 1.3045 (0.94); 1.2950 (1.34); 1.2863 (1.61); 1.2797 (2.04); 1.2703 (3.01);

1.2541 (1.61); 1.2431 (0.80); 1.2287 (6.76); 1.2130 (6.55); 0.8749 (1.76); 0.8582 (5.20); 0.8411 (1.83); −0.0002 (4.73)

›Example 286, Solvent: DMSO, Spectrometer: 399.95 MHz

11.7750 (1.35); 7.9533 (0.60); 7.7398 (0.37); 7.7340 (2.02); 7.7314 (2.73); 7.7275 (1.36); 7.7189 (0.84); 7.7138 (3.47); 7.7100 (2.46); 7.5626

(0.51); 7.5594 (0.34); 7.5512 (0.38); 7.5443 (1.73); 7.5384 (0.52); 7.5296 (0.99); 7.5262 (1.55); 7.5227 (0.77); 7.5004 (2.57); 7.4971 (1.18);

7.4854 (1.72); 7.4814 (3.18); 7.4680 (0.52); 7.4639 (1.26); 7.4603 (0.76); 7.2548 (3.95); 5.3572 (0.33); 5.2852 (5.91); 3.9704 (0.55); 3.9495

(4.69); 3.9327 (4.70); 3.3295 (58.14); 3.0320 (16.00); 3.0231 (0.61); 3.0055 (0.91); 2.8909 (4.96); 2.7322 (3.94); 2.7313 (3.79); 2.5251 (0.61);

2.5203 (1.00); 2.5118 (11.94); 2.5073 (23.81); 2.5027 (31.39); 2.4981 (22.76); 2.4936 (10.82); 1.9567 (0.44); 1.9399 (0.86); 1.9231 (1.11);

1.9063 (0.90); 1.8896 (0.45); 1.2350 (0.33); 1.1216 (0.52); 1.1064 (0.51); 0.9226 (15.33); 0.9058 (14.86); 0.8933 (0.33); 0.7691 (1.58); 0.7522

(1.53); 0.0079 (0.35); −0.0002 (10.48); −0.0085 (0.32)

›Example 287, Solvent: DMSO, Spectrometer: 399.95 MHz

10.7077 (2.17); 8.0144 (1.38); 7.9939 (1.80); 7.9534 (0.62); 7.8623 (1.36); 7.8430 (1.89); 7.8227 (1.15); 7.7275 (2.71); 7.7146 (0.94); 7.7097

(3.53); 7.7060 (2.49); 7.5683 (0.51); 7.5651 (0.34); 7.5562 (0.42); 7.5500 (1.70); 7.5444 (0.52); 7.5350 (0.95); 7.5317 (1.46); 7.5284 (0.75);

7.4994 (2.48); 7.4838 (1.86); 7.4802 (3.21); 7.4665 (0.56); 7.4624 (1.28); 7.4594 (0.74); 7.1953 (1.87); 7.1770 (1.81); 7.0770 (2.58); 7.0565

(3.04); 6.8270 (0.55); 6.8201 (3.88); 6.8154 (1.29); 6.8032 (1.28); 6.7986 (3.28); 6.7914 (0.35); 5.3807 (6.32); 5.0371 (0.35); 5.0208 (1.21);

5.0043 (1.22); 4.9881 (0.35); 3.3311 (69.44); 3.0567 (16.00); 2.8905 (4.81); 2.7320 (3.89); 2.5250 (0.77); 2.5117 (14.21); 2.5073 (26.90);

2.5027 (34.43); 2.4981 (24.82); 2.4937 (11.83); 2.1976 (10.16); 1.5119 (5.69); 1.4954 (5.63); −0.0002 (4.65)

›Example 288, Solvent: DMSO, Spectrometer: 399.95 MHz

10.4500 (2.47); 7.9533 (1.17); 7.8545 (0.85); 7.8337 (1.78); 7.8155 (1.90); 7.7901 (2.36); 7.7711 (1.12); 7.7244 (2.84); 7.7115 (0.89); 7.7066

(3.55); 7.7028 (2.54); 7.5624 (0.51); 7.5593 (0.34); 7.5506 (0.39); 7.5441 (1.74); 7.5385 (0.54); 7.5291 (0.96); 7.5259 (1.49); 7.5226 (0.80);

7.4958 (2.63); 7.4802 (1.83); 7.4766 (3.33); 7.4629 (0.53); 7.4589 (1.28); 7.4558 (0.74); 7.1345 (1.71); 7.1328 (1.71); 7.1166 (1.68); 7.1148

(1.58); 5.3445 (6.69); 4.3068 (2.26); 4.2918 (4.59); 4.2767 (2.35); 3.3322 (55.35); 3.0881 (0.45); 3.0698 (16.00); 2.9408 (2.44); 2.9257 (4.72);

2.9107 (2.35); 2.8907 (8.90); 2.7315 (7.16); 2.5252 (0.58); 2.5119 (10.49); 2.5074 (20.47); 2.5029 (26.75); 2.4983 (19.59); 2.4939 (9.53); −0.0002

(4.03)

›Example 289, Solvent: DMSO, Spectrometer: 399.95 MHz

12.8382 (0.82); 8.2864 (1.50); 8.2819 (2.62); 8.2774 (1.51); 8.0804 (0.90); 8.0778 (1.16); 8.0741 (0.90); 8.0608 (1.00); 8.0571 (1.22); 8.0545

(0.94); 7.9532 (0.46); 7.8530 (0.83); 7.8508 (0.95); 7.8482 (0.90); 7.8461 (0.82); 7.8330 (0.96); 7.8308 (1.03); 7.8282 (1.05); 7.8261 (0.89);

7.7496 (1.91); 7.7471 (2.60); 7.7431 (1.26); 7.7346 (0.77); 7.7295 (3.35); 7.7256 (2.30); 7.5686 (0.46); 7.5574 (0.33); 7.5503 (1.64); 7.5443

(0.51); 7.5327 (2.72); 7.5288 (0.89); 7.5134 (3.05); 7.5080 (2.62); 7.5046 (1.13); 7.4934 (2.73); 7.4890 (3.11); 7.4757 (0.49); 7.4715 (1.23);

7.4679 (0.72); 7.3997 (3.42); 5.3866 (5.58); 3.3426 (101.07); 3.0219 (16.00); 2.8915 (3.90); 2.7329 (3.01); 2.7320 (3.03); 2.5265 (0.57); 2.5217

(0.91); 2.5132 (11.98); 2.5086 (24.12); 2.5040 (31.99); 2.4994 (23.20); 2.4949 (11.01); −0.0002 (3.13)

›Example 290, Solvent: DMSO, Spectrometer: 400.13 MHz

10.3988 (2.83); 7.8336 (2.30); 7.8287 (2.35); 7.8207 (5.19); 7.8077 (0.34); 7.4434 (0.79); 7.4388 (1.18); 7.4220 (3.44); 7.4190 (3.83); 7.4157

(2.78); 7.4131 (2.79); 7.4076 (0.68); 7.3984 (3.61); 7.3958 (3.68); 7.3913 (1.19); 7.3792 (2.33); 7.3602 (0.72); 7.3557 (1.14); 7.3508 (0.57);

7.3459 (0.51); 7.3384 (1.09); 7.3215 (0.37); 7.2813 (1.35); 7.2790 (1.22); 7.2656 (0.72); 7.2618 (1.13); 7.2596 (0.95); 7.2437 (1.47); 7.2377

(1.88); 7.2336 (1.31); 7.1422 (1.05); 7.1403 (1.12); 7.1360 (1.09); 7.1341 (0.98); 7.1226 (1.64); 7.1154 (2.04); 7.1027 (1.16); 5.7688 (7.76);

5.3422 (5.76); 5.1856 (6.65); 3.7858 (16.00); 3.4000 (1.19); 3.3500 (96.57); 3.3264 (0.61); 3.3000 (0.91); 3.0634 (0.62); 3.0542 (14.52); 2.5599

(0.33); 2.5187 (9.19); 2.5143 (19.51); 2.5098 (26.74); 2.5053 (19.07); 2.5009 (8.79); 1.9968 (0.40)

›Example 291, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5535 (2.45); 8.0774 (1.51); 8.0567 (1.87); 7.9531 (1.07); 7.8944 (1.41); 7.8749 (2.05); 7.8549 (1.20); 7.7282 (2.93); 7.7103 (3.67); 7.7066

(2.68); 7.5666 (0.53); 7.5636 (0.36); 7.5546 (0.42); 7.5483 (1.81); 7.5428 (0.57); 7.5331 (1.02); 7.5301 (1.54); 7.5269 (0.85); 7.4990 (2.71);

7.4798 (3.47); 7.4659 (0.58); 7.4621 (1.33); 7.4591 (0.82); 7.3608 (1.26); 7.3418 (1.65); 7.2478 (0.66); 7.2297 (1.44); 7.2120 (2.96); 7.1941

(2.57); 7.1785 (1.52); 7.1614 (0.69); 7.0748 (1.56); 7.0567 (1.15); 5.3861 (6.82); 4.9128 (0.91); 4.8752 (2.31); 4.8329 (2.03); 4.7953 (0.79);

4.1945 (1.83); 4.1732 (1.91); 3.3299 (76.90); 3.2517 (0.66); 3.2333 (0.92); 3.2148 (0.63); 3.0958 (0.46); 3.0854 (0.44); 3.0703 (16.00); 2.8904

(7.84); 2.7317 (6.48); 2.5246 (0.89); 2.5113 (15.64); 2.5069 (30.26); 2.5024 (39.50); 2.4979 (29.41); 2.4936 (14.76); 1.2661 (6.42); 1.2488

(6.34); 1.2353 (0.43); −0.0002 (8.21)

›Example 292, Solvent: DMSO, Spectrometer: 400.13 MHz

10.0906 (2.91); 7.8316 (0.45); 7.8106 (2.16); 7.8001 (2.59); 7.7951 (4.96); 7.7795 (0.62); 7.7311 (2.80); 7.7181 (0.96); 7.7132 (3.48); 7.7096

(2.55); 7.5696 (0.51); 7.5665 (0.36); 7.5578 (0.42); 7.5513 (1.71); 7.5457 (0.55); 7.5363 (0.97); 7.5331 (1.51); 7.5299 (0.83); 7.5029 (2.57);

7.4873 (1.82); 7.4837 (3.22); 7.4701 (0.55); 7.4661 (1.22); 7.4630 (0.76); 7.1024 (1.36); 7.0967 (1.35); 7.0874 (1.22); 7.0817 (1.29); 5.7644

(2.15); 5.3389 (6.96); 4.6343 (1.09); 4.6189 (1.59); 4.6034 (1.10); 3.3258 (8.17); 3.3019 (0.51); 3.0752 (16.00); 2.5643 (0.36); 2.5598 (0.50);

2.5553 (0.37); 2.5184 (10.46); 2.5141 (20.80); 2.5097 (27.75); 2.5052 (20.12); 2.5011 (9.73); 1.9967 (0.88); 1.8155 (0.55); 1.7987 (0.87);

1.7834 (0.90); 1.7666 (0.60); 1.2867 (0.39); 1.2527 (1.85); 1.2003 (0.46); 1.1879 (7.34); 1.1720 (7.27); 0.9252 (6.99); 0.9176 (7.32); 0.9083

(7.07); 0.9007 (6.78); 0.8824 (0.96); 0.8657 (2.52); 0.8481 (1.04)

›Example 293, Solvent: DMSO, Spectrometer: 400.13 MHz

10.2789 (3.15); 7.8438 (0.62); 7.8228 (1.93); 7.8054 (3.57); 7.8002 (2.69); 7.7832 (0.75); 7.7793 (0.42); 7.7257 (2.84); 7.7078 (3.51); 7.7041

(2.48); 7.5642 (0.52); 7.5610 (0.35); 7.5520 (0.42); 7.5457 (1.74); 7.5402 (0.52); 7.5307 (0.93); 7.5275 (1.46); 7.4965 (2.61); 7.4809 (1.82);

7.4773 (3.26); 7.4636 (0.54); 7.4596 (1.24); 7.4567 (0.74); 7.1155 (1.45); 7.1117 (1.47); 7.0989 (1.36); 7.0951 (1.37); 5.3380 (6.63); 4.1862

(1.65); 4.1705 (3.40); 4.1547 (1.67); 3.3866 (0.40); 3.3374 (24.34); 3.2878 (0.41); 3.0613 (16.00); 2.5124 (2.45); 2.5081 (4.96); 2.5036 (6.66);

2.4992 (4.73); 2.4950 (2.19); 2.4122 (0.34); 2.3838 (0.60); 2.3638 (0.66); 2.3425 (0.65); 2.3154 (0.35); 1.9055 (0.43); 1.8899 (1.05); 1.8748

(1.00); 1.8663 (1.06); 1.8497 (0.95); 1.8339 (0.36); −0.0002 (3.50)

›Example 294, Solvent: DMSO, Spectrometer: 399.95 MHz

10.6890 (2.49); 8.1522 (0.93); 8.1315 (1.09); 7.8916 (1.25); 7.8721 (1.85); 7.8520 (1.16); 7.8050 (1.30); 7.8008 (1.38); 7.7857 (1.46); 7.7815

(1.41); 7.7131 (2.66); 7.7003 (0.83); 7.6952 (3.45); 7.6916 (2.47); 7.5588 (0.53); 7.5557 (0.33); 7.5466 (0.41); 7.5406 (1.71); 7.5349 (0.52);

7.5224 (2.03); 7.5186 (1.47); 7.5043 (1.15); 7.5021 (1.24); 7.5001 (1.26); 7.4979 (1.10); 7.4869 (2.60); 7.4837 (2.02); 7.4794 (1.19); 7.4712

(1.81); 7.4677 (3.23); 7.4540 (0.53); 7.4499 (1.28); 7.4469 (0.76); 7.4106 (1.68); 7.4054 (0.66); 7.3918 (2.78); 7.3893 (2.68); 7.3753 (0.88);

7.3706 (2.30); 7.2762 (1.04); 7.2738 (1.03); 7.2572 (1.72); 7.2551 (1.68); 7.2386 (0.87); 7.2362 (0.84); 7.2005 (1.89); 7.1871 (1.28); 7.1822

(1.99); 7.1687 (1.87); 7.1525 (0.51); 7.1501 (0.83); 7.1476 (0.52); 7.1309 (2.34); 7.1286 (2.70); 7.1093 (2.38); 6.9056 (1.77); 6.9041 (1.75);

6.8849 (1.69); 5.3532 (5.98); 3.3296 (46.78); 3.0321 (16.00); 2.8901 (1.73); 2.7318 (1.42); 2.7307 (1.38); 2.5249 (0.61); 2.5200 (0.95); 2.5115

(11.41); 2.5070 (22.62); 2.5024 (29.74); 2.4978 (21.66); 2.4933 (10.40); −0.0002 (7.59)

›Example 295, Solvent: DMSO, Spectrometer: 400.13 MHz

10.2021 (3.03); 7.8194 (2.48); 7.8139 (2.57); 7.8063 (5.69); 7.7929 (0.38); 7.6238 (0.66); 7.6198 (0.99); 7.6141 (0.93); 7.6087 (0.73); 7.6054

(1.17); 7.6020 (0.92); 7.5989 (0.96); 7.5945 (1.23); 7.5884 (2.44); 7.5859 (2.27); 7.5638 (0.76); 7.5496 (0.85); 7.5436 (1.15); 7.5292 (1.21);

7.5239 (0.60); 7.5086 (0.53); 7.4333 (0.52); 7.4305 (0.58); 7.4271 (0.53); 7.4241 (0.49); 7.4093 (0.93); 7.4053 (0.81); 7.3911 (0.42); 7.3883

(0.43); 7.3850 (0.40); 7.3822 (0.34); 7.1167 (1.31); 7.1091 (1.31); 7.1036 (1.13); 7.0960 (1.26); 5.7681 (4.69); 5.3569 (6.73); 4.1129 (2.13);

4.0963 (4.54); 4.0797 (2.17); 3.4003 (0.73); 3.3503 (83.72); 3.3005 (0.85); 3.0656 (16.00); 2.5321 (0.53); 2.5185 (12.25); 2.5142 (25.77);

2.5097 (35.14); 2.5053 (25.40); 2.5009 (11.99); 2.4642 (0.35); 2.4599 (0.42); 1.6318 (0.45); 1.6147 (1.42); 1.6084 (0.53); 1.5974 (1.82); 1.5777

(1.54); 1.5611 (0.62); 1.4181 (0.32); 1.3996 (1.13); 1.3805 (1.78); 1.3616 (1.80); 1.3435 (1.07); 0.9310 (4.22); 0.9127 (8.61); 0.8941 (3.62)

›Example 296, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5653 (2.11); 8.0322 (0.93); 8.0114 (1.20); 7.9526 (0.57); 7.8814 (1.32); 7.8622 (1.82); 7.8419 (1.12); 7.7279 (2.60); 7.7241 (1.26); 7.7152

(0.80); 7.7101 (3.42); 7.7064 (2.39); 7.5680 (0.49); 7.5560 (0.37); 7.5497 (1.65); 7.5439 (0.49); 7.5347 (0.88); 7.5314 (1.42); 7.5280 (0.72);

7.5001 (2.40); 7.4967 (1.02); 7.4847 (1.67); 7.4809 (3.11); 7.4673 (0.49); 7.4633 (1.23); 7.4601 (0.69); 7.2018 (1.78); 7.1835 (1.74); 7.1030

(2.47); 7.0826 (2.95); 6.8616 (0.47); 6.8542 (3.89); 6.8491 (1.20); 6.8377 (1.13); 6.8327 (3.27); 5.3810 (6.19); 4.7431 (6.57); 3.3497 (123.82);

3.0655 (16.00); 2.8907 (4.55); 2.7323 (3.65); 2.7313 (3.54); 2.5260 (0.60); 2.5128 (11.48); 2.5083 (22.74); 2.5037 (29.82); 2.4991 (21.60);

2.4946 (10.25); 2.2250 (10.15); −0.0002 (2.80)

›Example 297, Solvent: DMSO, Spectrometer: 400.13 MHz

7.3734 (0.52); 7.3625 (0.62); 5.8215 (0.71); 5.4128 (0.36); 3.4142 (16.00); 3.1179 (0.93); 2.5748 (0.94); 2.5704 (1.97); 2.5659 (2.68); 2.5614

(1.90); 2.5570 (0.88)

›Example 298, Solvent: DMSO, Spectrometer: 399.95 MHz

10.2484 (2.39); 7.9534 (0.83); 7.8248 (0.61); 7.8038 (1.65); 7.7867 (2.12); 7.7805 (1.88); 7.7772 (2.09); 7.7597 (0.68); 7.7563 (0.46); 7.7251

(1.89); 7.7226 (2.41); 7.7187 (1.18); 7.7099 (0.77); 7.7048 (3.20); 7.7011 (2.24); 7.6211 (1.42); 7.6182 (1.43); 7.6011 (1.55); 7.5982 (1.49);

7.5628 (0.46); 7.5509 (0.35); 7.5445 (1.55); 7.5388 (0.47); 7.5296 (0.84); 7.5262 (1.35); 7.5228 (0.69); 7.4956 (2.24); 7.4922 (0.97); 7.4802

(1.55); 7.4765 (2.89); 7.4629 (0.48); 7.4588 (1.19); 7.4556 (0.70); 7.4476 (0.99); 7.4433 (1.04); 7.4285 (1.51); 7.4243 (1.46); 7.3636 (0.83);

7.3606 (0.84); 7.3451 (1.48); 7.3421 (1.40); 7.3263 (0.74); 7.3232 (0.69); 7.2615 (0.42); 7.2452 (0.46); 7.2151 (0.84); 7.2107 (0.83); 7.1956

(1.11); 7.1918 (1.06); 7.1768 (0.62); 7.1724 (0.58); 7.1076 (1.33); 7.1042 (1.34); 7.0905 (1.29); 7.0870 (1.25); 5.3310 (5.73); 4.3271 (1.48);

4.3099 (3.37); 4.2927 (1.54); 3.3297 (54.92); 3.0986 (1.40); 3.0814 (2.94); 3.0634 (16.00); 2.8907 (6.64); 2.7322 (5.40); 2.7310 (5.22); 2.5252

(0.66); 2.5118 (11.96); 2.5073 (23.52); 2.5027 (30.86); 2.4981 (22.42); 2.4936 (10.72); −0.0002 (7.07)

›Example 300, Solvent: DMSO, Spectrometer: 400.13 MHz

10.1755 (6.27); 7.8379 (1.21); 7.8168 (4.35); 7.8011 (9.36); 7.7974 (6.41); 7.7874 (0.39); 7.7810 (1.42); 7.7763 (0.68); 7.7288 (4.42); 7.7264

(5.89); 7.7224 (2.90); 7.7138 (1.80); 7.7087 (7.61); 7.7049 (5.26); 7.5779 (0.59); 7.5748 (1.08); 7.5716 (0.75); 7.5631 (0.92); 7.5565 (3.72);

7.5507 (1.19); 7.5417 (2.13); 7.5383 (3.32); 7.5349 (1.70); 7.5105 (5.53); 7.5071 (2.44); 7.4953 (3.67); 7.4914 (6.78); 7.4779 (1.12); 7.4738

(2.70); 7.4705 (1.53); 7.0992 (3.00); 7.0946 (3.03); 7.0831 (2.78); 7.0785 (2.83); 5.3451 (14.17); 4.1046 (4.42); 4.0879 (9.60); 4.0712 (4.48);

3.5266 (1.80); 3.5085 (6.12); 3.4903 (6.24); 3.4722 (1.91); 3.4170 (0.98); 3.3670 (69.16); 3.3169 (0.75); 2.5647 (0.39); 2.5602 (0.58); 2.5557

(0.41); 2.5325 (0.90); 2.5191 (16.36); 2.5147 (33.99); 2.5102 (46.37); 2.5056 (32.84); 2.5012 (15.09); 2.4644 (0.37); 2.4600 (0.49); 2.4557

(0.37); 1.6470 (0.54); 1.6293 (1.98); 1.6121 (3.17); 1.5949 (2.25); 1.5778 (0.71); 1.3719 (1.55); 1.3653 (0.56); 1.3477 (2.42); 1.3444 (2.31);

1.3372 (4.03); 1.3296 (8.24); 1.3207 (6.12); 1.3116 (5.42); 1.2783 (0.39); 1.2413 (0.56); 1.0620 (6.97); 1.0439 (16.00); 1.0256 (6.73); 0.9020

(4.14); 0.8958 (2.36); 0.8887 (3.98); 0.8846 (11.41); 0.8728 (2.50); 0.8667 (3.29); 0.8535 (0.33)

›Example 301, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5817 (2.01); 8.0676 (1.09); 8.0469 (1.31); 7.9533 (0.61); 7.8393 (1.24); 7.8200 (1.68); 7.7997 (1.13); 7.7234 (1.93); 7.7207 (2.49); 7.7168

(1.18); 7.7080 (0.75); 7.7029 (3.37); 7.6992 (2.32); 7.5640 (0.48); 7.5521 (0.35); 7.5457 (1.60); 7.5400 (0.47); 7.5308 (0.84); 7.5274 (1.39);

7.5240 (0.69); 7.4957 (2.34); 7.4922 (0.98); 7.4803 (1.60); 7.4765 (3.03); 7.4629 (0.47); 7.4588 (1.22); 7.4556 (0.67); 7.2924 (1.43); 7.2870

(0.61); 7.2783 (1.68); 7.2706 (1.96); 7.2621 (0.73); 7.2566 (1.76); 7.1448 (1.71); 7.1259 (1.76); 7.1173 (2.20); 7.1118 (0.63); 7.1008 (0.73);

7.0949 (3.46); 7.0889 (0.72); 7.0779 (0.59); 7.0726 (1.70); 5.3495 (5.92); 3.3272 (45.85); 3.0539 (0.44); 3.0439 (16.00); 2.9030 (0.99); 2.8904

(5.61); 2.8848 (2.09); 2.8648 (1.47); 2.7318 (4.10); 2.7308 (3.99); 2.7112 (1.68); 2.6911 (2.30); 2.6724 (1.23); 2.5250 (0.71); 2.5202 (1.11);

2.5115 (13.41); 2.5070 (26.81); 2.5024 (35.26); 2.4978 (25.40); 2.4932 (11.99); 0.0080 (0.42); −0.0002 (12.90); −0.0085 (0.38)

›Example 302, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5751 (1.95); 8.0622 (1.18); 8.0415 (1.42); 7.8378 (1.28); 7.8186 (1.79); 7.7983 (1.19); 7.7239 (2.63); 7.7201 (1.30); 7.7112 (0.81); 7.7061

(3.53); 7.7023 (2.40); 7.5646 (0.48); 7.5527 (0.37); 7.5463 (1.68); 7.5406 (0.49); 7.5314 (0.89); 7.5280 (1.44); 7.5247 (0.73); 7.4975 (2.46);

7.4941 (1.05); 7.4821 (1.68); 7.4784 (3.15); 7.4648 (0.49); 7.4607 (1.24); 7.4575 (0.69); 7.1459 (1.79); 7.1275 (1.75); 5.3552 (6.34); 3.3313

(57.75); 3.0564 (16.00); 2.8909 (0.69); 2.8048 (1.11); 2.7982 (2.33); 2.7916 (1.11); 2.7322 (0.57); 2.5253 (0.64); 2.5205 (1.04); 2.5120 (11.23);

2.5075 (22.90); 2.5029 (28.76); 2.4983 (20.75); 2.4938 (10.21); 2.4883 (4.07); 2.4697 (1.89); 2.2215 (1.06); 2.2149 (1.11); 2.2035 (2.52);

2.1969 (2.46); 2.1858 (1.30); 2.1792 (1.22); 1.7808 (0.50); 1.7628 (1.78); 1.7446 (2.56); 1.7265 (1.66); 1.7082 (0.39); 0.8758 (0.46); −0.0002

(5.54)

›Example 303, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5034 (2.10); 8.0708 (1.22); 8.0501 (1.45); 7.8310 (1.27); 7.8118 (1.75); 7.7914 (1.20); 7.7258 (2.01); 7.7234 (2.56); 7.7195 (1.26); 7.7106

(0.79); 7.7055 (3.50); 7.7017 (2.38); 7.5638 (0.49); 7.5520 (0.36); 7.5456 (1.65); 7.5399 (0.48); 7.5306 (0.87); 7.5273 (1.41); 7.5239 (0.71);

7.4961 (2.41); 7.4927 (1.01); 7.4807 (1.65); 7.4769 (3.08); 7.4633 (0.48); 7.4593 (1.23); 7.4560 (0.67); 7.1401 (1.75); 7.1217 (1.72); 5.3530

(6.14); 3.3298 (59.04); 3.0538 (16.00); 2.5255 (0.55); 2.5207 (0.88); 2.5122 (10.97); 2.5076 (21.92); 2.5030 (28.82); 2.4984 (20.84); 2.4939

(9.85); 2.3883 (1.42); 2.3699 (2.74); 2.3515 (1.55); 1.5786 (0.72); 1.5611 (1.06); 1.5439 (0.73); 1.2645 (4.43); 1.2525 (4.67); 1.2380 (7.50);

0.8757 (0.48); 0.8610 (1.82); 0.8441 (5.76); 0.8267 (1.94); −0.0002 (6.01)

›Example 304, Solvent: DMSO, Spectrometer: 400.13 MHz

10.8355 (2.01); 8.1896 (1.63); 8.1692 (1.88); 7.8924 (1.28); 7.8729 (1.87); 7.8529 (1.22); 7.7345 (2.69); 7.7216 (0.91); 7.7167 (3.42); 7.7130

(2.45); 7.5740 (0.51); 7.5709 (0.35); 7.5620 (0.41); 7.5556 (1.64); 7.5500 (0.55); 7.5407 (0.94); 7.5374 (1.45); 7.5341 (0.78); 7.5063 (2.45);

7.4909 (1.73); 7.4872 (3.13); 7.4735 (0.55); 7.4695 (1.23); 7.4664 (0.72); 7.1973 (1.87); 7.1792 (1.78); 6.6584 (0.92); 6.6330 (1.09); 6.6159

(1.36); 6.5904 (1.30); 6.3429 (1.55); 6.3382 (1.57); 6.3004 (1.18); 6.2956 (1.16); 5.8106 (1.49); 5.8059 (1.27); 5.7853 (1.24); 5.7805 (1.38);

5.3846 (6.54); 3.4060 (4.17); 3.4030 (0.76); 3.3548 (290.02); 3.3064 (2.05); 3.3037 (2.28); 3.0602 (16.00); 2.6799 (0.45); 2.6755 (0.35); 2.5713

(0.43); 2.5668 (0.73); 2.5623 (0.90); 2.5577 (0.61); 2.5333 (1.13); 2.5197 (25.85); 2.5153 (54.79); 2.5109 (75.93); 2.5064 (57.01); 2.5020

(29.30); 2.4643 (1.40); 2.4599 (1.19); 2.3424 (0.35); 2.3378 (0.48); 2.3332 (0.37); 2.0844 (1.74)

›Example 305, Solvent: DMSO, Spectrometer: 400.13 MHz

10.1303 (1.45); 7.8128 (0.98); 7.8011 (1.25); 7.7970 (2.15); 7.7299 (1.32); 7.7120 (1.62); 7.7083 (1.19); 7.5496 (0.79); 7.5345 (0.45); 7.5314

(0.69); 7.5007 (1.20); 7.4849 (0.88); 7.4815 (1.51); 7.4639 (0.60); 7.1003 (0.64); 7.0950 (0.63); 7.0851 (0.58); 7.0797 (0.61); 5.3422 (3.17);

4.5504 (0.86); 4.5343 (0.87); 3.4017 (0.75); 3.3517 (60.76); 3.3007 (0.38); 3.0662 (7.33); 2.5121 (12.87); 2.5077 (17.01); 2.5034 (12.34);

1.1513 (3.30); 1.1352 (3.28); 0.9115 (16.00)

›Example 306, Solvent: DMSO, Spectrometer: 400.13 MHz

10.4951 (2.75); 7.8642 (0.94); 7.8437 (1.78); 7.8249 (1.67); 7.7724 (2.22); 7.7523 (1.40); 7.7318 (2.74); 7.7189 (0.93); 7.7139 (3.47); 7.7102

(2.47); 7.5692 (0.51); 7.5660 (0.38); 7.5574 (0.42); 7.5509 (1.74); 7.5452 (0.54); 7.5359 (0.95); 7.5327 (1.47); 7.5294 (0.77); 7.5024 (2.51);

7.4869 (1.75); 7.4833 (3.18); 7.4697 (0.53); 7.4656 (1.24); 7.4625 (0.75); 7.1503 (1.82); 7.1326 (1.75); 5.7642 (5.61); 5.3520 (6.47); 5.2171

(0.63); 5.2130 (0.74); 5.2020 (1.22); 5.1979 (0.64); 5.1909 (0.70); 5.1866 (0.76); 4.0461 (0.40); 4.0283 (0.40); 3.9591 (1.44); 3.9480 (1.61);

3.9294 (3.60); 3.9185 (3.17); 3.8929 (3.27); 3.8774 (3.29); 3.8632 (1.54); 3.8478 (1.49); 3.3268 (10.91); 3.0843 (16.00); 2.5319 (0.47); 2.5186

(9.15); 2.5142 (18.42); 2.5097 (24.73); 2.5053 (17.65); 2.5009 (8.30); 1.9968 (1.70); 1.3740 (0.87); 1.2540 (0.46); 1.2004 (0.47); 1.1826 (0.90);

1.1648 (0.44); 0.8658 (0.64)

›Example 307, Solvent: DMSO, Spectrometer: 400.13 MHz

11.7662 (2.02); 7.9923 (0.70); 7.9716 (2.06); 7.9544 (3.68); 7.9488 (2.77); 7.9322 (0.83); 7.7339 (2.77); 7.7160 (3.50); 7.7123 (2.60); 7.5723

(0.59); 7.5693 (0.44); 7.5604 (0.52); 7.5541 (1.76); 7.5484 (0.66); 7.5391 (1.04); 7.5358 (1.54); 7.5326 (0.92); 7.5039 (2.87); 7.4999 (2.41);

7.4942 (1.14); 7.4844 (4.11); 7.4788 (3.45); 7.4666 (1.94); 7.4600 (3.02); 7.4060 (3.23); 7.3866 (1.99); 7.3629 (0.96); 7.3601 (1.32); 7.3419

(2.03); 7.3372 (1.99); 7.3332 (1.68); 7.3267 (0.82); 7.3203 (1.75); 7.3163 (1.45); 5.7616 (1.24); 5.4392 (6.75); 3.3368 (242.25); 3.2532 (0.67);

3.2134 (0.36); 3.0760 (16.00); 2.6760 (0.42); 2.6712 (0.35); 2.5157 (22.45); 2.5113 (44.00); 2.5069 (58.73); 2.5024 (42.83); 2.4982 (21.79);

2.3380 (0.36); 2.3339 (0.46); 2.3291 (0.35); 1.9936 (0.48); 1.2393 (0.34)

›Example 308, Solvent: DMSO, Spectrometer: 400.13 MHz

8.4946 (0.35); 7.9608 (0.78); 7.5519 (5.07); 7.5313 (5.95); 7.2961 (5.25); 7.2760 (4.82); 7.0021 (3.34); 6.9834 (1.17); 6.9611 (0.58); 6.7589

(0.48); 6.7475 (0.48); 6.7362 (0.37); 6.7248 (0.36); 6.5653 (5.42); 5.2835 (0.60); 5.0766 (8.67); 3.1224 (0.36); 3.1101 (0.68); 3.1043 (1.12);

3.0860 (1.13); 3.0677 (0.42); 2.9646 (0.46); 2.9424 (0.59); 2.8976 (5.66); 2.7391 (4.59); 2.7380 (4.66); 2.5603 (0.41); 2.5557 (0.43); 2.5509

(0.42); 2.5331 (0.36); 2.5283 (0.65); 2.5194 (13.51); 2.5151 (29.37); 2.5106 (40.95); 2.5061 (30.28); 2.5018 (14.89); 2.4699 (0.46); 2.4652

(0.59); 2.4607 (0.70); 2.4562 (0.56); 2.4275 (0.36); 2.3926 (0.37); 2.3519 (16.00); 2.3206 (0.44); 2.3026 (0.40); 1.2036 (1.64); 1.1854 (3.50);

1.1672 (1.64)

›Example 309, Solvent: DMSO, Spectrometer: 399.95 MHz

10.3176 (1.10); 7.9596 (0.98); 7.9575 (1.12); 7.9391 (2.11); 7.9369 (1.93); 7.9072 (1.61); 7.8887 (1.76); 7.8681 (0.91); 7.7338 (1.85); 7.7311

(2.43); 7.7272 (1.22); 7.7185 (0.80); 7.7134 (3.35); 7.7096 (2.29); 7.5668 (0.48); 7.5550 (0.35); 7.5485 (1.58); 7.5428 (0.48); 7.5336 (0.85);

7.5302 (1.41); 7.5268 (0.70); 7.5044 (0.48); 7.4992 (2.31); 7.4957 (1.02); 7.4839 (1.57); 7.4801 (2.97); 7.4665 (0.46); 7.4624 (1.21); 7.4592

(0.67); 7.2448 (1.48); 7.2426 (1.52); 7.2265 (1.48); 7.2243 (1.42); 5.4005 (6.19); 3.3294 (55.22); 3.0910 (0.33); 3.0797 (16.00); 3.0660 (0.33);

2.8907 (2.20); 2.7320 (1.76); 2.7308 (1.72); 2.5249 (0.59); 2.5201 (0.98); 2.5116 (10.84); 2.5071 (21.47); 2.5025 (28.28); 2.4978 (20.42);

2.4933 (9.62); 1.4784 (0.34); 1.4674 (0.47); 1.4617 (0.90); 1.4543 (1.07); 1.4427 (0.67); 1.4338 (0.37); 1.4165 (0.84); 1.4104 (1.10); 1.4085

(1.14); 1.3983 (0.82); 1.3868 (0.36); 1.3685 (0.70); 1.3573 (1.37); 1.3479 (1.50); 1.3366 (1.20); 1.3342 (1.17); 1.3289 (0.93); 1.3108 (0.36);

0.8756 (0.43); −0.0002 (5.94)

›Example 310, Solvent: DMSO, Spectrometer: 399.95 MHz

10.2343 (1.95); 8.1087 (0.50); 8.0893 (0.32); 7.9529 (1.04); 7.9064 (0.39); 7.8876 (0.32); 7.8227 (0.48); 7.8017 (1.47); 7.7847 (2.76); 7.7794

(1.93); 7.7624 (0.53); 7.7226 (2.31); 7.7048 (3.01); 7.7011 (2.12); 7.6822 (0.56); 7.6642 (0.64); 7.6608 (0.50); 7.5892 (0.36); 7.5695 (0.37);

7.5630 (0.43); 7.5510 (0.37); 7.5447 (1.39); 7.5391 (0.63); 7.5299 (0.99); 7.5264 (1.34); 7.5229 (0.73); 7.4958 (2.30); 7.4924 (0.98); 7.4805

(1.57); 7.4767 (2.96); 7.4630 (0.78); 7.4590 (1.26); 7.4558 (0.76); 7.4514 (0.46); 7.4442 (0.58); 7.4398 (0.66); 7.4280 (0.69); 7.4239 (0.64);

7.4030 (0.34); 7.3382 (0.46); 7.3170 (0.57); 7.2332 (0.38); 7.2250 (3.92); 7.2219 (2.99); 7.2068 (5.84); 7.1038 (1.10); 7.0998 (1.12); 7.0872

(1.05); 7.0832 (1.05); 6.9745 (0.36); 6.8804 (0.36); 6.8730 (3.25); 6.8678 (0.97); 6.8565 (0.94); 6.8513 (2.89); 6.0032 (0.41); 5.5344 (1.14);

5.3314 (4.96); 5.1786 (0.99); 4.2520 (1.21); 4.2346 (2.78); 4.2173 (1.26); 3.7187 (16.00); 3.3402 (147.09); 3.0878 (2.53); 3.0642 (13.07);

3.0361 (3.25); 2.8906 (8.67); 2.8806 (1.16); 2.8632 (2.24); 2.8460 (1.04); 2.7322 (6.81); 2.7310 (6.82); 2.5255 (0.81); 2.5207 (1.32); 2.5122

(16.89); 2.5077 (33.74); 2.5031 (44.53); 2.4984 (32.34); 2.4939 (15.43); −0.0002 (2.35)

›Example 311, Solvent: DMSO, Spectrometer: 399.95 MHz

10.6801 (2.05); 8.0262 (0.75); 8.0054 (0.97); 7.9533 (0.54); 7.8844 (1.30); 7.8652 (1.73); 7.8449 (1.09); 7.7320 (1.88); 7.7293 (2.50); 7.7255

(1.19); 7.7167 (0.73); 7.7116 (3.35); 7.7079 (2.31); 7.5674 (0.47); 7.5555 (0.34); 7.5491 (1.59); 7.5434 (0.46); 7.5341 (0.84); 7.5308 (1.39);

7.5274 (0.69); 7.4996 (2.30); 7.4961 (0.96); 7.4842 (1.56); 7.4805 (2.97); 7.4669 (0.46); 7.4628 (1.20); 7.4596 (0.66); 7.3586 (0.64); 7.3378

(1.37); 7.3200 (1.26); 7.3173 (0.91); 7.2997 (0.59); 7.2070 (1.66); 7.1896 (1.61); 6.8686 (0.56); 6.8626 (1.23); 6.8567 (0.83); 6.8404 (0.46);

6.8346 (1.14); 6.8263 (1.20); 6.8241 (1.70); 6.8208 (1.28); 6.8182 (1.05); 6.8154 (0.70); 6.8034 (1.29); 6.7997 (1.72); 6.7976 (1.56); 6.7945

(1.01); 6.7790 (0.55); 6.7772 (0.50); 6.7730 (0.42); 6.7713 (0.37); 5.3863 (5.92); 4.8317 (6.00); 3.3310 (56.17); 3.0697 (16.00); 2.8905 (4.50);

2.7320 (3.56); 2.7309 (3.46); 2.5252 (0.59); 2.5204 (0.93); 2.5118 (11.75); 2.5073 (23.51); 2.5027 (30.97); 2.4980 (22.33); 2.4935 (10.51); −0.0002

(6.98)

›Example 312, Solvent: DMSO, Spectrometer: 399.95 MHz

12.4977 (1.07); 7.9530 (0.84); 7.7382 (1.90); 7.7354 (2.59); 7.7315 (1.23); 7.7230 (0.79); 7.7178 (3.43); 7.7140 (2.30); 7.5662 (0.47); 7.5547

(0.35); 7.5479 (1.64); 7.5420 (0.48); 7.5331 (0.90); 7.5297 (1.49); 7.5262 (0.73); 7.5031 (2.44); 7.4997 (1.01); 7.4880 (1.58); 7.4840 (3.01);

7.4707 (0.47); 7.4665 (1.22); 7.4630 (0.66); 7.3252 (4.43); 7.0772 (2.42); 7.0568 (2.80); 6.8137 (0.44); 6.8064 (3.66); 6.8014 (1.12); 6.7898

(1.08); 6.7849 (3.15); 5.3337 (5.52); 5.0082 (0.37); 4.9917 (1.44); 4.9751 (1.46); 4.9586 (0.37); 3.3371 (72.07); 3.0111 (16.00); 2.8904 (6.99);

2.7322 (5.42); 2.7310 (5.57); 2.5255 (0.52); 2.5207 (0.86); 2.5122 (10.05); 2.5077 (19.96); 2.5031 (26.22); 2.4985 (18.83); 2.4939 (8.79);

2.1960 (9.43); 1.5253 (5.41); 1.5088 (5.36); −0.0002 (3.46)

›Example 313, Solvent: DMSO, Spectrometer: 399.95 MHz

10.6270 (2.08); 8.0373 (0.90); 8.0167 (1.13); 7.9533 (0.58); 7.8838 (1.37); 7.8645 (1.85); 7.8443 (1.15); 7.7954 (0.39); 7.7303 (2.72); 7.7265

(1.56); 7.7176 (0.93); 7.7124 (3.49); 7.7086 (2.54); 7.5679 (0.51); 7.5647 (0.36); 7.5560 (0.40); 7.5496 (1.74); 7.5439 (0.69); 7.5346 (0.94);

7.5313 (1.53); 7.5279 (0.87); 7.5004 (2.59); 7.4970 (1.36); 7.4850 (1.77); 7.4812 (3.38); 7.4677 (0.56); 7.4636 (1.34); 7.4603 (0.84); 7.3224

(1.90); 7.3158 (0.54); 7.3026 (2.47); 7.2999 (2.29); 7.2896 (0.49); 7.2822 (2.23); 7.2042 (1.83); 7.1864 (1.74); 6.9787 (1.01); 6.9764 (0.98);

6.9660 (2.78); 6.9635 (3.38); 6.9597 (3.35); 6.9494 (1.08); 6.9429 (4.65); 6.9359 (0.32); 5.3856 (6.31); 5.3362 (0.58); 4.7944 (6.74); 3.8868

(0.36); 3.8701 (0.37); 3.3346 (65.65); 3.0692 (16.00); 3.0596 (0.58); 2.8903 (4.69); 2.7319 (3.67); 2.5255 (0.56); 2.5206 (0.90); 2.5121 (9.87);

2.5076 (19.62); 2.5030 (25.88); 2.4984 (18.88); 2.4939 (9.15); 1.2343 (0.56); 0.9274 (1.14); 0.9142 (0.37); 0.9106 (1.13); −0.0002 (5.70)

›Example 314, Solvent: DMSO, Spectrometer: 399.95 MHz

12.4317 (0.74); 7.9526 (1.20); 7.7390 (2.69); 7.7351 (1.30); 7.7266 (0.77); 7.7214 (3.45); 7.7176 (2.40); 7.5666 (0.47); 7.5552 (0.34); 7.5482

(1.66); 7.5423 (0.50); 7.5335 (0.92); 7.5301 (1.51); 7.5267 (0.76); 7.5046 (2.51); 7.5012 (1.07); 7.4895 (1.58); 7.4855 (3.09); 7.4722 (0.47);

7.4681 (1.21); 7.4645 (0.68); 7.3430 (4.60); 7.2834 (1.19); 7.2632 (2.64); 7.2428 (2.00); 7.2274 (1.42); 7.2223 (2.18); 7.2168 (1.66); 7.1772

(1.24); 7.1751 (1.50); 7.1730 (1.24); 7.1708 (1.12); 7.1575 (0.88); 7.1554 (0.93); 7.1532 (0.89); 7.1510 (0.72); 7.0102 (1.04); 7.0082 (1.11);

7.0040 (1.05); 7.0021 (1.00); 6.9894 (0.93); 6.9875 (0.92); 6.9832 (0.93); 6.9813 (0.86); 5.3457 (5.76); 4.8880 (7.21); 3.3347 (91.17); 3.0214

(16.00); 2.8904 (9.66); 2.7318 (7.62); 2.7308 (7.75); 2.5251 (0.80); 2.5202 (1.21); 2.5117 (14.62); 2.5072 (29.20); 2.5026 (38.58); 2.4980

(28.01); 2.4935 (13.36); −0.0002 (3.21)

›Example 315, Solvent: DMSO, Spectrometer: 399.95 MHz

12.4292 (1.10); 7.9524 (0.91); 7.7415 (1.96); 7.7389 (2.67); 7.7350 (1.31); 7.7265 (0.85); 7.7213 (3.46); 7.7175 (2.41); 7.5667 (0.49); 7.5635

(0.34); 7.5553 (0.35); 7.5483 (1.67); 7.5425 (0.53); 7.5337 (0.92); 7.5303 (1.53); 7.5268 (0.79); 7.5048 (2.53); 7.5014 (1.15); 7.4898 (1.63);

7.4858 (3.13); 7.4724 (0.52); 7.4683 (1.24); 7.4647 (0.71); 7.3352 (4.68); 7.3280 (0.42); 7.3212 (1.97); 7.3156 (0.68); 7.3087 (0.50); 7.2989

(2.61); 7.2927 (0.37); 7.2872 (0.74); 7.2811 (2.16); 6.9835 (1.01); 6.9813 (0.90); 6.9667 (4.14); 6.9515 (1.30); 6.9461 (5.18); 5.3429 (5.92);

4.8426 (8.14); 4.8334 (0.55); 3.3374 (135.09); 3.3008 (0.33); 3.0224 (16.00); 2.8902 (7.54); 2.7316 (5.86); 2.7307 (5.95); 2.5248 (0.78); 2.5116

(14.77); 2.5071 (29.36); 2.5025 (38.78); 2.4979 (28.33); 2.4934 (13.71); 1.2348 (0.34); 1.1312 (0.55); 1.1160 (0.54); 0.0080 (0.37); −0.0002

(10.08)

›Example 316, Solvent: DMSO, Spectrometer: 399.95 MHz

9.7797 (1.56); 8.0154 (1.22); 7.9956 (1.55); 7.8351 (1.07); 7.8160 (1.38); 7.7955 (0.95); 7.7281 (1.63); 7.7256 (2.08); 7.7218 (0.98); 7.7130

(0.64); 7.7079 (2.76); 7.7041 (1.91); 7.5637 (0.40); 7.5454 (1.33); 7.5397 (0.39); 7.5304 (0.69); 7.5271 (1.15); 7.5237 (0.58); 7.4951 (1.93);

7.4917 (0.83); 7.4796 (1.32); 7.4759 (2.50); 7.4623 (0.38); 7.4582 (1.00); 7.4551 (0.56); 7.1526 (1.38); 7.1350 (1.34); 5.3778 (4.99); 3.3271

(28.80); 3.1371 (0.50); 3.0675 (12.85); 2.5252 (0.48); 2.5204 (0.75); 2.5119 (9.13); 2.5073 (18.30); 2.5027 (24.18); 2.4981 (17.49); 2.4935

(8.27); 1.6465 (0.87); 1.6259 (0.76); 1.6175 (0.62); 1.6054 (1.01); 1.2727 (0.40); 1.2534 (0.96); 1.2353 (1.45); 1.2179 (0.87); 1.1885 (16.00);

1.1730 (1.20); 1.1623 (0.77); 1.1555 (0.63); 1.1440 (0.73); 1.1360 (0.58); 1.1287 (0.42); 1.1217 (0.45); 0.8557 (2.82); 0.8379 (5.68); 0.8196

(2.37); −0.0002 (9.76)

›Example 317, Solvent: DMSO, Spectrometer: 400.13 MHz

10.1338 (1.76); 7.8350 (0.51); 7.8142 (1.18); 7.7964 (1.33); 7.7795 (1.74); 7.7609 (0.75); 7.7317 (1.99); 7.7138 (2.40); 7.7102 (1.83); 7.5702

(0.34); 7.5584 (0.33); 7.5518 (1.17); 7.5465 (0.46); 7.5337 (1.03); 7.5038 (1.79); 7.4846 (2.24); 7.4670 (0.89); 7.1163 (1.11); 7.1003 (1.09);

5.7646 (4.79); 5.3393 (4.53); 3.5385 (3.49); 3.3282 (12.06); 3.3043 (1.20); 3.0957 (0.40); 3.0742 (10.25); 2.5146 (14.75); 2.5102 (19.75);

2.5059 (15.03); 2.4650 (0.47); 2.4605 (0.46); 1.9972 (0.51); 1.6757 (16.00); 1.6259 (0.32); 1.3742 (0.56)

›Example 318, Solvent: DMSO, Spectrometer: 399.95 MHz

12.4153 (0.70); 7.9530 (0.69); 7.7402 (2.57); 7.7363 (1.28); 7.7277 (0.77); 7.7226 (3.27); 7.7188 (2.30); 7.5665 (0.45); 7.5551 (0.32); 7.5481

(1.60); 7.5423 (0.49); 7.5335 (0.89); 7.5301 (1.46); 7.5266 (0.75); 7.5047 (2.43); 7.5014 (1.08); 7.4897 (1.54); 7.4857 (2.97); 7.4723 (0.47);

7.4682 (1.17); 7.4647 (0.67); 7.3372 (4.45); 7.2124 (1.11); 7.1936 (1.02); 7.1889 (1.27); 7.1761 (0.39); 7.1704 (1.14); 6.5674 (0.60); 6.5630

(1.09); 6.5598 (1.25); 6.5517 (0.54); 6.5452 (4.82); 6.5414 (5.79); 6.5253 (1.07); 6.5213 (1.17); 6.5174 (0.58); 5.3454 (5.49); 4.8238 (6.77);

3.7825 (0.48); 3.7233 (16.00); 3.3357 (39.45); 3.0205 (14.29); 2.8899 (5.54); 2.7318 (4.27); 2.7309 (4.41); 2.5253 (0.35); 2.5204 (0.56); 2.5120

(6.85); 2.5075 (13.71); 2.5029 (18.17); 2.4983 (13.29); 2.4938 (6.42); −0.0002 (3.59)

›Example 319, Solvent: DMSO, Spectrometer: 400.13 MHz

7.6252 (3.43); 7.6045 (3.97); 7.3099 (7.22); 7.3018 (2.61); 7.2960 (1.28); 7.2885 (3.34); 7.2832 (3.38); 7.2801 (2.98); 7.2662 (0.90); 7.2615

(2.31); 7.2557 (0.33); 7.2066 (0.49); 7.2041 (0.49); 7.1855 (0.37); 6.9577 (1.06); 6.9393 (1.89); 6.9207 (1.50); 6.9166 (2.90); 6.9143 (3.19);

6.8946 (2.91); 6.8224 (0.61); 6.8025 (0.49); 5.3124 (5.92); 5.0675 (0.41); 5.0511 (1.47); 5.0345 (1.48); 5.0181 (0.41); 3.3657 (19.18); 3.0017

(16.00); 2.5578 (0.36); 2.5303 (0.59); 2.5168 (11.86); 2.5124 (24.30); 2.5080 (32.65); 2.5035 (23.38); 2.4992 (11.02); 2.4580 (0.36); 2.3543

(9.77); 2.3350 (0.34); 1.9942 (0.85); 1.5485 (5.79); 1.5319 (5.78); 1.4177 (0.87); 1.4009 (0.86); 1.2493 (1.28); 1.1785 (0.47); 0.8785 (0.58);

0.8617 (1.87); 0.8441 (0.74)

›Example 320, Solvent: DMSO, Spectrometer: 400.13 MHz

10.9991 (2.97); 7.8393 (4.30); 7.8291 (3.79); 7.7294 (2.72); 7.7165 (0.96); 7.7115 (3.51); 7.7078 (2.54); 7.5691 (0.50); 7.5659 (0.35); 7.5571

(0.41); 7.5508 (1.72); 7.5452 (0.57); 7.5358 (0.98); 7.5325 (1.49); 7.5293 (0.81); 7.5013 (2.52); 7.4857 (1.83); 7.4821 (3.24); 7.4683 (0.66);

7.4644 (1.42); 7.4613 (0.90); 7.1624 (1.29); 7.1518 (2.06); 7.1415 (1.28); 5.7665 (4.47); 5.3558 (6.58); 3.3905 (0.41); 3.3403 (28.15); 3.2898

(0.38); 3.0603 (16.00); 2.8748 (1.96); 2.8568 (3.37); 2.8386 (2.06); 2.5624 (0.42); 2.5580 (0.59); 2.5536 (0.45); 2.5300 (1.29); 2.5166 (15.51);

2.5122 (31.16); 2.5078 (41.93); 2.5033 (30.56); 2.4990 (15.36); 2.4668 (0.80); 2.4620 (0.80); 2.4574 (0.81); 2.4529 (0.60); 1.9948 (0.57);

1.5845 (0.44); 1.5670 (1.20); 1.5483 (1.96); 1.5426 (1.04); 1.5310 (1.48); 1.5112 (0.67); 1.4100 (0.35); 1.3916 (1.16); 1.3726 (1.78); 1.3536

(1.74); 1.3359 (1.04); 1.3178 (0.34); 1.1792 (0.32); 0.9091 (4.22); 0.9016 (0.56); 0.8908 (8.65); 0.8724 (3.76); 0.8626 (0.53)

›Example 321, Solvent: DMSO, Spectrometer: 399.95 MHz

12.5670 (0.86); 7.9540 (0.93); 7.7375 (2.93); 7.7337 (1.42); 7.7247 (0.85); 7.7198 (3.63); 7.7159 (2.53); 7.5663 (0.50); 7.5631 (0.32); 7.5548

(0.36); 7.5478 (1.81); 7.5421 (0.52); 7.5331 (0.98); 7.5298 (1.58); 7.5264 (0.80); 7.5034 (2.72); 7.5001 (1.16); 7.4881 (1.77); 7.4842 (3.37);

7.4708 (0.52); 7.4667 (1.29); 7.4633 (0.74); 7.3461 (4.72); 7.3312 (1.09); 7.3279 (0.56); 7.3102 (2.36); 7.3037 (0.33); 7.2889 (1.57); 7.0250

(3.80); 7.0214 (3.46); 7.0153 (1.44); 7.0057 (1.38); 7.0028 (0.89); 6.9097 (1.02); 6.9063 (1.14); 6.9017 (0.93); 6.8874 (1.05); 6.8824 (0.99);

5.3439 (6.21); 5.1257 (0.41); 5.1093 (1.54); 5.0928 (1.56); 5.0763 (0.42); 3.3415 (50.51); 3.0153 (16.00); 2.8911 (7.51); 2.7325 (6.13); 2.5269

(0.35); 2.5136 (7.04); 2.5091 (14.06); 2.5046 (18.55); 2.5000 (13.49); 2.4955 (6.47); 1.5507 (6.03); 1.5342 (5.92); −0.0002 (4.06)

›Example 322, Solvent: DMSO, Spectrometer: 400.13 MHz

7.7379 (2.94); 7.7200 (3.52); 7.7163 (2.56); 7.5694 (0.52); 7.5578 (0.44); 7.5510 (1.74); 7.5455 (0.60); 7.5361 (1.02); 7.5330 (1.53); 7.5064

(2.70); 7.4872 (3.32); 7.4736 (0.59); 7.4697 (1.24); 7.3255 (5.12); 7.3002 (1.89); 7.2954 (0.97); 7.2820 (4.64); 7.2606 (4.97); 7.2472 (0.96);

7.2425 (2.28); 6.9589 (1.11); 6.9404 (2.25); 6.9183 (5.27); 6.8990 (3.84); 6.8659 (3.36); 6.8462 (3.04); 5.7584 (1.12); 5.3394 (6.42); 4.8693

(0.96); 4.8533 (1.96); 4.8379 (0.96); 4.5790 (1.00); 4.5662 (1.20); 4.5616 (1.30); 4.5487 (1.00); 3.3932 (4.87); 3.2928 (2.26); 3.1888 (0.79);

3.0122 (16.00); 2.9105 (0.57); 2.8929 (1.41); 2.8748 (1.43); 2.8568 (0.56); 2.5111 (24.58); 2.5067 (32.65); 2.5024 (23.72); 1.9635 (0.42);

1.9451 (1.56); 1.9272 (2.16); 1.9105 (1.87); 1.8889 (1.18); 1.8759 (0.93); 1.8691 (1.52); 1.8572 (0.92); 1.8503 (1.66); 1.8322 (1.13); 1.8149

(0.58); 1.1116 (2.12); 1.0936 (4.34); 1.0754 (2.05); 1.0080 (4.98); 0.9896 (10.27); 0.9710 (4.87)

›Example 323, Solvent: DMSO, Spectrometer: 399.95 MHz

10.6044 (0.99); 10.4354 (1.93); 8.0787 (0.63); 8.0580 (0.75); 7.9790 (1.43); 7.9572 (2.24); 7.8334 (0.64); 7.8142 (0.90); 7.7970 (1.39); 7.7780

(1.69); 7.7576 (1.12); 7.7265 (3.64); 7.7135 (1.07); 7.7087 (4.56); 7.7050 (3.21); 7.5689 (0.38); 7.5658 (0.68); 7.5626 (0.43); 7.5539 (0.51);

7.5475 (2.35); 7.5418 (0.67); 7.5326 (1.26); 7.5293 (2.03); 7.5259 (1.02); 7.4989 (3.43); 7.4957 (1.48); 7.4834 (2.33); 7.4797 (4.36); 7.4661

(0.67); 7.4621 (1.68); 7.4589 (0.96); 7.1395 (0.90); 7.1202 (1.06); 7.1163 (1.76); 7.0977 (1.65); 6.1620 (2.27); 6.1552 (1.74); 6.1486 (1.15);

6.1410 (1.11); 5.8283 (1.01); 5.8213 (1.02); 5.8143 (0.95); 5.8072 (0.92); 5.3617 (7.82); 3.3316 (117.10); 3.3079 (1.30); 3.1502 (0.43); 3.1402

(0.78); 3.1296 (0.66); 3.1178 (0.78); 3.1077 (0.45); 3.0716 (16.00); 3.0612 (8.68); 2.9179 (0.75); 2.8908 (12.80); 2.8643 (1.07); 2.7320 (10.02);

2.7309 (9.50); 2.6718 (0.34); 2.5251 (1.02); 2.5202 (1.58); 2.5117 (20.05); 2.5072 (39.90); 2.5026 (52.31); 2.4980 (37.67); 2.4935 (17.75);

2.4637 (0.34); 2.4537 (0.38); 2.4430 (0.36); 2.4321 (0.34); 2.3294 (0.33); 1.8768 (0.37); 1.8476 (0.40); 1.8195 (0.41); 1.8102 (0.44); 1.7966

(0.50); 1.7909 (0.69); 1.7876 (0.62); 1.7818 (0.53); 1.7683 (0.48); 1.7591 (0.44); 1.6280 (0.52); 1.6081 (0.56); 1.4122 (0.47); 1.4063 (0.58);

1.4017 (0.54); 1.3956 (0.51); 1.3836 (0.42); 1.3778 (0.51); 1.3732 (0.47); 1.3672 (0.45); 1.3235 (0.41); 1.3186 (0.37); 1.3031 (1.18); 1.2983

(1.30); 1.2931 (0.81); 1.2835 (1.60); 1.2685 (0.70); 1.2634 (0.79); 1.2409 (0.35); 1.2349 (0.43); 1.2254 (0.47); 1.2056 (0.37); 0.0080

(0.34); −0.0002 (10.51)

›Example 324, Solvent: CDCl3, Spectrometer: 300.16 MHz

8.1893 (1.90); 8.1624 (2.14); 7.8514 (2.74); 7.7462 (1.30); 7.7201 (2.44); 7.6936 (1.39); 7.6449 (3.76); 7.6305 (2.84); 7.3211 (1.25); 7.2968

(3.76); 7.2671 (5.70); 7.2520 (6.74); 7.2466 (6.67); 7.2265 (4.57); 7.1382 (2.37); 7.1101 (4.43); 7.0754 (3.73); 7.0471 (2.34); 5.2736 (9.20);

3.0797 (16.00); 3.0368 (2.87); 2.7426 (2.75); 2.7168 (4.45); 2.6922 (2.18); 2.0047 (1.07); −0.0002 (1.49)

›Example 325, Solvent: DMSO, Spectrometer: 400.13 MHz

10.2707 (2.81); 7.8308 (0.57); 7.8098 (1.73); 7.7927 (2.57); 7.7903 (2.20); 7.7861 (2.23); 7.7689 (0.62); 7.7653 (0.39); 7.4220 (1.01); 7.4021

(2.17); 7.3820 (1.57); 7.3181 (8.50); 7.3071 (9.73); 7.2974 (0.48); 7.2844 (1.53); 7.2809 (1.28); 7.2673 (0.83); 7.2636 (1.20); 7.2614 (1.02);

7.2457 (1.76); 7.2391 (2.78); 7.2361 (2.05); 7.2272 (1.18); 7.2151 (0.58); 7.1442 (1.07); 7.1425 (1.11); 7.1379 (0.99); 7.1363 (0.95); 7.1237

(0.96); 7.1218 (0.93); 7.1173 (0.94); 7.1153 (0.89); 7.1100 (1.38); 7.1063 (1.37); 7.0932 (1.28); 7.0894 (1.28); 5.7672 (6.91); 5.3371 (5.77);

4.3097 (1.63); 4.2924 (3.64); 4.2752 (1.67); 3.7886 (16.00); 3.4026 (1.13); 3.3522 (124.45); 3.3013 (1.15); 3.0531 (14.26); 2.9572 (1.57);

2.9399 (3.30); 2.9227 (1.50); 2.5599 (0.39); 2.5322 (0.61); 2.5187 (13.05); 2.5143 (27.08); 2.5099 (36.73); 2.5054 (26.27); 2.5010 (12.20);

2.4589 (0.37); 1.9964 (0.46); 1.2499 (0.40); 0.8639 (0.57)

›Example 326, Solvent: DMSO, Spectrometer: 400.13 MHz

7.6240 (3.18); 7.6034 (3.68); 7.3073 (2.91); 7.2872 (2.56); 6.9984 (3.45); 6.6183 (3.43); 5.0954 (6.06); 4.0425 (0.33); 4.0247 (0.34); 3.4017

(1.53); 3.3515 (96.15); 3.3014 (1.20); 3.0355 (16.00); 2.5304 (0.36); 2.5256 (0.58); 2.5170 (6.14); 2.5125 (12.69); 2.5080 (17.18); 2.5035

(12.15); 2.4990 (5.59); 2.3549 (9.06); 1.9942 (1.50); 1.1971 (0.40); 1.1793 (0.82); 1.1615 (0.39)

›Example 327, Solvent: DMSO, Spectrometer: 399.95 MHz

10.7598 (2.34); 8.1621 (1.47); 8.1418 (1.74); 7.9523 (0.98); 7.9060 (1.29); 7.8865 (1.81); 7.8664 (1.19); 7.7321 (2.68); 7.7283 (1.36); 7.7194

(0.80); 7.7143 (3.48); 7.7106 (2.42); 7.5659 (0.50); 7.5540 (0.35); 7.5475 (1.69); 7.5418 (0.49); 7.5326 (0.92); 7.5293 (1.50); 7.5259 (0.79);

7.4993 (2.48); 7.4961 (1.07); 7.4839 (1.67); 7.4802 (3.16); 7.4666 (0.48); 7.4626 (1.25); 7.4593 (0.71); 7.2973 (2.07); 7.2141 (1.81); 7.1964

(2.13); 7.1806 (1.75); 7.1771 (1.76); 7.1659 (2.86); 7.1464 (0.75); 5.3763 (6.18); 3.3460 (124.75); 3.0868 (16.00); 3.0776 (0.82); 3.0723 (0.46);

2.8906 (7.90); 2.7321 (6.17); 2.7312 (6.26); 2.5257 (0.61); 2.5209 (0.95); 2.5124 (11.99); 2.5078 (24.04); 2.5032 (31.79); 2.4986 (23.03);

2.4941 (10.93); 2.3341 (9.59); 2.3055 (8.92); −0.0002 (7.13)

›Example 328, Solvent: DMSO, Spectrometer: 400.13 MHz

10.5372 (1.96); 8.1004 (1.32); 8.0797 (1.57); 7.8440 (1.17); 7.8248 (1.62); 7.8045 (1.12); 7.4238 (1.00); 7.4038 (2.12); 7.3837 (1.56); 7.2895

(1.00); 7.2872 (1.33); 7.2857 (1.36); 7.2834 (1.26); 7.2702 (0.77); 7.2662 (1.16); 7.2640 (0.97); 7.2452 (1.47); 7.2393 (1.90); 7.2352 (1.40);

7.1517 (1.79); 7.1472 (1.25); 7.1450 (1.25); 7.1406 (1.14); 7.1384 (1.23); 7.1345 (1.81); 7.1264 (1.04); 7.1243 (1.00); 7.1200 (0.96); 7.1179

(0.86); 5.7690 (1.09); 5.3659 (5.52); 3.7891 (16.00); 3.7678 (0.41); 3.7601 (0.43); 3.3995 (1.96); 3.3494 (140.76); 3.3261 (1.70); 3.2996 (2.16);

3.0471 (14.86); 2.6932 (0.51); 2.6836 (0.59); 2.6792 (0.72); 2.6624 (0.37); 2.5603 (0.44); 2.5326 (0.44); 2.5191 (12.00); 2.5147 (25.85); 2.5102

(36.06); 2.5057 (26.73); 2.5013 (13.49); 2.4697 (0.68); 2.4650 (0.73); 2.4604 (0.75); 2.4559 (0.56); 1.5933 (0.43); 1.5889 (0.37); 1.5792 (0.46);

1.5728 (0.51); 1.5673 (0.39); 1.5579 (0.53); 1.3672 (0.69); 1.3318 (0.38); 1.3200 (0.47); 1.3065 (0.70); 1.2871 (0.87); 1.2728 (1.30); 1.2621

(0.71); 1.2528 (1.16); 1.2374 (0.92); 1.2198 (0.48); 1.2125 (0.34); 1.0700 (5.63); 1.0530 (5.66); 0.8844 (2.63); 0.8665 (5.38); 0.8485 (2.16)

›Example 329, Solvent: DMSO, Spectrometer: 399.95 MHz

10.9504 (2.41); 8.1344 (1.61); 8.1145 (1.96); 7.9535 (0.81); 7.9139 (1.31); 7.8946 (1.80); 7.8744 (1.20); 7.8248 (0.88); 7.8223 (1.15); 7.8187

(0.93); 7.8054 (1.03); 7.8017 (1.31); 7.7993 (1.00); 7.7325 (2.04); 7.7299 (2.67); 7.7261 (1.32); 7.7173 (0.87); 7.7122 (3.49); 7.7084 (2.44);

7.6280 (1.50); 7.6227 (1.93); 7.6180 (1.45); 7.5681 (0.33); 7.5652 (0.52); 7.5620 (0.35); 7.5532 (0.44); 7.5459 (2.53); 7.5413 (0.65); 7.5319

(1.02); 7.5283 (1.87); 7.5252 (3.14); 7.5053 (1.57); 7.4975 (2.43); 7.4941 (1.07); 7.4821 (1.69); 7.4784 (3.11); 7.4648 (0.56); 7.4607 (1.40);

7.4577 (1.09); 7.4524 (1.98); 7.4471 (0.73); 7.4397 (0.59); 7.4338 (2.83); 7.4310 (2.69); 7.4252 (0.43); 7.4173 (0.96); 7.4123 (2.43); 7.2653

(1.04); 7.2632 (1.12); 7.2590 (1.03); 7.2570 (1.01); 7.2449 (0.94); 7.2428 (0.94); 7.2386 (0.96); 7.2365 (0.90); 7.2256 (1.85); 7.2072 (2.89);

7.1887 (1.90); 7.1728 (0.47); 7.1702 (0.82); 7.1676 (0.47); 7.0967 (2.58); 7.0940 (3.16); 7.0887 (0.87); 7.0797 (0.94); 7.0775 (1.54); 7.0749

(2.73); 7.0726 (2.29); 7.0661 (0.33); 5.4049 (5.99); 3.3296 (62.97); 3.0799 (0.33); 3.0675 (16.00); 2.8906 (6.62); 2.7320 (5.17); 2.7311 (5.11);

2.5251 (0.76); 2.5202 (1.21); 2.5118 (13.85); 2.5073 (27.56); 2.5027 (36.33); 2.4980 (26.37); 2.4935 (12.57); 1.2898 (0.51); 0.0079 (0.34); −0.0002

(9.72)

›Example 331, Solvent: DMSO, Spectrometer: 399.95 MHz

11.0401 (2.57); 8.1582 (0.66); 8.1381 (0.77); 7.9294 (1.25); 7.9093 (3.59); 7.8888 (3.02); 7.7294 (2.91); 7.7115 (3.66); 7.7079 (2.66); 7.5630

(0.53); 7.5599 (0.34); 7.5511 (0.42); 7.5447 (1.75); 7.5390 (0.56); 7.5295 (1.03); 7.5264 (1.53); 7.5231 (0.82); 7.4958 (2.72); 7.4925 (1.51);

7.4766 (3.79); 7.4733 (2.64); 7.4625 (2.88); 7.4558 (4.95); 7.4439 (0.57); 7.2371 (1.95); 7.2265 (1.08); 7.2191 (2.64); 7.2111 (1.03); 7.2067

(1.10); 7.2040 (0.98); 7.1992 (0.81); 7.1916 (0.81); 7.1840 (0.73); 5.3767 (5.29); 3.3329 (31.64); 3.3266 (39.78); 3.0858 (16.00); 2.8898 (1.00);

2.7302 (0.83); 2.5237 (1.02); 2.5102 (18.01); 2.5060 (33.96); 2.5015 (43.58); 2.4970 (31.82); 2.4926 (15.48); 0.0079 (0.55); −0.0002

(13.09); −0.0085 (0.46)

›Example 332, Solvent: DMSO, Spectrometer: 399.95 MHz

11.1771 (2.60); 8.1574 (0.59); 8.1376 (0.68); 7.9524 (1.45); 7.9370 (1.28); 7.9174 (1.90); 7.8975 (1.13); 7.7298 (3.63); 7.7255 (5.59); 7.7129

(0.96); 7.7078 (3.66); 7.7042 (2.65); 7.6147 (2.05); 7.5941 (3.25); 7.5646 (0.56); 7.5526 (0.41); 7.5463 (1.80); 7.5407 (0.60); 7.5305 (3.04);

7.5283 (2.43); 7.5255 (2.83); 7.5099 (1.44); 7.5048 (1.56); 7.4967 (2.71); 7.4810 (1.91); 7.4774 (3.38); 7.4638 (0.56); 7.4598 (1.29); 7.4568

(0.80); 7.2497 (1.89); 7.2311 (1.80); 5.3772 (4.44); 3.3362 (67.00); 3.3337 (97.23); 3.0721 (16.00); 2.8904 (10.48); 2.7309 (8.65); 2.5248 (0.74);

2.5114 (14.81); 2.5071 (29.40); 2.5025 (38.83); 2.4980 (28.68); 2.4936 (14.10); −0.0002 (4.73)

›Example 333, Solvent: DMSO, Spectrometer: 300.16 MHz

9.8162 (1.07); 7.7866 (0.39); 7.7457 (0.73); 7.7216 (1.07); 7.7077 (3.99); 7.6938 (0.53); 7.6806 (0.38); 7.4843 (1.39); 7.4549 (1.52); 7.1399

(0.67); 7.1177 (0.73); 7.0930 (0.35); 7.0560 (7.69); 6.9663 (1.52); 6.9368 (1.35); 5.3862 (0.48); 5.1534 (2.18); 4.0814 (0.50); 4.0577 (1.53);

4.0339 (1.56); 4.0103 (0.53); 3.8358 (1.09); 3.7949 (0.46); 3.7814 (5.68); 2.5266 (1.11); 2.5211 (1.47); 2.5156 (1.09); 2.0068 (6.43); 1.4777

(16.00); 1.2146 (1.68); 1.1909 (3.31); 1.1672 (1.64)

›Example 334, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5735 (2.04); 8.0370 (0.83); 8.0163 (1.06); 7.9528 (0.46); 7.8839 (1.29); 7.8647 (1.75); 7.8444 (1.10); 7.7311 (1.91); 7.7284 (2.51); 7.7246

(1.20); 7.7159 (0.74); 7.7107 (3.37); 7.7070 (2.34); 7.5670 (0.48); 7.5551 (0.34); 7.5488 (1.60); 7.5430 (0.47); 7.5338 (0.85); 7.5304 (1.40);

7.5270 (0.69); 7.4991 (2.30); 7.4956 (0.97); 7.4837 (1.59); 7.4800 (3.00); 7.4664 (0.46); 7.4623 (1.22); 7.4591 (0.67); 7.2044 (1.70); 7.1861

(1.78); 7.1704 (1.78); 7.1497 (1.05); 6.7869 (3.05); 6.7701 (1.09); 6.7687 (1.09); 6.7526 (0.84); 6.7489 (0.89); 6.7449 (0.60); 6.7315 (0.85);

6.7251 (0.69); 5.3834 (5.94); 4.7651 (6.17); 3.3380 (87.86); 3.0675 (16.00); 2.8905 (3.90); 2.7320 (3.13); 2.7309 (2.98); 2.5254 (0.60); 2.5206

(0.95); 2.5120 (11.85); 2.5075 (23.70); 2.5029 (31.15); 2.4983 (22.41); 2.4937 (10.52); 2.2718 (9.63); −0.0002 (1.06)

›Example 335, Solvent: DMSO, Spectrometer: 399.95 MHz

10.8446 (1.99); 8.0209 (0.87); 8.0003 (1.08); 7.9528 (1.10); 7.8447 (1.33); 7.8255 (1.79); 7.8052 (1.17); 7.7315 (2.67); 7.7275 (1.28); 7.7186

(0.82); 7.7136 (3.47); 7.7098 (2.40); 7.6157 (1.48); 7.6129 (1.48); 7.5958 (1.67); 7.5929 (1.61); 7.5688 (0.49); 7.5570 (0.35); 7.5504 (1.67);

7.5448 (0.49); 7.5356 (0.89); 7.5323 (1.44); 7.5290 (0.73); 7.5017 (2.41); 7.4984 (1.04); 7.4862 (1.66); 7.4825 (3.09); 7.4689 (0.49); 7.4648

(1.21); 7.4617 (0.68); 7.4224 (0.86); 7.4180 (0.95); 7.4034 (1.69); 7.3990 (1.61); 7.3695 (0.98); 7.3666 (0.97); 7.3511 (1.61); 7.3481 (1.51);

7.3324 (0.74); 7.3294 (0.69); 7.2373 (0.91); 7.2327 (0.91); 7.2178 (1.21); 7.2135 (1.15); 7.1990 (0.69); 7.1945 (0.62); 7.1670 (1.82); 7.1491

(1.74); 5.3809 (6.19); 3.9370 (5.68); 3.3354 (140.14); 3.3090 (0.35); 3.0674 (16.00); 2.8904 (9.16); 2.7313 (7.18); 2.5251 (0.83); 2.5201 (1.35);

2.5117 (15.68); 2.5072 (30.91); 2.5026 (40.50); 2.4980 (29.29); 2.4935 (13.85); −0.0002 (3.42)

›Example 336, Solvent: DMSO, Spectrometer: 399.95 MHz

12.4786 (2.21); 7.9529 (1.52); 7.7420 (3.01); 7.7242 (3.76); 7.7204 (2.69); 7.5661 (0.54); 7.5629 (0.38); 7.5547 (0.48); 7.5478 (1.81); 7.5419

(0.65); 7.5330 (1.19); 7.5297 (1.68); 7.5263 (0.91); 7.5052 (2.78); 7.4900 (2.12); 7.4862 (3.46); 7.4726 (0.75); 7.4686 (1.41); 7.4651 (0.85);

7.3748 (2.53); 7.3540 (4.70); 7.2546 (0.81); 7.2351 (1.91); 7.2324 (1.87); 7.2090 (2.85); 7.1895 (1.17); 5.3579 (6.69); 3.3459 (152.72); 3.0510

(16.00); 2.8913 (11.04); 2.7325 (9.33); 2.5123 (16.67); 2.5080 (29.40); 2.5035 (36.54); 2.4990 (26.79); 2.4947 (13.64); 2.3392 (10.84); 2.3099

(10.35); −0.0002 (2.20)

›Example 337, Solvent: DMSO, Spectrometer: 399.95 MHz

10.1862 (2.95); 7.9534 (0.44); 7.8307 (0.54); 7.8097 (2.03); 7.7940 (4.41); 7.7908 (3.18); 7.7744 (0.63); 7.7236 (2.85); 7.7058 (3.61); 7.7022

(2.59); 7.5629 (0.52); 7.5598 (0.34); 7.5510 (0.40); 7.5446 (1.72); 7.5390 (0.54); 7.5295 (1.01); 7.5264 (1.50); 7.5231 (0.80); 7.4960 (2.59);

7.4802 (1.94); 7.4769 (3.32); 7.4630 (0.58); 7.4592 (1.29); 7.4561 (0.78); 7.1029 (1.46); 7.0983 (1.45); 7.0869 (1.36); 7.0823 (1.38); 5.3351

(6.99); 3.9970 (0.94); 3.9821 (0.97); 3.9705 (1.49); 3.9556 (1.54); 3.8991 (1.51); 3.8821 (1.50); 3.8727 (0.96); 3.8555 (0.95); 3.3407 (108.77);

3.0658 (16.00); 2.8913 (3.20); 2.7327 (2.69); 2.7319 (2.63); 2.5258 (0.67); 2.5124 (11.47); 2.5082 (21.72); 2.5037 (27.88); 2.4992 (20.48);

2.4948 (10.09); 1.8031 (0.35); 1.7862 (0.53); 1.7707 (0.54); 1.7555 (0.38); 1.3887 (0.65); 1.3765 (1.06); 1.3689 (1.10); 1.3600 (1.18); 1.3549

(0.95); 1.3473 (0.96); 1.3411 (0.84); 1.3345 (0.66); 1.3259 (0.53); 1.3165 (0.44); 1.3110 (0.38); 1.3081 (0.37); 1.2857 (0.50); 1.2815 (0.60);

1.2746 (0.44); 1.2636 (0.60); 1.2456 (0.39); 1.2348 (0.43); 1.1501 (0.42); 1.1284 (0.70); 1.1131 (0.48); 1.1082 (0.69); 1.0886 (0.35); 0.9151

(7.35); 0.8982 (7.21); 0.8915 (3.49); 0.8735 (5.28); 0.8561 (2.17); −0.0002 (1.69)

›Example 338, Solvent: DMSO, Spectrometer: 400.13 MHz

12.5513 (1.17); 7.6263 (1.09); 7.6205 (1.13); 7.6179 (1.06); 7.6144 (1.30); 7.6111 (0.95); 7.6054 (0.98); 7.5949 (3.13); 7.5701 (0.78); 7.5561

(0.92); 7.5500 (1.21); 7.5357 (1.22); 7.5307 (0.75); 7.5149 (0.53); 7.4333 (0.56); 7.4307 (0.65); 7.4271 (0.60); 7.4245 (0.57); 7.4095 (1.05);

7.4052 (0.93); 7.3912 (0.51); 7.3881 (0.52); 7.3824 (0.41); 7.3566 (4.83); 7.3044 (1.84); 7.2858 (2.87); 7.2829 (2.93); 7.2643 (2.36); 6.9620

(1.09); 6.9437 (1.94); 6.9250 (1.40); 6.9166 (3.31); 6.8969 (2.97); 5.3601 (6.34); 5.0709 (0.44); 5.0545 (1.58); 5.0379 (1.60); 5.0215 (0.46);

3.3929 (2.83); 3.3899 (2.70); 3.3520 (253.47); 3.3140 (2.34); 3.3114 (2.50); 3.0141 (16.00); 2.5491 (0.83); 2.5451 (0.86); 2.5302 (1.04); 2.5166

(19.07); 2.5124 (38.30); 2.5080 (51.33); 2.5036 (37.65); 2.4711 (0.82); 2.4670 (0.79); 2.3348 (0.32); 1.9940 (1.18); 1.5532 (6.01); 1.5367 (6.00);

1.2496 (0.83); 1.1969 (0.34); 1.1791 (0.64); 0.8790 (0.36); 0.8623 (1.06); 0.8446 (0.43)

›Example 339, Solvent: DMSO, Spectrometer: 400.13 MHz

11.7047 (1.36); 9.3587 (0.63); 7.6178 (3.59); 7.5972 (4.11); 7.3051 (3.39); 7.2849 (3.06); 7.2361 (4.24); 7.0024 (0.53); 6.9802 (1.03); 6.9581

(0.62); 6.7544 (0.67); 6.7430 (0.69); 6.7373 (0.37); 6.7318 (0.56); 6.7204 (0.53); 5.7642 (5.42); 5.2561 (6.14); 4.7129 (0.43); 4.6996 (0.53);

4.6901 (0.80); 4.6805 (0.61); 4.6677 (0.42); 3.3989 (0.92); 3.3491 (61.31); 3.2987 (1.04); 3.2816 (0.37); 3.0239 (16.00); 2.5579 (0.41); 2.5534

(0.34); 2.5167 (11.74); 2.5124 (23.24); 2.5080 (31.00); 2.5035 (22.77); 2.4993 (11.62); 2.4669 (0.67); 2.4622 (0.71); 2.4576 (0.72); 2.3524

(10.31); 1.9943 (0.57); 1.9148 (0.85); 1.8958 (0.91); 1.8832 (1.04); 1.8713 (1.12); 1.8640 (1.12); 1.7223 (0.91); 1.7130 (0.98); 1.7003 (1.04);

1.6924 (1.00); 1.5303 (0.48); 1.5199 (0.51); 1.5002 (0.57); 1.4660 (0.54); 1.4594 (0.44); 1.4340 (1.01); 1.4095 (1.30); 1.3838 (1.40); 1.3571

(1.24); 1.3311 (0.97); 1.3251 (1.05); 1.3055 (0.47); 1.2982 (0.56); 1.2685 (0.47); 1.2593 (0.41); 1.2389 (0.78); 1.2120 (0.47); 1.1969 (0.39);

1.1791 (0.45)

›Example 340, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5036 (1.94); 8.0858 (1.31); 8.0652 (1.55); 7.8345 (1.28); 7.8151 (1.77); 7.7949 (1.20); 7.7260 (2.01); 7.7236 (2.59); 7.7197 (1.30); 7.7108

(0.81); 7.7057 (3.49); 7.7019 (2.40); 7.5644 (0.49); 7.5525 (0.37); 7.5461 (1.64); 7.5404 (0.49); 7.5311 (0.88); 7.5278 (1.42); 7.5245 (0.73);

7.4967 (2.43); 7.4933 (1.06); 7.4813 (1.66); 7.4776 (3.09); 7.4640 (0.48); 7.4599 (1.23); 7.4567 (0.68); 7.1437 (1.77); 7.1261 (1.72); 5.3567

(6.33); 3.3291 (56.94); 3.0541 (16.00); 2.8910 (2.50); 2.7322 (1.97); 2.5254 (0.55); 2.5120 (11.03); 2.5075 (21.92); 2.5029 (28.90); 2.4983

(21.10); 2.4938 (10.12); 2.2770 (3.50); 2.2591 (4.27); 2.0961 (0.39); 2.0792 (0.72); 2.0623 (0.85); 2.0452 (0.66); 2.0279 (0.33); 0.9218 (14.86);

0.9052 (14.47); 0.8759 (0.48); −0.0002 (5.49)

›Example 341, Solvent: DMSO, Spectrometer: 399.95 MHz

10.7964 (1.97); 8.0347 (1.30); 8.0140 (1.60); 7.9532 (0.78); 7.8342 (1.32); 7.8150 (1.85); 7.7947 (1.20); 7.7226 (2.72); 7.7187 (1.40); 7.7097

(0.90); 7.7047 (3.49); 7.7010 (2.45); 7.5644 (0.52); 7.5613 (0.36); 7.5524 (0.39); 7.5460 (1.75); 7.5404 (0.59); 7.5311 (0.99); 7.5278 (1.53);

7.5244 (0.86); 7.4962 (2.57); 7.4930 (1.19); 7.4807 (1.81); 7.4770 (3.25); 7.4634 (0.56); 7.4593 (1.32); 7.4562 (0.78); 7.3568 (0.70); 7.3519

(1.12); 7.3465 (0.58); 7.3357 (4.33); 7.3312 (6.36); 7.3133 (3.71); 7.3088 (1.21); 7.2984 (0.72); 7.2939 (1.35); 7.2627 (0.47); 7.2586 (0.87);

7.2539 (1.12); 7.2487 (0.64); 7.2437 (0.69); 7.2370 (1.15); 7.2302 (0.38); 7.2245 (0.35); 7.2202 (0.50); 7.1578 (1.86); 7.1399 (1.81); 5.3691

(6.42); 3.7173 (6.49); 3.5605 (0.68); 3.3349 (84.22); 3.2182 (0.39); 3.0879 (0.37); 3.0505 (16.00); 3.0168 (0.34); 2.8902 (5.85); 2.7315 (4.65);

2.5252 (0.64); 2.5118 (13.25); 2.5074 (26.44); 2.5028 (34.90); 2.4982 (25.49); 2.4937 (12.32); 1.2348 (0.41); −0.0002 (8.23)

›Example 342, Solvent: DMSO, Spectrometer: 400.13 MHz

10.4822 (4.13); 7.8668 (0.86); 7.8466 (2.31); 7.8282 (2.23); 7.8111 (3.59); 7.7906 (1.43); 7.7318 (4.01); 7.7129 (4.58); 7.5700 (0.66); 7.5519

(2.01); 7.5335 (1.91); 7.5035 (3.37); 7.4843 (4.28); 7.4660 (1.59); 7.1433 (2.51); 7.1258 (2.41); 5.7680 (0.34); 5.3517 (8.92); 4.7808 (6.78);

4.7769 (7.14); 3.5835 (3.23); 3.3459 (39.30); 3.0750 (16.00); 2.5109 (30.31); 1.9974 (0.61); 1.2506 (1.30); 1.1818 (0.33); 0.8802 (0.47); 0.8650

(1.04); 0.8478 (0.49)

›Example 343, Solvent: DMSO, Spectrometer: 400.13 MHz

10.3290 (2.95); 7.8459 (0.69); 7.8250 (1.97); 7.8078 (2.49); 7.8025 (2.32); 7.7990 (2.59); 7.7816 (0.86); 7.7780 (0.57); 7.5391 (2.24); 7.5239

(0.69); 7.5151 (1.06); 7.5118 (1.10); 7.5063 (0.62); 7.5024 (0.90); 7.4979 (0.68); 7.3894 (0.41); 7.3699 (2.39); 7.3643 (1.61); 7.3582 (3.22);

7.3558 (3.08); 7.1130 (1.48); 7.1096 (1.50); 7.0959 (1.43); 7.0925 (1.38); 5.7689 (2.85); 5.3584 (0.35); 5.3325 (6.35); 4.1952 (2.12); 4.1785

(4.56); 4.1618 (2.09); 3.3706 (1.83); 3.3438 (51.96); 3.3167 (1.57); 3.0893 (0.64); 3.0769 (0.49); 3.0625 (16.00); 3.0354 (0.54); 2.9238 (1.38);

2.9172 (3.15); 2.9106 (1.46); 2.5792 (1.30); 2.5725 (1.38); 2.5625 (2.74); 2.5558 (2.68); 2.5456 (2.18); 2.5380 (3.34); 2.5326 (3.29); 2.5278

(3.13); 2.5187 (19.36); 2.5143 (38.86); 2.5099 (52.05); 2.5054 (37.06); 2.5010 (17.23); 2.4865 (2.10); 2.4827 (2.22); 2.3644 (0.57); 2.3383

(10.64); 2.3121 (0.49); 1.9970 (0.58)

›Example 344, Solvent: DMSO, Spectrometer: 399.95 MHz

10.7868 (2.09); 8.1713 (1.58); 8.1514 (1.87); 7.9532 (0.61); 7.9195 (1.28); 7.9001 (1.74); 7.8799 (1.20); 7.8640 (1.84); 7.8250 (0.59); 7.8210

(0.85); 7.8161 (0.47); 7.8139 (0.42); 7.8089 (0.71); 7.8046 (0.99); 7.7995 (0.54); 7.7405 (1.85); 7.7379 (2.49); 7.7340 (1.17); 7.7254 (0.73);

7.7202 (3.32); 7.7164 (2.24); 7.5674 (0.47); 7.5556 (0.34); 7.5490 (1.58); 7.5433 (0.46); 7.5342 (0.84); 7.5308 (1.39); 7.5274 (0.69); 7.5011

(2.32); 7.4977 (0.95); 7.4859 (1.53); 7.4820 (2.96); 7.4685 (0.45); 7.4644 (1.19); 7.4611 (0.64); 7.4030 (3.39); 7.3871 (1.65); 7.3683 (0.40);

7.2243 (1.73); 7.2067 (1.66); 5.4161 (6.03); 3.3297 (54.18); 3.0852 (16.00); 2.8903 (5.08); 2.7319 (3.93); 2.7309 (4.00); 2.5249 (0.63); 2.5201

(0.99); 2.5115 (11.45); 2.5070 (22.78); 2.5024 (29.99); 2.4978 (21.53); 2.4932 (10.10); 2.3876 (10.11); −0.0002 (1.26)

›Example 345, Solvent: DMSO, Spectrometer: 399.95 MHz

10.4697 (2.08); 8.1064 (1.50); 8.0868 (1.86); 7.9533 (0.64); 7.8958 (1.24); 7.8765 (1.68); 7.8563 (1.12); 7.7348 (1.87); 7.7321 (2.43); 7.7281

(1.15); 7.7195 (0.73); 7.7144 (3.31); 7.7106 (2.26); 7.5668 (0.47); 7.5549 (0.34); 7.5485 (1.59); 7.5427 (0.51); 7.5323 (2.61); 7.5310 (2.82);

7.5237 (2.16); 7.4998 (2.27); 7.4963 (0.95); 7.4846 (1.53); 7.4807 (2.93); 7.4672 (0.44); 7.4631 (1.20); 7.4598 (0.64); 7.1991 (1.65); 7.1980

(1.66); 7.1806 (1.63); 6.3325 (1.53); 6.3301 (1.53); 6.3240 (1.54); 6.3216 (1.45); 5.4021 (5.83); 3.3378 (106.36); 3.3155 (0.35); 3.0735 (16.00);

2.8911 (5.51); 2.7324 (4.38); 2.7312 (4.18); 2.5258 (0.64); 2.5210 (0.99); 2.5124 (11.87); 2.5079 (23.75); 2.5033 (31.29); 2.4986 (22.51);

2.4941 (10.49); 2.3698 (8.46); −0.0002 (3.20)

›Example 346, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5880 (2.15); 8.0620 (1.14); 8.0412 (1.37); 7.9531 (0.72); 7.8386 (1.27); 7.8192 (1.77); 7.7990 (1.15); 7.7201 (2.60); 7.7164 (1.25); 7.7075

(0.79); 7.7024 (3.39); 7.6987 (2.36); 7.5642 (0.48); 7.5522 (0.35); 7.5458 (1.63); 7.5402 (0.48); 7.5308 (0.86); 7.5276 (1.41); 7.5242 (0.72);

7.4959 (2.41); 7.4926 (1.02); 7.4804 (1.67); 7.4767 (3.09); 7.4631 (0.49); 7.4591 (1.22); 7.4559 (0.70); 7.3427 (2.55); 7.3377 (0.98); 7.3267

(1.32); 7.3214 (5.36); 7.3158 (0.80); 7.2799 (4.54); 7.2748 (1.20); 7.2635 (0.97); 7.2586 (2.31); 7.1451 (1.80); 7.1272 (1.72); 5.3493 (6.15);

3.3324 (100.44); 3.0448 (16.00); 2.9063 (1.07); 2.8903 (7.38); 2.8683 (1.61); 2.7319 (4.73); 2.7310 (4.74); 2.7178 (1.73); 2.6980 (2.37); 2.6797

(1.18); 2.6720 (0.37); 2.5251 (0.80); 2.5117 (14.73); 2.5073 (29.28); 2.5027 (38.54); 2.4981 (27.95); 2.4936 (13.25); −0.0002 (6.71)

›Example 347, Solvent: DMSO, Spectrometer: 400.13 MHz

10.6002 (3.59); 8.0852 (1.89); 8.0645 (2.24); 7.8484 (1.48); 7.8288 (2.54); 7.8089 (1.33); 7.7306 (3.99); 7.7117 (4.54); 7.5715 (0.67); 7.5536

(2.01); 7.5355 (1.89); 7.5043 (3.34); 7.4851 (4.28); 7.4668 (1.60); 7.3025 (1.13); 7.2837 (3.96); 7.2569 (6.77); 7.2397 (2.08); 7.1962 (1.30);

7.1790 (1.87); 7.1537 (2.83); 7.1350 (2.53); 5.3585 (8.79); 4.0629 (0.89); 4.0452 (2.68); 4.0274 (2.71); 4.0095 (0.92); 3.3444 (33.26); 3.0515

(16.00); 2.9208 (1.78); 2.9022 (3.80); 2.8826 (2.74); 2.7336 (2.73); 2.7137 (3.81); 2.6952 (1.83); 2.5108 (27.61); 1.9971 (10.87); 1.1994 (2.84);

1.1816 (5.58); 1.1639 (2.80)

›Example 348, Solvent: DMSO, Spectrometer: 399.95 MHz

12.1340 (1.33); 8.0098 (0.92); 7.9897 (1.70); 7.9704 (1.43); 7.8942 (1.77); 7.8742 (1.25); 7.7286 (1.89); 7.7260 (2.42); 7.7221 (1.15); 7.7133

(0.75); 7.7082 (3.32); 7.7045 (2.30); 7.5683 (0.49); 7.5562 (0.35); 7.5500 (1.57); 7.5444 (0.46); 7.5350 (0.82); 7.5316 (1.36); 7.5283 (0.67);

7.4979 (2.26); 7.4943 (0.94); 7.4824 (1.60); 7.4787 (2.99); 7.4650 (0.46); 7.4609 (1.22); 7.4578 (0.67); 7.3792 (1.59); 7.3606 (1.55); 5.4394

(5.96); 3.3379 (128.50); 3.0662 (16.00); 2.8915 (2.29); 2.7327 (1.82); 2.7315 (1.75); 2.5259 (0.67); 2.5212 (1.10); 2.5126 (13.63); 2.5081

(27.26); 2.5034 (35.89); 2.4988 (25.83); 2.4943 (12.10); −0.0002 (7.61)

›Example 349, Solvent: DMSO, Spectrometer: 399.95 MHz

10.2543 (2.68); 7.9532 (0.70); 7.8227 (0.67); 7.8017 (1.71); 7.7843 (2.07); 7.7746 (1.94); 7.7716 (2.20); 7.7538 (0.80); 7.7506 (0.60); 7.7248

(1.94); 7.7223 (2.60); 7.7185 (1.26); 7.7097 (0.79); 7.7046 (3.41); 7.7008 (2.38); 7.5633 (0.50); 7.5514 (0.38); 7.5449 (1.63); 7.5392 (0.50);

7.5300 (0.88); 7.5267 (1.42); 7.5233 (0.73); 7.4959 (2.39); 7.4925 (1.02); 7.4805 (1.63); 7.4768 (3.06); 7.4632 (0.48); 7.4591 (1.22); 7.4559

(0.69); 7.3997 (0.43); 7.3784 (0.92); 7.3728 (0.59); 7.3708 (0.47); 7.3646 (0.39); 7.3502 (11.60); 7.3482 (10.51); 7.3394 (0.61); 7.3357 (0.98);

7.3248 (0.51); 7.3145 (0.42); 7.2606 (1.89); 7.2443 (2.11); 7.1051 (1.44); 7.1020 (1.46); 7.0877 (1.40); 7.0846 (1.37); 5.3312 (6.08); 4.4282

(0.33); 4.4117 (0.75); 4.3952 (0.34); 4.2926 (1.54); 4.2759 (3.53); 4.2592 (1.60); 3.3372 (126.35); 3.0610 (16.00); 2.9947 (0.56); 2.9453 (1.49);

2.9287 (3.14); 2.9120 (1.42); 2.8908 (5.74); 2.7323 (4.49); 2.7313 (4.48); 2.5256 (0.73); 2.5208 (1.20); 2.5123 (13.89); 2.5078 (27.62); 2.5032

(36.45); 2.4986 (26.54); 2.4940 (12.71); −0.0002 (3.57)

›Example 350, Solvent: DMSO, Spectrometer: 399.95 MHz

10.1864 (3.02); 7.9534 (0.57); 7.8312 (0.56); 7.8101 (2.19); 7.7945 (4.46); 7.7756 (0.82); 7.7707 (0.43); 7.7238 (2.98); 7.7058 (3.78); 7.7021

(2.84); 7.5630 (0.54); 7.5600 (0.40); 7.5510 (0.49); 7.5446 (1.81); 7.5389 (0.75); 7.5296 (1.11); 7.5265 (1.59); 7.4962 (2.76); 7.4805 (2.13);

7.4770 (3.51); 7.4634 (0.83); 7.4593 (1.45); 7.1028 (1.50); 7.0980 (1.55); 7.0870 (1.47); 7.0822 (1.53); 5.3350 (7.21); 4.0014 (0.95); 3.9861

(1.00); 3.9749 (1.68); 3.9595 (1.75); 3.9165 (1.66); 3.8997 (1.68); 3.8900 (1.07); 3.8731 (1.01); 3.3788 (0.32); 3.3388 (105.68); 3.0660 (16.00);

2.8913 (4.01); 2.8852 (0.59); 2.7321 (3.34); 2.5122 (12.39); 2.5080 (23.10); 2.5035 (30.13); 2.4990 (23.51); 2.4948 (13.50); 1.7201 (0.47);

1.7041 (0.77); 1.6875 (0.83); 1.6713 (0.59); 1.4677 (0.46); 1.4535 (0.61); 1.4490 (0.57); 1.4345 (0.96); 1.4200 (0.66); 1.4154 (0.78); 1.4014

(0.58); 1.3968 (0.34); 1.2034 (0.60); 1.1845 (0.95); 1.1662 (0.81); 1.1507 (0.82); 1.1321 (0.54); 0.9153 (8.10); 0.9093 (2.02); 0.8987 (9.35);

0.8827 (8.44); 0.8640 (3.59); −0.0002 (2.41)

›Example 351, Solvent: CDCl3, Spectrometer: 300.16 MHz

7.9367 (2.19); 7.9094 (2.80); 7.7273 (1.51); 7.7010 (2.68); 7.6738 (3.71); 7.6503 (4.21); 7.6298 (2.91); 7.3598 (3.09); 7.2657 (3.71); 7.1381

(2.56); 7.1102 (4.82); 7.0824 (2.43); 7.0175 (2.74); 6.9931 (2.57); 5.2887 (10.20); 4.7665 (1.61); 3.1025 (16.00); 2.0103 (1.78); 1.9000 (2.89);

1.7612 (2.38); 1.7329 (2.66); 1.6600 (1.31); 1.5381 (2.17); 1.5043 (2.70); 1.4667 (2.95); 1.4382 (3.08); 1.4133 (2.78); 1.3737 (2.38); 1.3325

(1.78); 1.2914 (1.31); 1.2566 (1.36); −0.0002 (1.31)

›Example 352, Solvent: DMSO, Spectrometer: 399.95 MHz

11.1247 (2.29); 8.2819 (3.02); 8.2767 (3.08); 8.1528 (1.61); 8.1327 (1.99); 7.9901 (1.54); 7.9848 (1.44); 7.9691 (1.89); 7.9638 (1.89); 7.9541

(0.84); 7.9401 (1.33); 7.9207 (1.83); 7.9005 (1.20); 7.8033 (3.39); 7.7823 (2.78); 7.7390 (1.93); 7.7366 (2.53); 7.7327 (1.21); 7.7239 (0.72);

7.7188 (3.37); 7.7150 (2.34); 7.5684 (0.48); 7.5566 (0.34); 7.5501 (1.65); 7.5444 (0.46); 7.5352 (0.85); 7.5318 (1.41); 7.5284 (0.70); 7.5017

(2.36); 7.4982 (0.97); 7.4863 (1.56); 7.4825 (3.06); 7.4690 (0.46); 7.4649 (1.22); 7.4616 (0.66); 7.2556 (1.79); 7.2375 (1.74); 5.4211 (6.09);

3.3313 (38.37); 3.0778 (16.00); 2.8913 (6.82); 2.7325 (5.36); 2.5261 (0.44); 2.5213 (0.70); 2.5127 (8.87); 2.5082 (17.81); 2.5036 (23.56);

2.4990 (16.98); 2.4944 (8.00); −0.0002 (0.96)

›Example 353, Solvent: DMSO, Spectrometer: 400.13 MHz

9.8641 (1.93); 7.8004 (0.48); 7.7793 (1.24); 7.7622 (1.72); 7.7578 (1.49); 7.7541 (1.65); 7.7368 (0.71); 7.7321 (1.59); 7.7293 (1.89); 7.7255

(0.93); 7.7166 (0.58); 7.7115 (2.42); 7.7078 (1.70); 7.5676 (0.35); 7.5493 (1.16); 7.5436 (0.35); 7.5344 (0.63); 7.5311 (1.03); 7.5276 (0.53);

7.5004 (1.70); 7.4971 (0.75); 7.4851 (1.17); 7.4813 (2.18); 7.4678 (0.35); 7.4637 (0.87); 7.4604 (0.50); 7.0788 (0.97); 7.0752 (0.98); 7.0619

(0.92); 7.0583 (0.92); 5.3244 (4.26); 3.3896 (0.47); 3.3397 (41.48); 3.2899 (0.41); 3.0675 (11.33); 2.5304 (0.45); 2.5256 (0.75); 2.5169 (8.87);

2.5124 (18.25); 2.5079 (24.61); 2.5034 (17.32); 2.4989 (7.90); 1.7635 (0.58); 1.7461 (0.73); 1.7234 (0.82); 1.4389 (16.00); 1.3560 (0.38);

1.3488 (0.38); 1.3420 (0.50); 1.3322 (0.55); 1.3257 (0.57); 1.3174 (0.75); 1.3034 (0.99); 1.2877 (0.84); 1.2722 (0.64); 1.2522 (0.34); 0.9024

(1.88); 0.8850 (3.91); 0.8671 (1.36)

›Example 354, Solvent: DMSO, Spectrometer: 400.13 MHz

7.5870 (0.36); 7.5372 (1.48); 7.5179 (2.69); 7.4986 (1.54); 7.4596 (1.32); 7.4401 (2.73); 7.4203 (1.72); 7.2590 (2.93); 7.2373 (5.70); 7.1701

(2.39); 7.1499 (2.05); 6.6317 (2.81); 6.6140 (2.67); 6.5162 (2.85); 6.4956 (2.72); 6.3123 (0.60); 6.2567 (0.53); 5.8756 (0.50); 5.8170 (0.73);

5.7902 (0.56); 5.7836 (0.56); 5.7699 (0.56); 5.2813 (9.40); 3.8363 (16.00); 2.5626 (19.23)

›Example 355, Solvent: DMSO, Spectrometer: 400.13 MHz

10.5306 (2.21); 8.0790 (1.28); 8.0583 (1.51); 7.8391 (1.28); 7.8197 (1.77); 7.7996 (1.16); 7.5405 (2.15); 7.5254 (0.63); 7.5216 (0.55); 7.5165

(0.97); 7.5134 (0.96); 7.5083 (0.59); 7.5039 (0.86); 7.4994 (0.65); 7.3715 (2.45); 7.3666 (1.59); 7.3602 (3.09); 7.3577 (3.11); 7.1366 (1.85);

7.1189 (1.73); 5.3526 (6.21); 3.3938 (0.48); 3.3440 (44.99); 3.2942 (0.40); 3.0464 (16.00); 2.5642 (0.42); 2.5597 (0.57); 2.5552 (0.45); 2.5322

(1.20); 2.5188 (17.84); 2.5144 (36.19); 2.5099 (48.86); 2.5055 (35.26); 2.5011 (16.57); 2.4647 (0.35); 2.4602 (0.45); 2.4556 (0.35); 2.3971

(1.70); 2.3787 (3.20); 2.3601 (1.92); 2.3385 (10.36); 1.6135 (0.39); 1.5951 (1.12); 1.5767 (1.56); 1.5588 (1.08); 1.5405 (0.36); 1.3257 (0.40);

1.3094 (0.87); 1.2930 (1.76); 1.2855 (2.58); 1.2781 (2.17); 1.2682 (1.76); 1.2583 (1.31); 1.2477 (0.78); 0.8868 (2.57); 0.8697 (6.50); 0.8520

(2.62)

›Example 356, Solvent: DMSO, Spectrometer: 399.95 MHz

12.4055 (0.86); 7.9526 (0.97); 7.7416 (1.96); 7.7391 (2.66); 7.7351 (1.30); 7.7266 (0.78); 7.7214 (3.44); 7.7176 (2.41); 7.5662 (0.47); 7.5548

(0.33); 7.5478 (1.66); 7.5420 (0.49); 7.5332 (0.91); 7.5298 (1.50); 7.5263 (0.75); 7.5042 (2.51); 7.5008 (1.08); 7.4892 (1.59); 7.4851 (3.10);

7.4718 (0.48); 7.4677 (1.21); 7.4641 (0.68); 7.3329 (4.75); 7.1872 (1.01); 7.1682 (1.82); 7.1475 (1.01); 6.7907 (3.25); 6.7723 (1.16); 6.7526

(0.88); 6.7489 (0.93); 6.7314 (0.91); 6.7253 (0.75); 5.3425 (5.89); 4.8140 (7.72); 3.3331 (69.47); 3.0202 (16.00); 2.8901 (8.02); 2.7316 (6.28);

2.7308 (6.36); 2.5248 (0.60); 2.5199 (0.94); 2.5114 (12.08); 2.5069 (24.17); 2.5023 (31.84); 2.4977 (23.01); 2.4932 (10.92); 2.2687 (10.20); −0.0002

(9.31)

›Example 357, Solvent: DMSO, Spectrometer: 399.95 MHz

10.8133 (2.49); 8.1659 (1.62); 8.1458 (1.95); 8.0943 (0.48); 8.0872 (3.90); 8.0821 (1.24); 8.0702 (1.31); 8.0650 (4.12); 8.0579 (0.47); 7.9137

(1.27); 7.8944 (1.78); 7.8742 (1.19); 7.7353 (2.62); 7.7315 (1.35); 7.7228 (0.88); 7.7176 (3.44); 7.7139 (2.43); 7.5662 (0.49); 7.5631 (0.33);

7.5544 (0.38); 7.5480 (1.68); 7.5423 (0.55); 7.5330 (0.92); 7.5297 (1.49); 7.5263 (0.79); 7.4998 (2.53); 7.4963 (1.37); 7.4893 (2.12); 7.4843

(2.40); 7.4807 (3.39); 7.4706 (3.07); 7.4679 (3.14); 7.4630 (1.77); 7.4599 (0.98); 7.4543 (1.00); 7.4493 (2.50); 7.4436 (0.39); 7.2677 (0.71);

7.2650 (1.21); 7.2624 (0.74); 7.2465 (1.90); 7.2306 (0.55); 7.2280 (0.91); 7.2253 (0.59); 7.2181 (1.82); 7.2002 (1.78); 7.1452 (2.67); 7.1424

(3.27); 7.1373 (1.02); 7.1260 (1.59); 7.1234 (2.80); 7.1211 (2.39); 7.0606 (0.63); 7.0533 (4.09); 7.0482 (1.25); 7.0413 (0.43); 7.0362 (1.26);

7.0311 (3.97); 7.0240 (0.40); 5.4142 (5.96); 3.3293 (61.05); 3.1567 (0.32); 3.0799 (16.00); 3.0545 (0.34); 2.8905 (0.51); 2.7320 (0.41); 2.7309

(0.41); 2.5250 (0.84); 2.5116 (14.83); 2.5071 (29.04); 2.5025 (37.92); 2.4979 (27.39); 2.4934 (12.99); 1.3070 (0.44); 0.8796 (0.73); 0.0080

(0.38); −0.0002 (9.88)

›Example 358, Solvent: DMSO, Spectrometer: 400.13 MHz

10.5367 (2.33); 8.0813 (1.35); 8.0606 (1.61); 7.8411 (1.25); 7.8216 (1.86); 7.8016 (1.16); 7.4233 (1.04); 7.4034 (2.27); 7.3833 (1.63); 7.2856

(1.58); 7.2660 (1.27); 7.2454 (1.65); 7.2397 (2.17); 7.2356 (1.50); 7.1459 (3.06); 7.1398 (1.36); 7.1265 (2.45); 7.1191 (1.10); 5.3603 (6.33);

3.7888 (16.00); 3.7596 (0.70); 3.3985 (0.35); 3.3486 (43.41); 3.2984 (0.45); 3.0441 (14.87); 2.5600 (0.36); 2.5319 (0.79); 2.5141 (28.51);

2.5097 (38.02); 2.5054 (27.97); 2.4638 (0.48); 2.4596 (0.54); 2.4055 (1.86); 2.3872 (3.47); 2.3686 (2.04); 1.5944 (0.48); 1.5762 (1.43); 1.5576

(2.01); 1.5390 (1.52); 1.5201 (0.60); 1.3663 (1.57); 1.3482 (0.34); 1.3296 (1.15); 1.3108 (1.88); 1.2920 (1.88); 1.2738 (1.12); 1.2556 (0.37);

0.9049 (4.05); 0.8867 (8.05); 0.8682 (3.41)

›Example 359, Solvent: DMSO, Spectrometer: 399.95 MHz

10.2837 (2.70); 7.9529 (0.61); 7.8240 (0.70); 7.8030 (1.72); 7.7855 (2.06); 7.7745 (1.96); 7.7717 (2.20); 7.7537 (0.82); 7.7508 (0.65); 7.7206

(2.64); 7.7168 (1.31); 7.7080 (0.83); 7.7029 (3.46); 7.6991 (2.45); 7.5630 (0.50); 7.5598 (0.32); 7.5511 (0.38); 7.5447 (1.65); 7.5390 (0.52);

7.5298 (0.90); 7.5265 (1.45); 7.5231 (0.76); 7.4955 (2.45); 7.4921 (1.09); 7.4800 (1.70); 7.4763 (3.15); 7.4627 (0.51); 7.4586 (1.25); 7.4555

(0.73); 7.4144 (1.30); 7.4101 (2.22); 7.4064 (1.41); 7.3538 (0.61); 7.3448 (0.32); 7.3383 (0.78); 7.3309 (1.48); 7.3162 (2.37); 7.2947 (2.87);

7.2931 (2.90); 7.2901 (3.18); 7.2784 (1.27); 7.2731 (1.52); 7.2677 (0.91); 7.2600 (1.27); 7.2437 (1.56); 7.1062 (1.48); 7.1034 (1.52); 7.0889

(1.49); 7.0859 (1.43); 5.3320 (6.22); 4.4341 (0.54); 4.3114 (1.59); 4.2948 (3.64); 4.2783 (1.67); 3.3484 (195.53); 3.0598 (16.00); 3.0114 (0.40);

2.9615 (1.41); 2.9449 (2.93); 2.9285 (1.37); 2.8911 (4.89); 2.7326 (3.85); 2.7316 (3.88); 2.5263 (0.82); 2.5129 (15.31); 2.5085 (30.23); 2.5039

(39.71); 2.4993 (28.97); 2.4947 (13.99); 1.2345 (0.38); −0.0002 (1.72)

›Example 360, Solvent: DMSO, Spectrometer: 499.93 MHz

8.6977 (5.13); 7.6370 (4.31); 7.6207 (4.47); 7.4018 (4.84); 7.3731 (0.38); 7.3568 (0.34); 7.3117 (4.27); 7.2955 (3.73); 7.0151 (0.49); 6.6708

(0.35); 5.3552 (8.40); 5.3273 (0.42); 5.1904 (0.78); 3.8201 (0.43); 3.5097 (15.51); 3.3228 (20.07); 3.2996 (0.64); 3.2803 (0.69); 3.0748 (16.00);

3.0403 (0.51); 2.5163 (2.66); 2.5132 (3.23); 2.3805 (1.26); 2.3747 (1.77); 2.3602 (13.33); 1.9994 (0.39); 1.2548 (0.41); 0.8685 (0.45)

›Example 361, Solvent: DMSO, Spectrometer: 400.13 MHz

7.8582 (0.57); 5.3915 (0.63); 4.1510 (0.45); 3.8436 (1.74); 3.4133 (16.00); 3.1114 (1.61); 2.9519 (0.35); 2.5740 (0.97); 2.5696 (2.00); 2.5650

(2.71); 2.5605 (1.91); 2.5561 (0.87); 0.9860 (0.43); 0.9676 (0.88); 0.9491 (0.36)

›Example 362, Solvent: DMSO, Spectrometer: 300.16 MHz

10.5351 (2.08); 8.1083 (1.37); 8.0811 (1.69); 7.8613 (1.22); 7.8356 (1.74); 7.8086 (1.11); 7.4422 (0.88); 7.4159 (2.15); 7.3892 (1.62); 7.3001

(1.49); 7.2728 (1.17); 7.2575 (1.54); 7.2497 (1.95); 7.2442 (1.31); 7.1632 (2.71); 7.1541 (1.14); 7.1403 (1.87); 7.1269 (0.92); 5.7807 (0.43);

5.3737 (5.71); 3.8222 (0.34); 3.8008 (16.00); 3.7716 (0.49); 3.3520 (75.07); 3.0552 (14.49); 2.5332 (8.46); 2.5272 (17.99); 2.5212 (24.66);

2.5152 (17.79); 2.5093 (8.39); 2.2963 (3.23); 2.2725 (4.11); 2.1237 (0.35); 2.1014 (0.69); 2.0787 (0.80); 2.0562 (0.59); 1.3779 (0.98); 0.9412

(14.50); 0.9191 (14.05)

›Example 363, Solvent: DMSO, Spectrometer: 399.95 MHz

10.2058 (2.43); 7.8309 (0.51); 7.8099 (2.06); 7.7968 (2.75); 7.7941 (3.85); 7.7762 (0.59); 7.7248 (2.08); 7.7224 (2.63); 7.7185 (1.25); 7.7097

(0.84); 7.7046 (3.45); 7.7009 (2.35); 7.5621 (0.50); 7.5502 (0.39); 7.5438 (1.68); 7.5381 (0.49); 7.5289 (0.92); 7.5256 (1.45); 7.5221 (0.73);

7.4951 (2.45); 7.4917 (1.04); 7.4797 (1.71); 7.4760 (3.13); 7.4624 (0.50); 7.4583 (1.23); 7.4551 (0.68); 7.1052 (1.36); 7.1002 (1.37); 7.0896

(1.21); 7.0845 (1.27); 5.8636 (0.62); 5.8548 (0.33); 5.8378 (0.95); 5.8207 (0.99); 5.8117 (0.36); 5.8038 (0.36); 5.7949 (0.75); 5.7781 (0.35);

5.3311 (6.55); 5.1709 (0.49); 5.1670 (1.16); 5.1623 (1.23); 5.1584 (0.51); 5.1278 (0.45); 5.1239 (1.03); 5.1191 (1.09); 5.1153 (0.45); 5.0897

(0.60); 5.0870 (1.17); 5.0845 (0.98); 5.0821 (1.01); 5.0792 (0.49); 5.0641 (0.55); 5.0614 (1.08); 5.0589 (0.90); 5.0565 (0.94); 5.0536 (0.44);

4.1605 (2.18); 4.1436 (4.67); 4.1267 (2.22); 3.3294 (51.59); 3.0657 (16.00); 2.8907 (1.00); 2.7320 (0.79); 2.7311 (0.79); 2.5251 (0.60); 2.5118

(10.47); 2.5073 (20.50); 2.5027 (26.80); 2.4981 (19.33); 2.4936 (9.13); 2.4081 (0.71); 2.4050 (0.48); 2.3945 (1.33); 2.3913 (2.11); 2.3881 (1.33);

2.3777 (1.36); 2.3745 (2.08); 2.3712 (1.27); 2.3608 (0.50); 2.3576 (0.69); 0.9336 (0.63); −0.0002 (8.80)

›Example 364, Solvent: DMSO, Spectrometer: 399.95 MHz

10.9348 (2.13); 8.1578 (1.55); 8.1380 (1.90); 8.1219 (1.89); 8.1165 (0.74); 8.1082 (2.06); 8.0996 (2.10); 8.0914 (0.76); 8.0859 (1.94); 7.9532

(0.70); 7.9258 (1.27); 7.9065 (1.73); 7.8863 (1.16); 7.7387 (1.86); 7.7360 (2.47); 7.7321 (1.19); 7.7234 (0.75); 7.7183 (3.30); 7.7145 (2.28);

7.5684 (0.47); 7.5566 (0.33); 7.5501 (1.60); 7.5444 (0.48); 7.5352 (0.87); 7.5319 (1.43); 7.5284 (0.73); 7.5021 (2.30); 7.4986 (1.02); 7.4868

(1.54); 7.4829 (3.00); 7.4694 (0.47); 7.4653 (1.23); 7.4620 (0.70); 7.3623 (2.08); 7.3570 (0.63); 7.3452 (0.74); 7.3401 (3.94); 7.3349 (0.72);

7.3232 (0.64); 7.3179 (1.93); 7.2351 (1.69); 7.2167 (1.66); 5.4185 (5.92); 3.3521 (65.03); 3.3478 (91.92); 3.0808 (16.00); 2.8914 (5.86); 2.7327

(4.71); 2.7318 (4.45); 2.5266 (0.55); 2.5219 (0.86); 2.5133 (11.02); 2.5088 (22.14); 2.5041 (29.22); 2.4995 (21.11); 2.4950 (9.92); −0.0002 (0.99)

›Example 365, Solvent: DMSO, Spectrometer: 399.95 MHz

10.4916 (1.94); 8.0771 (1.31); 8.0565 (1.55); 7.9535 (0.37); 7.8305 (1.26); 7.8112 (1.74); 7.7909 (1.19); 7.7260 (1.96); 7.7235 (2.58); 7.7196

(1.29); 7.7109 (0.81); 7.7057 (3.49); 7.7020 (2.37); 7.5641 (0.49); 7.5522 (0.37); 7.5458 (1.63); 7.5401 (0.49); 7.5309 (0.87); 7.5275 (1.43);

7.5241 (0.72); 7.4964 (2.42); 7.4929 (1.04); 7.4810 (1.65); 7.4772 (3.08); 7.4637 (0.48); 7.4596 (1.24); 7.4564 (0.69); 7.1404 (1.74); 7.1230

(1.68); 5.3549 (6.16); 3.3289 (49.21); 3.0551 (16.00); 2.8908 (3.03); 2.7323 (2.37); 2.7312 (2.39); 2.5254 (0.56); 2.5205 (0.88); 2.5120 (10.34);

2.5075 (20.59); 2.5029 (27.23); 2.4983 (19.80); 2.4937 (9.46); 2.3940 (3.07); 2.3755 (3.88); 2.2278 (0.67); 2.2090 (0.83); 2.1898 (0.63); 1.7463

(0.62); 1.7344 (0.86); 1.7166 (0.92); 1.7061 (0.68); 1.7036 (0.69); 1.6962 (0.37); 1.6881 (0.42); 1.6193 (0.36); 1.6130 (0.56); 1.6045 (0.82);

1.5924 (1.07); 1.5852 (0.66); 1.5811 (0.68); 1.5752 (0.82); 1.5689 (0.49); 1.5648 (0.42); 1.5597 (0.38); 1.5521 (0.38); 1.5359 (0.40); 1.5197

(0.49); 1.5173 (0.50); 1.5104 (0.79); 1.5011 (0.83); 1.4927 (0.96); 1.4806 (0.80); 1.4739 (0.54); 1.2029 (0.32); 1.1844 (0.80); 1.1707 (0.73);

1.1652 (0.88); 1.1538 (0.81); 1.1456 (0.59); 1.1350 (0.66); 0.8757 (0.47); −0.0002 (9.08)

›Example 366, Solvent: DMSO, Spectrometer: 399.95 MHz

12.5689 (0.71); 7.9536 (0.80); 7.7420 (1.98); 7.7394 (2.76); 7.7355 (1.39); 7.7269 (0.78); 7.7218 (3.54); 7.7180 (2.54); 7.5676 (0.49); 7.5561

(0.35); 7.5492 (1.73); 7.5434 (0.51); 7.5345 (0.95); 7.5311 (1.58); 7.5276 (0.79); 7.5052 (2.60); 7.5019 (1.14); 7.4901 (1.63); 7.4862 (3.19);

7.4728 (0.53); 7.4686 (1.41); 7.4641 (1.72); 7.4599 (1.63); 7.4443 (1.37); 7.4403 (1.71); 7.3470 (4.63); 7.2809 (0.73); 7.2769 (0.72); 7.2619

(1.14); 7.2605 (1.14); 7.2572 (1.38); 7.2416 (0.98); 7.2375 (0.92); 6.9949 (0.82); 6.9916 (1.12); 6.9760 (1.25); 6.9723 (3.41); 6.9565 (0.65);

6.9530 (1.52); 6.9507 (1.71); 5.3432 (5.84); 5.1284 (0.38); 5.1120 (1.40); 5.0953 (1.41); 5.0788 (0.38); 3.3436 (52.87); 3.0291 (16.00); 3.0209

(0.61); 3.0145 (0.82); 2.8910 (6.58); 2.7328 (5.23); 2.7318 (5.12); 2.5267 (0.40); 2.5218 (0.61); 2.5133 (7.53); 2.5088 (15.09); 2.5042 (19.94);

2.4996 (14.42); 2.4950 (6.79); 1.5950 (5.61); 1.5785 (5.57); 1.5502 (0.34); −0.0002 (2.09)

›Example 367, Solvent: DMSO, Spectrometer: 399.95 MHz

10.1886 (1.49); 7.9742 (1.03); 7.9533 (1.86); 7.8599 (0.98); 7.8409 (1.25); 7.8204 (0.78); 7.7249 (1.38); 7.7222 (1.84); 7.7184 (0.88); 7.7096

(0.56); 7.7045 (2.43); 7.7008 (1.68); 7.5637 (0.35); 7.5454 (1.15); 7.5397 (0.34); 7.5304 (0.61); 7.5271 (1.00); 7.5237 (0.51); 7.4954 (1.70);

7.4919 (0.73); 7.4799 (1.18); 7.4762 (2.17); 7.4626 (0.35); 7.4585 (0.88); 7.4554 (0.49); 7.1829 (1.23); 7.1657 (1.17); 5.3786 (4.29); 3.3399

(87.21); 3.0540 (11.56); 2.8907 (3.99); 2.7321 (3.20); 2.7308 (3.19); 2.5254 (0.51); 2.5205 (0.82); 2.5120 (9.20); 2.5075 (18.19); 2.5029 (23.84);

2.4983 (17.24); 2.4937 (8.10); 2.0474 (11.49); 1.5590 (16.00); −0.0002 (1.91)

›Example 368, Solvent: DMSO, Spectrometer: 399.95 MHz

12.4336 (0.66); 7.9525 (1.16); 7.7388 (2.80); 7.7349 (1.38); 7.7263 (0.82); 7.7211 (3.54); 7.7173 (2.48); 7.5670 (0.48); 7.5638 (0.32); 7.5557

(0.35); 7.5487 (1.73); 7.5428 (0.53); 7.5340 (0.95); 7.5306 (1.56); 7.5272 (0.81); 7.5051 (2.64); 7.5019 (1.16); 7.4901 (1.67); 7.4861 (3.22);

7.4727 (0.50); 7.4686 (1.25); 7.4651 (0.71); 7.3431 (5.06); 7.3246 (2.70); 7.3042 (1.76); 7.0929 (1.38); 7.0875 (2.46); 7.0820 (1.79); 7.0472

(1.17); 7.0455 (1.36); 7.0425 (1.07); 7.0407 (1.04); 7.0274 (1.05); 7.0256 (1.13); 7.0226 (1.00); 7.0208 (0.90); 6.9708 (1.10); 6.9692 (1.16);

6.9647 (1.05); 6.9631 (1.01); 6.9499 (1.01); 6.9483 (1.01); 6.9437 (0.97); 6.9421 (0.90); 5.3456 (5.96); 4.8919 (7.46); 3.3483 (158.79); 3.0350

(0.40); 3.0221 (16.00); 2.8908 (9.32); 2.7319 (7.35); 2.7314 (7.37); 2.5259 (0.72); 2.5126 (14.07); 2.5081 (27.94); 2.5035 (36.92); 2.4989

(26.94); 2.4945 (12.93); 2.2231 (0.42); −0.0002 (0.60)

›Example 369, Solvent: DMSO, Spectrometer: 399.95 MHz

10.2328 (2.72); 7.9531 (0.61); 7.8207 (0.61); 7.7997 (1.83); 7.7827 (3.03); 7.7763 (2.46); 7.7591 (0.69); 7.7554 (0.41); 7.7231 (2.73); 7.7053

(3.53); 7.7016 (2.50); 7.5627 (0.50); 7.5595 (0.32); 7.5507 (0.38); 7.5444 (1.68); 7.5387 (0.52); 7.5293 (0.97); 7.5261 (1.48); 7.5228 (0.77);

7.4954 (2.50); 7.4798 (1.84); 7.4763 (3.22); 7.4625 (0.55); 7.4586 (1.28); 7.4555 (0.75); 7.2587 (1.38); 7.2423 (1.85); 7.1920 (2.44); 7.1721

(4.14); 7.1597 (0.80); 7.1392 (0.66); 7.1156 (3.70); 7.1024 (2.04); 7.0986 (2.85); 7.0861 (1.52); 7.0823 (1.42); 5.3304 (6.54); 4.3815 (0.70);

4.3646 (0.32); 4.2681 (1.69); 4.2507 (3.80); 4.2334 (1.75); 3.3295 (63.37); 3.0624 (16.00); 2.9435 (0.52); 2.8990 (1.52); 2.8903 (5.03); 2.8817

(3.06); 2.8646 (1.38); 2.7319 (3.79); 2.7310 (3.61); 2.5247 (0.75); 2.5113 (14.79); 2.5069 (28.69); 2.5023 (37.13); 2.4978 (27.13); 2.4933

(13.12); 2.2794 (1.68); 2.2636 (10.00); 1.2348 (0.33); 0.0079 (0.33); −0.0002 (9.04)

›Example 370, Solvent: DMSO, Spectrometer: 400.13 MHz

12.1253 (2.00); 7.6237 (1.13); 7.6171 (1.49); 7.6135 (1.37); 7.6026 (0.98); 7.5961 (2.56); 7.5930 (3.18); 7.5691 (0.79); 7.5550 (0.89); 7.5489

(1.24); 7.5346 (1.15); 7.5300 (0.75); 7.5137 (0.48); 7.4304 (0.58); 7.4277 (0.63); 7.4242 (0.58); 7.4214 (0.54); 7.4069 (1.04); 7.4025 (0.92);

7.3882 (0.48); 7.3845 (0.49); 7.3793 (0.37); 7.2839 (4.74); 5.7615 (0.39); 5.3434 (6.68); 3.4016 (3.20); 3.3516 (203.75); 3.3016 (2.30); 3.0126

(16.00); 2.5620 (0.58); 2.5577 (0.74); 2.5532 (0.65); 2.5163 (15.04); 2.5122 (28.70); 2.5078 (37.42); 2.5034 (26.78); 2.4624 (0.40); 2.4577

(0.45); 2.4532 (0.37); 2.4321 (2.08); 2.4137 (3.72); 2.3950 (2.20); 1.6063 (0.54); 1.5880 (1.54); 1.5694 (2.11); 1.5508 (1.58); 1.5318 (0.61);

1.3402 (0.36); 1.3216 (1.22); 1.3028 (1.98); 1.2841 (1.97); 1.2658 (1.18); 1.2477 (0.39); 0.8961 (4.28); 0.8778 (8.45); 0.8593 (3.56)

›Example 371, Solvent: DMSO, Spectrometer: 399.95 MHz

10.6146 (2.17); 8.0199 (1.49); 8.0000 (1.97); 7.9530 (1.33); 7.8761 (1.36); 7.8569 (1.80); 7.8366 (1.14); 7.7192 (2.63); 7.7155 (1.24); 7.7064

(0.87); 7.7015 (3.46); 7.6978 (2.36); 7.5628 (0.51); 7.5596 (0.33); 7.5507 (0.40); 7.5445 (1.65); 7.5389 (0.49); 7.5295 (0.89); 7.5262 (1.41);

7.5228 (0.70); 7.4927 (2.39); 7.4893 (1.01); 7.4771 (1.74); 7.4735 (3.10); 7.4598 (0.51); 7.4558 (1.24); 7.4527 (0.68); 7.2076 (1.78); 7.1900

(1.69); 5.3794 (6.02); 3.3328 (126.76); 3.0495 (16.00); 2.8911 (10.81); 2.7323 (8.42); 2.7313 (8.66); 2.5253 (0.91); 2.5120 (16.93); 2.5075

(32.95); 2.5029 (42.83); 2.4983 (30.77); 2.4937 (14.35); 2.1610 (1.78); 2.1401 (1.87); 1.7355 (0.68); 1.7206 (2.55); 1.7002 (2.42); 1.2522 (5.41);

1.2352 (5.18); 1.0915 (4.77); 1.0742 (4.48); 0.0080 (0.45); −0.0002 (12.06); −0.0085 (0.35)

›Example 372, Solvent: DMSO, Spectrometer: 399.95 MHz

10.2150 (1.04); 7.8145 (0.82); 7.7973 (1.51); 7.7918 (1.11); 7.7284 (0.90); 7.7257 (1.13); 7.7219 (0.55); 7.7131 (0.36); 7.7080 (1.50); 7.7043

(1.05); 7.5454 (0.73); 7.5304 (0.40); 7.5270 (0.64); 7.4967 (1.06); 7.4932 (0.45); 7.4813 (0.74); 7.4776 (1.36); 7.4599 (0.55); 7.1047 (0.61);

7.1007 (0.62); 7.0881 (0.59); 7.0841 (0.57); 5.3430 (2.80); 3.7969 (4.10); 3.3291 (22.59); 3.0627 (7.19); 2.8911 (1.94); 2.7323 (1.60); 2.7311

(1.49); 2.5204 (0.44); 2.5119 (4.93); 2.5074 (9.74); 2.5028 (12.79); 2.4982 (9.24); 2.4937 (4.38); 0.9337 (16.00); 0.9052 (0.49); −0.0002 (4.50)

›Example 373, Solvent: DMSO, Spectrometer: 399.95 MHz

12.8166 (1.73); 8.0306 (0.53); 8.0246 (3.75); 8.0201 (1.32); 8.0077 (1.43); 8.0031 (4.57); 7.9973 (0.64); 7.9532 (1.72); 7.7729 (4.38); 7.7684

(1.48); 7.7513 (4.17); 7.7453 (3.35); 7.7325 (0.91); 7.7275 (3.54); 7.7237 (2.55); 7.5677 (0.47); 7.5646 (0.34); 7.5564 (0.36); 7.5492 (1.74);

7.5435 (0.55); 7.5346 (0.97); 7.5313 (1.57); 7.5279 (0.85); 7.5067 (2.68); 7.4914 (1.72); 7.4875 (3.28); 7.4741 (0.52); 7.4700 (1.24); 7.4665

(0.78); 7.3919 (3.72); 5.3835 (6.09); 3.3302 (82.54); 3.0168 (16.00); 2.8909 (13.13); 2.7316 (10.91); 2.5252 (0.87); 2.5118 (16.23); 2.5074

(31.73); 2.5029 (41.54); 2.4984 (30.46); 2.4939 (14.82); 0.0078 (0.53); −0.0002 (13.09); −0.0085 (0.43)

›Example 374, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5338 (2.12); 8.0745 (1.30); 8.0537 (1.55); 7.8361 (1.30); 7.8168 (1.83); 7.7966 (1.19); 7.7234 (2.66); 7.7105 (0.83); 7.7055 (3.46); 7.7017

(2.39); 7.5648 (0.48); 7.5528 (0.38); 7.5464 (1.69); 7.5408 (0.47); 7.5315 (0.91); 7.5282 (1.41); 7.5249 (0.71); 7.4974 (2.46); 7.4818 (1.72);

7.4781 (3.15); 7.4645 (0.49); 7.4605 (1.23); 7.4572 (0.69); 7.1438 (1.86); 7.1256 (1.78); 5.3553 (6.54); 3.5493 (2.35); 3.5325 (5.06); 3.5157

(2.42); 3.3346 (104.02); 3.0721 (0.33); 3.0543 (16.00); 2.8910 (2.52); 2.7319 (2.05); 2.5253 (0.71); 2.5204 (1.10); 2.5119 (14.07); 2.5074

(27.95); 2.5029 (36.72); 2.4983 (26.58); 2.4938 (12.60); 2.4108 (1.52); 2.3926 (3.02); 2.3741 (1.66); 1.8517 (0.47); 1.8347 (1.35); 1.8168 (1.56);

1.7975 (1.43); 1.7806 (0.54); 1.6361 (0.36); 1.6177 (1.09); 1.5990 (1.53); 1.5801 (1.22); 1.5613 (0.48); 1.4378 (0.49); 1.4239 (0.68); 1.4180

(1.11); 1.4079 (0.65); 1.4001 (1.50); 1.3863 (0.57); 1.3797 (0.77); −0.0002 (4.11)

›Example 375, Solvent: DMSO, Spectrometer: 399.95 MHz

10.7390 (1.95); 8.0257 (1.22); 8.0050 (1.51); 7.9529 (0.71); 7.8287 (1.27); 7.8095 (1.74); 7.7891 (1.15); 7.7214 (2.53); 7.7176 (1.21); 7.7088

(0.75); 7.7037 (3.38); 7.6999 (2.36); 7.5638 (0.47); 7.5519 (0.34); 7.5455 (1.60); 7.5399 (0.46); 7.5305 (0.84); 7.5272 (1.38); 7.5238 (0.69);

7.4953 (2.34); 7.4918 (0.98); 7.4798 (1.61); 7.4761 (3.06); 7.4625 (0.48); 7.4584 (1.23); 7.4552 (0.68); 7.2292 (2.44); 7.2092 (3.60); 7.1518

(1.74); 7.1328 (1.91); 7.1252 (3.15); 7.1056 (2.16); 5.3645 (6.09); 3.6570 (5.26); 3.3287 (60.75); 3.0473 (16.00); 2.8901 (5.80); 2.7316 (4.56);

2.7307 (4.56); 2.5247 (0.55); 2.5199 (0.94); 2.5114 (13.05); 2.5069 (26.19); 2.5023 (34.53); 2.4976 (24.97); 2.4931 (11.82); 2.2637 (9.60);

0.0080 (0.53); −0.0002 (15.92); −0.0086 (0.47)

›Example 376, Solvent: DMSO, Spectrometer: 400.13 MHz

10.5833 (2.13); 8.1412 (1.25); 8.1205 (1.46); 7.8987 (1.25); 7.8794 (1.75); 7.8591 (1.15); 7.6809 (0.63); 7.6768 (0.94); 7.6712 (0.89); 7.6656

(0.68); 7.6624 (1.10); 7.6588 (0.88); 7.6560 (0.93); 7.6516 (1.17); 7.6454 (2.31); 7.6427 (2.11); 7.6216 (0.72); 7.6074 (0.82); 7.6015 (1.08);

7.5870 (1.18); 7.5819 (0.55); 7.5664 (0.51); 7.4921 (0.50); 7.4892 (0.56); 7.4857 (0.49); 7.4828 (0.46); 7.4679 (0.86); 7.4642 (0.75); 7.4498

(0.40); 7.4469 (0.41); 7.4438 (0.38); 7.2126 (1.79); 7.1949 (1.71); 5.8243 (2.54); 5.4358 (6.17); 3.4481 (0.51); 3.3982 (42.17); 3.3482 (0.41);

3.1093 (16.00); 2.6199 (0.41); 2.6154 (0.58); 2.6109 (0.43); 2.5880 (0.82); 2.5833 (1.32); 2.5744 (16.94); 2.5700 (35.55); 2.5655 (48.62);

2.5610 (34.80); 2.5567 (16.18); 2.5201 (0.38); 2.5155 (0.49); 2.5110 (0.36); 2.4528 (1.65); 2.4344 (3.10); 2.4158 (1.79); 1.6686 (0.36); 1.6502

(1.06); 1.6318 (1.48); 1.6139 (1.03); 1.5956 (0.34); 1.3808 (0.37); 1.3648 (0.79); 1.3481 (1.60); 1.3406 (2.40); 1.3333 (2.01); 1.3233 (1.64);

1.3135 (1.18); 1.3028 (0.62); 1.2954 (0.48); 0.9418 (2.45); 0.9247 (6.33); 0.9069 (2.54)

›Example 377, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5486 (2.09); 8.0769 (1.15); 8.0562 (1.36); 7.9534 (0.40); 7.8355 (1.28); 7.8162 (1.74); 7.7960 (1.17); 7.7238 (2.56); 7.7199 (1.23); 7.7111

(0.75); 7.7060 (3.41); 7.7022 (2.36); 7.5630 (0.48); 7.5511 (0.34); 7.5447 (1.65); 7.5390 (0.47); 7.5298 (0.85); 7.5264 (1.40); 7.5230 (0.71);

7.4954 (2.37); 7.4919 (1.01); 7.4799 (1.61); 7.4762 (3.08); 7.4626 (0.46); 7.4585 (1.21); 7.4553 (0.68); 7.2984 (1.10); 7.2945 (0.45); 7.2799

(2.65); 7.2661 (0.85); 7.2616 (2.54); 7.2105 (3.24); 7.1929 (2.59); 7.1743 (1.40); 7.1691 (0.35); 7.1597 (0.35); 7.1563 (0.55); 7.1434 (1.77);

7.1255 (1.71); 5.3532 (6.15); 3.3283 (54.14); 3.0539 (16.00); 2.8904 (3.35); 2.7316 (2.62); 2.6157 (1.44); 2.5970 (1.93); 2.5770 (1.62); 2.5249

(0.68); 2.5202 (1.04); 2.5116 (12.85); 2.5071 (25.62); 2.5025 (33.69); 2.4979 (24.30); 2.4933 (11.46); 2.4397 (1.45); 2.4214 (2.77); 2.4029

(1.64); 1.9101 (0.44); 1.8910 (1.21); 1.8719 (1.51); 1.8530 (1.12); 1.8344 (0.35); 0.0080 (0.35); −0.0002 (10.62)

›Example 378, Solvent: DMSO, Spectrometer: 399.95 MHz

12.4210 (2.01); 7.9530 (1.04); 7.7377 (1.93); 7.7351 (2.62); 7.7311 (1.25); 7.7227 (0.78); 7.7175 (3.41); 7.7136 (2.33); 7.5639 (0.46); 7.5525

(0.33); 7.5456 (1.65); 7.5397 (0.48); 7.5309 (0.91); 7.5275 (1.49); 7.5240 (0.74); 7.5017 (2.48); 7.4983 (1.05); 7.4867 (1.59); 7.4826 (3.05);

7.4693 (0.48); 7.4651 (1.20); 7.4616 (0.66); 7.3453 (0.34); 7.3315 (0.52); 7.3262 (3.12); 7.3209 (3.45); 7.3124 (12.83); 7.3042 (0.57); 7.2996

(0.69); 7.2771 (4.45); 7.2657 (0.78); 7.2633 (0.69); 7.2597 (0.55); 7.2542 (0.62); 7.2508 (0.78); 7.2458 (0.53); 7.2405 (0.34); 7.2370 (0.39);

5.3279 (5.95); 3.7498 (7.45); 3.3295 (25.43); 3.3275 (36.79); 3.0163 (16.00); 2.8900 (8.57); 2.7315 (6.74); 2.5246 (0.63); 2.5198 (0.98); 2.5114

(11.58); 2.5068 (22.97); 2.5022 (30.18); 2.4976 (21.76); 2.4931 (10.27); 0.0080 (0.42); −0.0002 (11.84); −0.0085 (0.35)

›Example 379, Solvent: DMSO, Spectrometer: 399.95 MHz

10.0901 (1.67); 8.0496 (1.08); 8.0289 (1.34); 7.8809 (1.28); 7.8615 (1.78); 7.8414 (1.10); 7.7331 (0.32); 7.7276 (1.93); 7.7249 (2.49); 7.7211

(1.26); 7.7124 (0.82); 7.7072 (3.43); 7.7035 (2.32); 7.5652 (0.48); 7.5533 (0.36); 7.5469 (1.58); 7.5412 (0.48); 7.5320 (0.86); 7.5286 (1.39);

7.5252 (0.71); 7.4976 (2.35); 7.4941 (1.03); 7.4822 (1.61); 7.4785 (2.99); 7.4649 (0.47); 7.4608 (1.20); 7.4576 (0.66); 7.1874 (1.70); 7.1700

(1.64); 5.3671 (6.32); 4.0642 (8.62); 3.3601 (19.81); 3.3284 (43.74); 3.0675 (16.00); 2.5251 (0.60); 2.5202 (0.98); 2.5117 (10.28); 2.5072

(20.13); 2.5026 (26.35); 2.4980 (19.02); 2.4935 (8.98); 0.8758 (0.53); 0.0080 (0.32); −0.0002 (8.55)

›Example 380, Solvent: DMSO, Spectrometer: 399.95 MHz

11.0468 (2.33); 8.2087 (1.47); 8.2042 (2.62); 8.1998 (1.55); 8.1544 (1.61); 8.1345 (1.97); 8.0191 (0.91); 8.0166 (1.21); 8.0128 (0.93); 7.9996

(1.03); 7.9969 (1.25); 7.9958 (1.26); 7.9932 (0.98); 7.9531 (0.92); 7.9344 (1.31); 7.9151 (1.83); 7.8949 (1.17); 7.8119 (0.91); 7.8095 (1.05);

7.8070 (0.99); 7.8046 (0.90); 7.7919 (1.07); 7.7895 (1.12); 7.7870 (1.15); 7.7846 (0.98); 7.7390 (1.93); 7.7365 (2.57); 7.7326 (1.26); 7.7239

(0.76); 7.7187 (3.37); 7.7150 (2.37); 7.5684 (0.47); 7.5565 (0.33); 7.5500 (1.61); 7.5443 (0.48); 7.5351 (0.86); 7.5318 (1.42); 7.5284 (0.74);

7.5015 (3.00); 7.4867 (1.68); 7.4810 (4.00); 7.4694 (0.53); 7.4653 (1.29); 7.4609 (1.73); 7.2472 (1.78); 7.2293 (1.72); 5.4193 (6.15); 3.3474

(79.23); 3.3440 (115.92); 3.0810 (16.00); 2.8912 (7.35); 2.7325 (5.82); 2.7316 (5.74); 2.5262 (0.60); 2.5215 (0.91); 2.5129 (12.27); 2.5084

(24.79); 2.5038 (32.90); 2.4992 (24.02); 2.4947 (11.54); −0.0002 (7.80)

›Example 381, Solvent: DMSO, Spectrometer: 399.95 MHz

10.8881 (1.89); 8.0482 (1.10); 8.0275 (1.34); 7.9534 (1.17); 7.8927 (2.02); 7.8861 (1.51); 7.8778 (2.27); 7.8692 (2.28); 7.8581 (2.00); 7.8435

(1.97); 7.8362 (1.41); 7.8169 (1.65); 7.7965 (1.12); 7.7256 (1.87); 7.7229 (2.46); 7.7190 (1.18); 7.7103 (0.75); 7.7051 (3.35); 7.7014 (2.30);

7.5624 (0.48); 7.5504 (0.35); 7.5441 (1.59); 7.5384 (0.47); 7.5291 (0.90); 7.5257 (1.53); 7.5217 (1.95); 7.5170 (1.62); 7.5052 (1.46); 7.4996

(2.24); 7.4952 (4.17); 7.4886 (2.90); 7.4813 (1.57); 7.4780 (2.28); 7.4744 (3.58); 7.4566 (1.36); 7.4538 (0.79); 7.1606 (1.66); 7.1431 (1.61);

5.3758 (5.74); 3.9037 (4.99); 3.3314 (84.48); 3.0547 (16.00); 2.8902 (9.91); 2.7319 (7.85); 2.7308 (7.61); 2.5251 (0.76); 2.5204 (1.22); 2.5118

(14.47); 2.5073 (28.90); 2.5027 (38.06); 2.4980 (27.38); 2.4935 (12.84); −0.0002 (8.50)

›Example 382, Solvent: DMSO, Spectrometer: 399.95 MHz

10.6884 (2.06); 8.0222 (0.67); 8.0016 (0.87); 7.8850 (1.29); 7.8658 (1.69); 7.8455 (1.07); 7.7315 (1.88); 7.7287 (2.48); 7.7249 (1.18); 7.7162

(0.74); 7.7110 (3.35); 7.7073 (2.30); 7.5671 (0.48); 7.5552 (0.34); 7.5488 (1.58); 7.5431 (0.46); 7.5339 (0.84); 7.5305 (1.39); 7.5271 (0.69);

7.4993 (2.27); 7.4958 (0.95); 7.4839 (1.56); 7.4802 (2.95); 7.4666 (0.46); 7.4625 (1.21); 7.4593 (0.65); 7.2827 (1.19); 7.2625 (2.51); 7.2421

(1.92); 7.2081 (1.68); 7.1996 (1.41); 7.1945 (2.27); 7.1891 (3.17); 7.1695 (1.29); 7.1673 (1.51); 7.1652 (1.12); 7.1629 (1.00); 7.1498 (0.92);

7.1476 (0.93); 7.1453 (0.86); 7.1432 (0.68); 6.9984 (1.00); 6.9963 (1.04); 6.9922 (0.98); 6.9901 (0.93); 6.9776 (0.91); 6.9755 (0.88); 6.9713

(0.88); 6.9693 (0.78); 5.3865 (5.76); 4.8406 (5.38); 3.3339 (77.04); 3.0689 (16.00); 2.8905 (0.35); 2.5253 (0.71); 2.5205 (1.15); 2.5119 (13.10);

2.5074 (26.04); 2.5027 (34.22); 2.4981 (24.64); 2.4935 (11.54); −0.0002 (2.40)

›Example 383, Solvent: CDCl3, Spectrometer: 300.16 MHz

7.9456 (2.10); 7.9178 (2.65); 7.7269 (1.43); 7.7001 (2.53); 7.6728 (3.34); 7.6472 (3.04); 7.6295 (2.57); 7.2642 (9.28); 7.1378 (2.26); 7.1118

(4.37); 7.0844 (2.20); 7.0178 (2.62); 6.9930 (2.44); 5.2842 (9.93); 5.0332 (0.71); 5.0110 (1.22); 4.9903 (1.22); 4.9702 (0.68); 3.1054 (16.00);

1.7335 (0.39); 1.7115 (0.86); 1.6900 (1.19); 1.6663 (1.21); 1.6532 (1.29); 1.6116 (8.38); 1.5884 (1.39); 1.5662 (0.71); 1.3629 (0.77); 1.3428

(1.15); 1.3207 (1.40); 1.2955 (8.48); 1.2748 (8.38); 0.9369 (14.57); 0.9159 (13.90); −0.0002 (2.87)

›Example 384, Solvent: DMSO, Spectrometer: 400.13 MHz

10.5328 (2.13); 8.0787 (1.28); 8.0580 (1.52); 7.8384 (1.28); 7.8190 (1.79); 7.7988 (1.19); 7.5405 (2.14); 7.5253 (0.63); 7.5209 (0.53); 7.5165

(0.93); 7.5132 (0.95); 7.5079 (0.57); 7.5038 (0.87); 7.4993 (0.64); 7.3901 (0.41); 7.3711 (2.32); 7.3656 (1.55); 7.3595 (3.13); 7.3570 (3.09);

7.1364 (1.83); 7.1186 (1.74); 5.3530 (6.22); 4.0613 (0.50); 4.0435 (1.53); 4.0257 (1.55); 4.0079 (0.51); 3.3952 (0.54); 3.3452 (30.65); 3.2949

(0.53); 3.0474 (16.00); 2.5596 (0.38); 2.5320 (0.53); 2.5273 (0.87); 2.5186 (8.94); 2.5142 (18.43); 2.5097 (24.98); 2.5052 (17.82); 2.5008 (8.22);

2.4593 (0.39); 2.4548 (0.33); 2.4071 (1.81); 2.3888 (3.41); 2.3702 (1.98); 2.3381 (10.37); 1.9963 (6.81); 1.5958 (0.46); 1.5776 (1.34); 1.5589

(1.85); 1.5405 (1.38); 1.5215 (0.57); 1.3308 (1.10); 1.3119 (1.73); 1.2931 (1.73); 1.2750 (1.05); 1.2569 (0.32); 1.1984 (1.83); 1.1806 (3.67);

1.1628 (1.79); 0.9054 (4.10); 0.8871 (8.36); 0.8768 (0.37); 0.8686 (3.44)

›Example 385, Solvent: CDCl3, Spectrometer: 300.16 MHz

9.2433 (0.89); 8.5283 (0.54); 8.5013 (0.59); 7.7846 (1.15); 7.7590 (1.66); 7.7317 (1.19); 7.6522 (1.59); 7.6480 (2.15); 7.6425 (1.14); 7.6325

(0.78); 7.6254 (2.72); 7.6199 (2.23); 7.5104 (0.33); 7.4857 (1.22); 7.4771 (0.46); 7.4676 (0.95); 7.4626 (1.50); 7.4572 (0.85); 7.4521 (0.64);

7.4443 (2.50); 7.4397 (1.17); 7.4262 (1.22); 7.4244 (1.23); 7.4197 (2.46); 7.4025 (0.49); 7.3968 (0.87); 7.3907 (0.58); 7.2636 (2.74); 7.1610

(1.64); 7.1363 (1.53); 5.3624 (6.90); 3.3141 (2.09); 3.2896 (2.97); 3.2648 (2.24); 3.1101 (16.00); 1.7511 (0.39); 1.7274 (1.01); 1.7022 (1.79);

1.6935 (0.93); 1.6770 (2.45); 1.6520 (0.70); 1.4949 (0.98); 1.4698 (1.45); 1.4442 (1.46); 1.4203 (0.90); 0.9759 (3.50); 0.9516 (7.07); 0.9272

(2.94); −0.0002 (1.15)

›Example 386, Solvent: DMSO, Spectrometer: 399.95 MHz

10.7418 (1.97); 8.0578 (1.25); 8.0371 (1.50); 7.9533 (0.93); 7.8227 (1.27); 7.8033 (1.72); 7.7831 (1.15); 7.7071 (2.56); 7.7033 (1.22); 7.6943

(0.75); 7.6893 (3.36); 7.6856 (2.33); 7.5568 (0.49); 7.5446 (0.37); 7.5385 (1.60); 7.5329 (0.47); 7.5234 (0.83); 7.5201 (1.35); 7.5168 (0.68);

7.4857 (2.36); 7.4821 (0.99); 7.4700 (1.63); 7.4664 (3.04); 7.4527 (0.48); 7.4487 (1.21); 7.4457 (0.68); 7.4087 (1.51); 7.4052 (2.08); 7.3875

(2.96); 7.3314 (1.73); 7.3269 (0.57); 7.3132 (3.23); 7.2939 (1.65); 7.2470 (0.67); 7.2438 (1.17); 7.2406 (0.66); 7.2308 (0.50); 7.2256 (1.51);

7.2202 (0.37); 7.2106 (0.33); 7.2075 (0.53); 7.1365 (1.76); 7.1187 (1.70); 5.3438 (5.95); 3.8183 (0.56); 3.8019 (0.77); 3.7968 (0.75); 3.7803

(0.59); 3.3264 (38.18); 3.0233 (16.00); 2.8902 (7.74); 2.7317 (6.02); 2.7308 (6.16); 2.5248 (0.79); 2.5115 (14.43); 2.5070 (28.64); 2.5024

(37.59); 2.4977 (27.04); 2.4932 (12.69); 2.0947 (0.34); 2.0765 (0.43); 2.0730 (0.39); 2.0612 (0.49); 2.0548 (0.43); 2.0429 (0.48); 2.0395 (0.48);

2.0212 (0.39); 1.7198 (0.40); 1.7031 (0.61); 1.6854 (0.73); 1.6680 (0.53); 1.6514 (0.36); 0.8610 (2.77); 0.8427 (6.03); 0.8244 (2.55); 0.0079

(0.53); −0.0002 (15.46); −0.0086 (0.44)

›Example 387, Solvent: DMSO, Spectrometer: 400.13 MHz

9.8767 (0.82); 8.0246 (0.58); 8.0043 (0.73); 7.8474 (0.47); 7.8280 (0.64); 7.8078 (0.40); 7.5412 (0.75); 7.5163 (0.33); 7.5132 (0.33); 7.3712

(0.86); 7.3598 (1.08); 7.3575 (1.05); 7.1489 (0.66); 7.1306 (0.62); 5.7689 (2.10); 5.3786 (2.23); 3.3443 (11.96); 3.0684 (5.46); 2.5321 (0.36);

2.5186 (5.00); 2.5143 (10.13); 2.5098 (13.61); 2.5053 (9.71); 2.5010 (4.51); 2.3374 (3.68); 1.2399 (16.00)

›Example 388, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5007 (1.97); 8.0764 (1.46); 8.0557 (1.74); 7.9532 (0.33); 7.8306 (1.27); 7.8113 (1.80); 7.7910 (1.17); 7.7230 (2.63); 7.7193 (1.31); 7.7103

(0.84); 7.7053 (3.41); 7.7016 (2.43); 7.5650 (0.49); 7.5532 (0.36); 7.5468 (1.63); 7.5410 (0.50); 7.5318 (0.90); 7.5285 (1.43); 7.5251 (0.74);

7.4978 (2.44); 7.4945 (1.10); 7.4824 (1.70); 7.4787 (3.12); 7.4650 (0.51); 7.4610 (1.24); 7.4578 (0.73); 7.1384 (1.81); 7.1201 (1.76); 5.3573

(6.42); 3.3418 (105.76); 3.0589 (16.00); 2.9544 (0.50); 2.9354 (0.75); 2.9162 (0.61); 2.8913 (2.56); 2.7326 (2.09); 2.7315 (2.00); 2.6341 (0.39);

2.5260 (0.69); 2.5126 (12.21); 2.5082 (23.81); 2.5036 (31.00); 2.4991 (22.64); 2.4946 (10.96); 1.8666 (0.36); 1.8464 (0.93); 1.8260 (1.13);

1.8167 (0.76); 1.8120 (0.85); 1.8005 (0.55); 1.7931 (0.35); 1.7859 (0.42); 1.7809 (0.42); 1.7151 (0.80); 1.7092 (0.57); 1.6964 (1.13); 1.6900

(1.00); 1.6813 (1.32); 1.6776 (1.38); 1.6644 (1.97); 1.6524 (1.31); 1.6464 (1.13); 1.6329 (0.81); 1.6272 (0.68); 1.6138 (0.43); 1.6069 (0.55);

1.5839 (0.50); 1.5754 (0.57); 1.5717 (0.55); 1.5470 (1.08); 1.5376 (1.16); 1.5304 (1.34); 1.5186 (1.09); 1.5118 (0.88); 1.4909 (0.36)

›Example 389, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5069 (1.95); 8.0631 (1.20); 8.0424 (1.43); 7.8301 (1.26); 7.8108 (1.73); 7.7905 (1.14); 7.7318 (0.34); 7.7262 (2.03); 7.7237 (2.61); 7.7199

(1.27); 7.7110 (0.83); 7.7059 (3.46); 7.7022 (2.40); 7.5643 (0.50); 7.5611 (0.32); 7.5524 (0.38); 7.5460 (1.67); 7.5403 (0.50); 7.5311 (0.90);

7.5278 (1.45); 7.5243 (0.73); 7.4967 (2.44); 7.4933 (1.05); 7.4813 (1.69); 7.4776 (3.13); 7.4640 (0.49); 7.4599 (1.24); 7.4567 (0.69); 7.1397

(1.75); 7.1213 (1.70); 5.3531 (6.21); 3.3287 (43.18); 3.0720 (0.45); 3.0539 (16.00); 2.8908 (2.58); 2.7322 (2.01); 2.7312 (2.01); 2.5253 (0.61);

2.5204 (0.97); 2.5119 (10.42); 2.5074 (20.51); 2.5028 (26.96); 2.4982 (19.56); 2.4937 (9.34); 2.3033 (1.58); 2.2849 (2.51); 2.2656 (1.81);

2.2574 (0.75); 2.2377 (0.96); 2.2183 (0.80); 2.1989 (0.38); 2.0272 (0.36); 2.0171 (0.40); 2.0086 (0.62); 2.0066 (0.63); 2.0027 (0.64); 1.9984

(0.94); 1.9880 (0.83); 1.9843 (0.77); 1.9778 (0.93); 1.9744 (0.77); 1.9695 (0.66); 1.9660 (0.70); 1.9607 (0.43); 1.9550 (0.34); 1.9491 (0.43);

1.8059 (0.48); 1.8029 (0.64); 1.8012 (0.64); 1.7871 (0.58); 1.7820 (1.15); 1.7676 (0.89); 1.7584 (0.90); 1.7470 (0.55); 1.7403 (0.55); 1.7364

(0.35); 1.6892 (0.93); 1.6702 (2.13); 1.6514 (2.03); 1.6328 (0.83); 1.6254 (0.43); 1.6188 (0.33); 1.6034 (1.04); 1.5967 (0.79); 1.5799 (1.13);

1.5744 (1.16); 1.5587 (0.66); 1.5535 (0.90); 0.8622 (0.71); −0.0002 (8.05)

›Example 390, Solvent: DMSO, Spectrometer: 399.95 MHz

10.0026 (2.06); 8.0726 (1.55); 8.0521 (1.93); 7.8842 (1.32); 7.8649 (1.90); 7.8448 (1.16); 7.7254 (2.72); 7.7127 (0.89); 7.7076 (3.54); 7.7039

(2.49); 7.5647 (0.51); 7.5615 (0.32); 7.5527 (0.40); 7.5464 (1.71); 7.5408 (0.51); 7.5314 (0.96); 7.5281 (1.45); 7.5247 (0.75); 7.4964 (2.47);

7.4808 (1.78); 7.4771 (3.21); 7.4635 (0.52); 7.4594 (1.29); 7.4563 (0.77); 7.1984 (1.85); 7.1801 (1.80); 5.3767 (6.51); 4.1631 (0.45); 4.1464

(1.65); 4.1298 (1.67); 4.1132 (0.47); 3.3329 (83.44); 3.3215 (1.62); 3.3124 (1.81); 3.2953 (1.74); 3.2809 (1.67); 3.2635 (1.68); 3.2554 (0.80);

3.2376 (0.81); 3.0797 (16.00); 3.0659 (0.37); 2.8913 (0.54); 2.7325 (0.44); 2.5256 (0.68); 2.5123 (11.39); 2.5079 (22.13); 2.5033 (28.90);

2.4987 (21.01); 2.4942 (10.08); 1.3121 (6.45); 1.2955 (6.33); 1.0487 (0.43); 1.0463 (0.44); 1.0409 (0.41); 1.0370 (0.35); 1.0289 (0.75); 1.0207

(0.35); 1.0167 (0.45); 1.0116 (0.44); 1.0090 (0.44); 0.4849 (0.73); 0.4779 (1.04); 0.4735 (1.56); 0.4706 (1.10); 0.4639 (1.32); 0.4594 (1.00);

0.4575 (1.01); 0.4533 (1.43); 0.4475 (0.82); 0.4433 (0.78); 0.2019 (0.81); 0.1930 (1.81); 0.1895 (2.21); 0.1808 (2.16); 0.1776 (1.65); 0.1682

(0.67); −0.0002 (4.96)

›Example 391, Solvent: DMSO, Spectrometer: 400.13 MHz

11.0276 (2.51); 8.1691 (1.68); 8.1490 (2.03); 7.9445 (1.33); 7.9250 (1.90); 7.9049 (1.26); 7.8944 (1.33); 7.8919 (1.10); 7.8750 (1.67); 7.8724

(1.49); 7.8636 (1.00); 7.8600 (0.66); 7.8448 (0.82); 7.8387 (0.91); 7.8346 (0.67); 7.6024 (0.58); 7.5877 (0.69); 7.5821 (1.09); 7.5675 (1.27);

7.5618 (1.30); 7.5539 (2.26); 7.5489 (1.48); 7.5387 (0.67); 7.5339 (0.60); 7.5303 (0.95); 7.5268 (0.99); 7.5174 (0.93); 7.5129 (0.69); 7.4866

(0.58); 7.4845 (0.63); 7.4801 (0.57); 7.4781 (0.56); 7.4631 (0.96); 7.4580 (0.85); 7.4442 (0.43); 7.4419 (0.44); 7.4376 (0.40); 7.4355 (0.37);

7.3955 (0.33); 7.3764 (2.22); 7.3703 (1.53); 7.3644 (3.16); 7.3619 (3.11); 7.2441 (1.85); 7.2261 (1.78); 5.4218 (6.20); 3.3943 (1.10); 3.3445

(54.95); 3.2947 (0.83); 3.0750 (16.00); 2.6789 (0.33); 2.5688 (0.39); 2.5643 (0.77); 2.5598 (1.05); 2.5553 (0.76); 2.5508 (0.39); 2.5323 (1.05);

2.5188 (19.92); 2.5144 (40.84); 2.5099 (55.29); 2.5055 (39.65); 2.5011 (18.54); 2.4693 (0.34); 2.4648 (0.57); 2.4602 (0.76); 2.4556 (0.55);

2.3407 (10.44); 1.9970 (1.24); 1.2523 (0.92); 1.1992 (0.36); 1.1814 (0.67); 1.1636 (0.32); 0.8812 (0.42); 0.8645 (1.36); 0.8469 (0.52)

›Example 392, Solvent: DMSO, Spectrometer: 400.13 MHz

12.5733 (1.72); 7.6261 (3.54); 7.6055 (4.12); 7.3568 (4.66); 7.3091 (3.37); 7.2889 (2.96); 7.0152 (1.30); 6.9964 (1.75); 6.9942 (1.67); 6.9157

(0.67); 6.9082 (0.88); 6.9009 (0.96); 6.8934 (1.47); 6.8892 (0.62); 6.8812 (0.75); 6.8742 (1.83); 6.8629 (4.80); 6.8586 (3.14); 6.8477 (1.14);

6.8438 (0.93); 5.3230 (6.03); 5.1546 (1.11); 5.1461 (2.10); 5.1364 (1.16); 4.4366 (2.33); 4.4323 (2.52); 4.4261 (2.87); 4.0421 (0.58); 4.0242

(0.58); 3.3970 (0.66); 3.3471 (67.02); 3.2973 (0.68); 2.9986 (16.00); 2.5578 (0.39); 2.5301 (0.75); 2.5165 (14.60); 2.5123 (29.33); 2.5078

(39.11); 2.5034 (28.35); 2.4994 (13.71); 2.4626 (0.40); 2.4580 (0.46); 2.4536 (0.35); 2.3547 (10.22); 2.3350 (0.40); 1.9948 (2.54); 1.1969 (0.68);

1.1791 (1.35); 1.1613 (0.67)

›Example 393, Solvent: DMSO, Spectrometer: 399.95 MHz

12.5563 (0.44); 8.1105 (0.44); 8.1034 (3.66); 8.0984 (1.15); 8.0861 (1.23); 8.0811 (3.92); 8.0737 (0.41); 7.9532 (0.76); 7.9040 (1.39); 7.8988

(0.43); 7.8868 (0.45); 7.8817 (1.47); 7.7487 (2.00); 7.7461 (2.66); 7.7422 (1.30); 7.7337 (0.82); 7.7285 (3.41); 7.7247 (2.38); 7.5681 (0.47);

7.5568 (0.34); 7.5498 (1.63); 7.5438 (0.50); 7.5351 (0.94); 7.5317 (1.51); 7.5282 (0.77); 7.5076 (2.49); 7.5042 (1.10); 7.4926 (1.61); 7.4886

(3.05); 7.4753 (0.51); 7.4711 (1.23); 7.4675 (0.73); 7.3845 (0.89); 7.3625 (0.94); 7.3443 (4.57); 7.0898 (0.44); 7.0825 (3.84); 7.0775 (1.19);

7.0650 (1.17); 7.0601 (3.68); 7.0526 (0.46); 7.0294 (1.51); 7.0243 (0.44); 7.0122 (0.43); 7.0071 (1.35); 6.9765 (0.91); 6.9546 (0.80); 5.3767

(5.61); 3.8453 (16.00); 3.8243 (6.22); 3.7997 (0.36); 3.7896 (3.84); 3.3424 (91.62); 3.0171 (15.48); 2.9458 (4.16); 2.8912 (6.02); 2.7850 (0.66);

2.7325 (4.75); 2.5262 (0.75); 2.5128 (14.48); 2.5084 (28.24); 2.5038 (36.64); 2.4992 (26.44); 2.4947 (12.48); −0.0002 (3.63)

›Example 394, Solvent: DMSO, Spectrometer: 399.95 MHz

11.7925 (1.40); 7.9532 (0.38); 7.7322 (2.03); 7.7294 (2.72); 7.7254 (1.35); 7.7170 (0.97); 7.7118 (3.54); 7.7080 (2.39); 7.5623 (0.53); 7.5590

(0.35); 7.5509 (0.41); 7.5440 (1.74); 7.5381 (0.55); 7.5293 (1.01); 7.5259 (1.58); 7.5224 (0.80); 7.4997 (2.63); 7.4963 (1.17); 7.4847 (1.76);

7.4807 (3.26); 7.4673 (0.54); 7.4632 (1.31); 7.4597 (0.76); 7.2557 (3.92); 5.8452 (0.62); 5.8362 (0.33); 5.8193 (0.95); 5.8022 (0.98); 5.7931

(0.36); 5.7853 (0.36); 5.7764 (0.75); 5.7597 (0.35); 5.2821 (5.80); 5.1694 (0.50); 5.1655 (1.19); 5.1608 (1.28); 5.1569 (0.54); 5.1263 (0.45);

5.1224 (1.07); 5.1177 (1.17); 5.1139 (0.49); 5.0947 (0.62); 5.0919 (1.22); 5.0892 (0.99); 5.0870 (1.07); 5.0841 (0.52); 5.0691 (0.56); 5.0662

(1.11); 5.0637 (0.89); 5.0613 (0.99); 5.0585 (0.46); 4.2279 (0.54); 4.2217 (2.07); 4.2049 (4.40); 4.1882 (2.08); 3.3339 (96.70); 3.0302 (16.00);

2.9895 (0.64); 2.8907 (3.07); 2.7322 (2.36); 2.7311 (2.43); 2.5253 (0.63); 2.5205 (1.04); 2.5120 (11.75); 2.5075 (23.44); 2.5029 (30.95); 2.4982

(22.50); 2.4937 (10.74); 2.4225 (0.71); 2.4194 (0.50); 2.4090 (1.29); 2.4058 (2.07); 2.4026 (1.35); 2.3923 (1.29); 2.3890 (2.03); 2.3859 (1.30);

2.3754 (0.48); 2.3723 (0.69); 1.2348 (0.32); 1.1206 (0.53); 1.1054 (0.52); 0.9300 (1.12); 0.0080 (0.33); −0.0002 (9.72)

›Example 395, Solvent: DMSO, Spectrometer: 399.95 MHz

10.1127 (2.58); 7.9532 (0.35); 7.8282 (0.49); 7.8071 (2.01); 7.7951 (2.36); 7.7914 (3.78); 7.7743 (0.55); 7.7257 (1.90); 7.7230 (2.58); 7.7191

(1.22); 7.7105 (0.77); 7.7053 (3.46); 7.7015 (2.34); 7.5623 (0.49); 7.5504 (0.35); 7.5439 (1.62); 7.5382 (0.47); 7.5291 (0.86); 7.5257 (1.44);

7.5222 (0.71); 7.4955 (2.38); 7.4921 (0.99); 7.4802 (1.59); 7.4764 (3.03); 7.4629 (0.46); 7.4588 (1.22); 7.4555 (0.66); 7.1012 (1.29); 7.0958

(1.29); 7.0857 (1.16); 7.0804 (1.21); 5.3305 (6.04); 4.8838 (0.40); 4.8703 (0.58); 4.8681 (0.58); 4.8650 (0.52); 4.8547 (0.58); 4.8513 (0.60);

4.8357 (0.41); 3.3290 (56.41); 3.0698 (16.00); 2.8906 (2.95); 2.7977 (1.23); 2.7910 (2.92); 2.7844 (1.24); 2.7321 (2.26); 2.7309 (2.29); 2.5250

(0.63); 2.5203 (1.02); 2.5117 (11.93); 2.5071 (23.85); 2.5025 (31.49); 2.4979 (22.71); 2.4933 (10.66); 2.2839 (0.80); 2.2773 (0.87); 2.2650

(1.70); 2.2584 (1.61); 2.2472 (1.00); 2.2406 (0.92); 1.7763 (0.54); 1.7588 (1.05); 1.7489 (0.36); 1.7405 (1.33); 1.7350 (0.84); 1.7218 (1.11);

1.7157 (0.41); 1.7017 (0.47); 1.2559 (6.32); 1.2403 (6.30); −0.0002 (1.30)

›Example 396, Solvent: DMSO, Spectrometer: 400.13 MHz

9.8305 (1.11); 7.7772 (0.77); 7.7613 (1.78); 7.7574 (1.15); 7.6655 (1.58); 7.6603 (0.50); 7.6482 (0.52); 7.6430 (1.74); 7.0663 (0.55); 7.0619

(0.57); 7.0502 (0.54); 7.0455 (0.68); 7.0374 (1.69); 7.0322 (0.52); 7.0200 (0.49); 7.0149 (1.57); 5.2763 (2.54); 3.8139 (6.53); 3.3288 (12.65);

3.0511 (6.27); 2.5186 (2.23); 2.5142 (4.61); 2.5097 (6.28); 2.5052 (4.47); 2.5008 (2.09); 1.4705 (16.00)

›Example 397, Solvent: DMSO, Spectrometer: 399.95 MHz

9.0453 (2.48); 8.1017 (1.76); 8.0810 (2.02); 7.8722 (1.32); 7.8528 (1.87); 7.8327 (1.26); 7.7023 (2.63); 7.6985 (1.27); 7.6895 (0.86); 7.6845

(3.61); 7.6807 (2.77); 7.6620 (0.49); 7.6582 (0.34); 7.5610 (0.55); 7.5577 (0.38); 7.5489 (0.40); 7.5427 (1.73); 7.5373 (0.65); 7.5276 (0.91);

7.5243 (1.52); 7.5209 (0.89); 7.4905 (2.49); 7.4868 (1.21); 7.4808 (0.42); 7.4749 (1.78); 7.4713 (3.26); 7.4576 (0.54); 7.4535 (1.29); 7.4505

(0.76); 7.4086 (0.42); 7.3884 (0.56); 7.2850 (2.35); 7.2654 (3.36); 7.2387 (0.35); 7.1763 (4.31); 7.1700 (2.44); 7.1562 (3.05); 7.1507 (2.41);

6.8849 (0.45); 6.8674 (1.97); 6.8497 (1.99); 6.8320 (0.46); 5.3154 (6.26); 5.2630 (0.88); 3.3290 (62.14); 2.9998 (16.00); 2.9549 (2.24); 2.8905

(2.33); 2.7319 (1.82); 2.7313 (1.81); 2.5251 (0.74); 2.5201 (1.19); 2.5117 (13.15); 2.5072 (25.84); 2.5026 (33.70); 2.4980 (24.25); 2.4935

(11.40); 2.3602 (9.97); 2.3417 (1.53); 1.6974 (6.56); 1.6797 (6.47); 1.5052 (0.40); 1.4977 (0.43); 1.1423 (0.43); 1.1347 (0.41); 0.0080

(0.34); −0.0002 (9.54)

›Example 398, Solvent: DMSO, Spectrometer: 399.95 MHz

10.7213 (2.08); 8.0266 (1.24); 8.0060 (1.60); 7.9532 (0.59); 7.8650 (1.33); 7.8457 (1.81); 7.8254 (1.15); 7.7276 (2.02); 7.7250 (2.61); 7.7212

(1.27); 7.7123 (0.83); 7.7072 (3.48); 7.7035 (2.39); 7.5673 (0.50); 7.5553 (0.38); 7.5490 (1.68); 7.5434 (0.49); 7.5340 (0.89); 7.5307 (1.43);

7.5273 (0.72); 7.4981 (2.39); 7.4947 (1.01); 7.4827 (1.73); 7.4790 (3.12); 7.4653 (0.51); 7.4613 (1.27); 7.4581 (0.70); 7.1950 (1.77); 7.1774

(1.72); 7.1591 (1.06); 7.1409 (1.15); 7.1175 (0.50); 7.1143 (0.46); 7.0983 (1.07); 7.0783 (0.68); 7.0752 (0.59); 6.8510 (0.93); 6.8327 (1.64);

6.8167 (2.06); 6.7977 (1.42); 5.3797 (5.98); 5.0599 (1.08); 5.0435 (1.08); 3.3321 (65.01); 3.0608 (0.76); 3.0520 (16.00); 2.8904 (4.79); 2.7320

(3.80); 2.7309 (3.73); 2.5252 (0.63); 2.5118 (12.29); 2.5073 (24.36); 2.5027 (31.90); 2.4981 (23.00); 2.4936 (10.86); 2.2186 (9.97); 1.5536

(5.61); 1.5372 (5.60); −0.0002 (4.58)

›Example 399, Solvent: DMSO, Spectrometer: 400.13 MHz

11.0289 (2.45); 8.1728 (1.63); 8.1526 (1.96); 7.9463 (1.26); 7.9268 (1.80); 7.9067 (1.19); 7.8936 (1.28); 7.8910 (1.07); 7.8741 (1.59); 7.8716

(1.41); 7.8624 (0.97); 7.8588 (0.65); 7.8435 (0.78); 7.8376 (0.89); 7.8335 (0.66); 7.6017 (0.52); 7.5871 (0.65); 7.5815 (1.03); 7.5669 (1.09);

7.5620 (0.77); 7.5472 (0.68); 7.4857 (0.57); 7.4837 (0.62); 7.4792 (0.56); 7.4773 (0.55); 7.4623 (0.95); 7.4573 (0.88); 7.4432 (0.43); 7.4411

(0.46); 7.4368 (0.43); 7.4347 (0.41); 7.4278 (1.03); 7.4079 (2.19); 7.3878 (1.58); 7.2994 (1.45); 7.2982 (1.46); 7.2959 (1.30); 7.2825 (0.77);

7.2787 (1.19); 7.2765 (0.99); 7.2595 (1.82); 7.2541 (3.75); 7.2500 (1.65); 7.2363 (1.73); 7.1494 (1.04); 7.1476 (1.12); 7.1431 (0.98); 7.1412

(0.97); 7.1288 (0.92); 7.1269 (0.92); 7.1225 (0.88); 7.1206 (0.79); 5.4295 (5.89); 3.7900 (16.00); 3.3955 (0.36); 3.3456 (29.34); 3.0728 (14.83);

2.5598 (0.39); 2.5323 (0.66); 2.5187 (11.27); 2.5144 (22.95); 2.5099 (30.99); 2.5054 (22.33); 2.5011 (10.50); 1.9966 (0.95); 1.2494 (0.59);

1.1809 (0.52); 0.8632 (0.82); 0.8455 (0.32)

›Example 400, Solvent: DMSO, Spectrometer: 399.95 MHz

10.2652 (2.65); 7.9532 (0.51); 7.8332 (0.58); 7.8167 (0.44); 7.8122 (2.01); 7.7962 (4.69); 7.7920 (2.88); 7.7755 (0.67); 7.7227 (2.71); 7.7189

(1.30); 7.7100 (0.83); 7.7050 (3.50); 7.7012 (2.41); 7.5618 (0.49); 7.5499 (0.36); 7.5434 (1.68); 7.5377 (0.49); 7.5285 (0.90); 7.5252 (1.45);

7.5218 (0.74); 7.4951 (2.48); 7.4918 (1.06); 7.4797 (1.68); 7.4760 (3.16); 7.4624 (0.49); 7.4583 (1.24); 7.4551 (0.69); 7.1102 (1.40); 7.1058

(1.42); 7.0940 (1.30); 7.0896 (1.32); 5.3309 (6.64); 4.2254 (2.02); 4.2167 (1.77); 4.2138 (2.33); 4.2101 (1.66); 4.2018 (2.14); 3.6070 (2.19);

3.5988 (1.70); 3.5950 (2.32); 3.5921 (1.75); 3.5834 (2.00); 3.4983 (1.51); 3.4808 (4.76); 3.4633 (4.82); 3.4458 (1.57); 3.3406 (100.43); 3.0718

(16.00); 2.8910 (4.19); 2.7316 (3.26); 2.5259 (0.50); 2.5126 (9.41); 2.5081 (18.75); 2.5035 (24.77); 2.4989 (18.10); 2.4944 (8.73); 1.1268 (4.89);

1.1093 (9.87); 1.0918 (4.78); −0.0002 (0.94)

›Example 401, Solvent: DMSO, Spectrometer: 399.95 MHz

10.6923 (2.12); 8.1675 (1.56); 8.1475 (1.87); 7.9531 (0.74); 7.9087 (1.25); 7.8894 (1.70); 7.8692 (1.19); 7.8525 (1.75); 7.8486 (1.79); 7.7784

(1.00); 7.7738 (0.87); 7.7589 (1.12); 7.7541 (0.99); 7.7393 (1.85); 7.7368 (2.47); 7.7328 (1.18); 7.7242 (0.71); 7.7190 (3.30); 7.7152 (2.27);

7.5668 (0.47); 7.5550 (0.33); 7.5484 (1.60); 7.5427 (0.45); 7.5336 (0.83); 7.5302 (1.39); 7.5268 (0.68); 7.5056 (0.43); 7.5004 (2.31); 7.4970

(0.96); 7.4851 (1.51); 7.4813 (2.96); 7.4678 (0.44); 7.4636 (1.20); 7.4603 (0.65); 7.2728 (1.66); 7.2529 (1.47); 7.2122 (1.71); 7.1945 (1.65);

5.4134 (5.91); 3.3294 (54.85); 3.0831 (16.00); 2.8904 (6.35); 2.7318 (4.93); 2.7309 (4.81); 2.5249 (0.62); 2.5201 (0.96); 2.5115 (12.18); 2.5070

(24.48); 2.5023 (32.36); 2.4977 (23.26); 2.4932 (10.91); 2.2935 (12.89); −0.0002 (1.32)

›Example 402, Solvent: DMSO, Spectrometer: 399.95 MHz

10.6837 (2.17); 8.0205 (0.72); 8.0000 (0.94); 7.9529 (0.74); 7.8817 (1.31); 7.8624 (1.78); 7.8422 (1.10); 7.7283 (2.59); 7.7244 (1.27); 7.7156

(0.78); 7.7105 (3.40); 7.7068 (2.38); 7.5683 (0.48); 7.5564 (0.36); 7.5500 (1.61); 7.5443 (0.48); 7.5350 (0.87); 7.5317 (1.42); 7.5283 (0.73);

7.5005 (2.38); 7.4971 (1.03); 7.4851 (1.62); 7.4814 (3.05); 7.4678 (0.49); 7.4637 (1.22); 7.4605 (0.70); 7.3639 (0.36); 7.3549 (4.10); 7.3493

(1.24); 7.3380 (1.33); 7.3323 (4.70); 7.3234 (0.42); 7.2045 (1.75); 7.1867 (1.67); 7.0019 (0.42); 6.9930 (4.43); 6.9873 (1.29); 6.9760 (1.23);

6.9704 (3.94); 6.9614 (0.33); 5.3827 (6.08); 4.8101 (5.71); 3.3411 (108.47); 3.3105 (0.34); 3.0665 (16.00); 2.8907 (5.99); 2.7322 (4.69); 2.7312

(4.75); 2.5258 (0.62); 2.5210 (1.00); 2.5124 (12.35); 2.5079 (24.66); 2.5033 (32.54); 2.4987 (23.64); 2.4942 (11.28); −0.0002 (0.78)

›Example 403, Solvent: DMSO, Spectrometer: 400.13 MHz

12.1396 (0.34); 10.6020 (5.21); 8.0801 (2.66); 8.0593 (3.18); 7.8492 (2.85); 7.8298 (4.09); 7.8096 (2.63); 7.7252 (6.00); 7.7123 (1.93); 7.7074

(7.71); 7.7037 (5.56); 7.5767 (1.06); 7.5736 (0.73); 7.5649 (0.87); 7.5583 (3.73); 7.5527 (1.20); 7.5435 (2.08); 7.5402 (3.28); 7.5369 (1.73);

7.5109 (5.58); 7.4955 (3.81); 7.4917 (7.02); 7.4782 (1.16); 7.4741 (2.74); 7.4709 (1.62); 7.3007 (2.23); 7.2969 (1.10); 7.2818 (6.98); 7.2700

(2.13); 7.2645 (9.09); 7.2571 (7.02); 7.2528 (9.59); 7.2367 (4.30); 7.2202 (0.72); 7.1994 (1.65); 7.1950 (2.14); 7.1902 (1.44); 7.1779 (3.18);

7.1718 (1.01); 7.1655 (0.85); 7.1607 (1.19); 7.1566 (0.70); 7.1426 (4.24); 7.1247 (4.03); 5.3626 (14.12); 4.0441 (0.58); 4.0264 (0.60); 3.4953

(1.84); 3.4772 (6.19); 3.4590 (6.30); 3.4409 (1.93); 3.3931 (0.43); 3.3431 (44.47); 3.2933 (0.42); 2.9174 (2.61); 2.8991 (5.31); 2.8790 (4.02);

2.8387 (0.55); 2.8198 (1.09); 2.8007 (0.68); 2.7299 (4.19); 2.7096 (5.67); 2.6912 (2.75); 2.6835 (0.93); 2.6786 (0.97); 2.6742 (0.70); 2.5639

(1.08); 2.5597 (1.42); 2.5520 (1.40); 2.5321 (4.02); 2.5184 (48.43); 2.5141 (98.74); 2.5096 (132.35); 2.5051 (94.84); 2.5008 (44.47); 2.4641

(1.30); 2.4597 (1.50); 2.4554 (1.06); 2.3408 (0.60); 2.3365 (0.82); 2.3319 (0.59); 1.9969 (2.54); 1.3714 (0.45); 1.2858 (0.43); 1.2512 (1.99);

1.1990 (0.75); 1.1812 (1.36); 1.1634 (0.67); 1.0448 (7.07); 1.0363 (1.50); 1.0268 (16.00); 1.0085 (6.83); 0.8816 (0.93); 0.8648 (2.88); 0.8472

(1.13)

›Example 404, Solvent: DMSO, Spectrometer: 399.95 MHz

10.5534 (2.01); 8.0729 (1.22); 8.0522 (1.45); 7.8401 (1.30); 7.8208 (1.76); 7.8006 (1.19); 7.7322 (0.35); 7.7264 (2.00); 7.7240 (2.61); 7.7201

(1.31); 7.7113 (0.84); 7.7062 (3.52); 7.7024 (2.38); 7.5648 (0.50); 7.5616 (0.32); 7.5529 (0.39); 7.5465 (1.65); 7.5408 (0.49); 7.5316 (0.88);

7.5283 (1.43); 7.5249 (0.73); 7.4974 (2.45); 7.4940 (1.05); 7.4820 (1.67); 7.4782 (3.09); 7.4647 (0.48); 7.4606 (1.22); 7.4573 (0.68); 7.1481

(1.77); 7.1305 (1.70); 5.3570 (6.23); 3.6704 (1.67); 3.6549 (4.26); 3.6391 (2.08); 3.3331 (49.99); 3.0551 (16.00); 2.8909 (0.91); 2.7321 (0.72);

2.5253 (0.68); 2.5203 (1.12); 2.5120 (11.22); 2.5075 (22.00); 2.5029 (28.85); 2.4983 (20.85); 2.4937 (9.84); 2.4414 (1.44); 2.4237 (2.88);

2.4066 (1.29); 1.7634 (0.38); 1.7563 (0.57); 1.7500 (0.59); 1.7402 (1.08); 1.7339 (1.04); 1.7256 (1.73); 1.7232 (1.86); 1.7171 (1.69); 1.7098

(1.67); 1.7064 (1.63); 1.6982 (0.90); 1.6920 (0.97); 1.6895 (0.96); 1.6802 (0.51); 1.6756 (0.44); 1.6695 (0.40); 0.8758 (0.41); −0.0002 (5.70)

›Example 405, Solvent: DMSO, Spectrometer: 400.13 MHz

10.3160 (6.78); 7.8533 (1.75); 7.8325 (4.32); 7.8148 (5.04); 7.8014 (6.46); 7.7829 (2.51); 7.6768 (6.98); 7.6588 (8.41); 7.6555 (6.62); 7.5450

(1.24); 7.5266 (4.04); 7.5086 (3.65); 7.4800 (6.49); 7.4607 (7.93); 7.4432 (3.06); 7.1375 (4.04); 7.1213 (3.91); 5.7628 (0.84); 5.7146 (0.63);

5.7002 (1.42); 5.6866 (1.08); 5.6732 (1.75); 5.6586 (1.71); 5.6455 (1.24); 5.6316 (1.73); 5.6172 (0.83); 5.3241 (16.00); 4.9940 (7.64); 4.9675

(3.49); 4.9519 (3.13); 4.1928 (5.00); 4.1762 (10.71); 4.1591 (9.33); 4.1408 (6.81); 4.0420 (0.33); 3.3307 (39.53); 3.3070 (2.64); 2.9096 (3.20);

2.9031 (6.76); 2.8966 (3.51); 2.6759 (0.36); 2.5735 (3.32); 2.5670 (3.62); 2.5569 (6.81); 2.5503 (6.79); 2.5403 (4.17); 2.5337 (4.19); 2.5107

(47.57); 2.5065 (62.01); 2.5024 (47.29); 2.3335 (0.43); 2.0786 (0.64); 1.9935 (1.09); 1.2831 (0.70); 1.2497 (2.51); 1.1964 (0.38); 1.1787 (0.61);

1.1609 (0.33); 0.8785 (1.09); 0.8709 (0.93); 0.8620 (2.78); 0.8444 (1.25)

›Example 406, Solvent: DMSO, Spectrometer: 400.13 MHz

10.2539 (0.81); 7.8730 (0.64); 7.8671 (0.67); 7.8597 (1.50); 7.6428 (0.64); 7.6402 (0.60); 7.5831 (0.32); 7.1711 (0.34); 7.1636 (0.34); 7.1503

(0.33); 5.8222 (0.93); 5.4111 (1.74); 4.1580 (0.52); 4.1413 (1.13); 4.1245 (0.53); 3.4038 (16.00); 3.1203 (4.23); 2.5728 (2.56); 2.5685 (5.38);

2.5640 (7.36); 2.5595 (5.31); 2.5552 (2.49); 1.6679 (0.39); 1.3915 (0.48); 1.3839 (0.98); 1.3749 (0.74); 1.3659 (0.65); 0.9568 (0.49); 0.9394

(1.34); 0.9216 (0.41)

›Example 407, Solvent: DMSO, Spectrometer: 400.13 MHz

9.8766 (0.83); 8.0274 (0.58); 8.0071 (0.73); 7.8498 (0.46); 7.8305 (0.64); 7.8103 (0.40); 7.4234 (0.37); 7.4035 (0.80); 7.3834 (0.57); 7.2852

(0.53); 7.2830 (0.47); 7.2657 (0.43); 7.2635 (0.35); 7.2446 (0.57); 7.2388 (0.73); 7.2346 (0.51); 7.1584 (0.67); 7.1440 (0.55); 7.1401 (0.99);

7.1257 (0.35); 7.1239 (0.34); 7.1194 (0.33); 5.3862 (2.20); 3.7878 (5.76); 3.3441 (14.78); 3.0656 (5.35); 2.5319 (0.41); 2.5186 (5.93); 2.5143

(11.80); 2.5099 (15.73); 2.5054 (11.28); 2.5011 (5.31); 1.2390 (16.00)

›Example 410, Solvent: DMSO, Spectrometer: 400.13 MHz

7.7340 (3.19); 7.7162 (3.95); 7.7125 (2.78); 7.5658 (0.63); 7.5543 (0.55); 7.5475 (2.12); 7.5416 (0.66); 7.5327 (1.26); 7.5293 (1.89); 7.5259

(0.95); 7.5026 (3.16); 7.4874 (2.23); 7.4836 (3.92); 7.4701 (0.67); 7.4660 (1.58); 7.4626 (0.88); 7.3214 (0.66); 5.7573 (1.04); 5.3255 (5.92);

4.4343 (0.84); 3.4826 (0.32); 3.4596 (0.70); 3.4511 (0.36); 3.4434 (0.38); 3.4089 (16.00); 3.3931 (2.39); 3.3590 (1431.96); 3.3092 (15.32);

3.2880 (0.55); 3.2766 (0.48); 3.2700 (0.33); 3.2601 (0.65); 3.0287 (15.76); 2.6776 (0.63); 2.6730 (0.82); 2.6684 (0.60); 2.5583 (1.05); 2.5537

(1.42); 2.5494 (1.07); 2.5262 (2.40); 2.5128 (52.34); 2.5084 (105.57); 2.5039 (140.95); 2.4995 (100.24); 2.4951 (46.94); 2.4587 (1.33); 2.4540

(1.62); 2.4496 (1.24); 2.3351 (0.67); 2.3306 (0.88); 2.3262 (0.65); 1.6967 (0.98); 1.4294 (0.74); 1.4123 (1.33); 1.3936 (1.32); 1.3749 (0.77);

1.2340 (0.36); 0.9333 (4.56); 0.9150 (9.21); 0.8964 (3.99); −0.0002 (2.70)

›Example 416, Solvent: DMSO, Spectrometer: 400.13 MHz

7.6661 (0.70); 7.6572 (0.72); 7.6498 (1.01); 7.6463 (0.99); 7.6407 (1.73); 7.6269 (1.33); 7.6212 (1.32); 7.6142 (1.04); 7.6031 (0.75); 7.5947

(0.69); 7.3986 (0.81); 7.3919 (3.33); 7.3785 (2.97); 7.3706 (8.67); 7.3610 (6.61); 7.3532 (7.71); 7.3396 (0.62); 6.4579 (4.46); 6.4401 (4.29);

6.3782 (4.59); 6.3578 (4.47); 6.0313 (0.38); 5.9906 (7.71); 5.7606 (0.92); 5.2246 (0.60); 5.1700 (16.00); 4.0378 (0.38); 4.0200 (0.39); 3.4003

(0.38); 3.3850 (0.48); 3.3506 (37.42); 3.3353 (40.85); 3.3010 (0.53); 3.2857 (0.54); 3.2129 (1.21); 2.5527 (0.39); 2.5253 (0.70); 2.5118 (15.44);

2.5074 (31.58); 2.5030 (42.53); 2.4985 (30.35); 2.4942 (14.22); 2.4623 (0.33); 2.4579 (0.49); 2.4534 (0.56); 2.4488 (0.37); 1.9898 (1.70);

1.1923 (0.47); 1.1745 (0.91); 1.1568 (0.46); −0.0002 (4.74)

›Example 417, Solvent: DMSO, Spectrometer: 400.13 MHz

10.1117 (2.91); 7.8366 (0.35); 7.8154 (2.25); 7.8083 (2.37); 7.8015 (5.52); 7.7873 (0.42); 7.6835 (0.58); 7.6796 (0.68); 7.6743 (0.38); 7.6637

(0.42); 7.6587 (0.66); 7.6544 (0.57); 7.5521 (0.58); 7.5484 (0.39); 7.5360 (0.93); 7.5321 (0.99); 7.5162 (0.68); 7.3833 (0.42); 7.3796 (0.44);

7.3708 (0.42); 7.3671 (0.49); 7.3628 (0.66); 7.3592 (0.67); 7.3502 (0.62); 7.3469 (0.66); 7.3427 (0.35); 7.1168 (1.28); 7.1100 (1.26); 7.1029

(1.09); 7.0961 (1.23); 5.3771 (6.26); 4.6774 (0.38); 4.6647 (0.42); 4.6548 (0.71); 4.6453 (0.51); 4.6322 (0.34); 3.4011 (2.49); 3.3700 (0.51);

3.3509 (185.01); 3.3006 (1.44); 3.1931 (16.00); 2.5581 (0.40); 2.5304 (0.44); 2.5256 (0.73); 2.5169 (10.75); 2.5125 (22.54); 2.5080 (30.69);

2.5035 (21.63); 2.4990 (9.87); 1.8775 (0.68); 1.8646 (0.79); 1.8514 (0.82); 1.8457 (0.82); 1.7337 (0.68); 1.7241 (0.74); 1.7105 (0.78); 1.7033

(0.73); 1.5281 (0.35); 1.5188 (0.37); 1.4985 (0.42); 1.4331 (0.79); 1.4083 (1.04); 1.3840 (1.15); 1.3578 (0.93); 1.3513 (0.71); 1.3320 (0.69);

1.3257 (0.79); 1.2997 (0.40); 1.2754 (0.34); 1.2458 (0.53)

›Example 420, Solvent: DMSO, Spectrometer: 400.13 MHz

10.5177 (1.98); 8.0906 (1.25); 8.0699 (1.48); 7.8464 (1.24); 7.8272 (1.69); 7.8069 (1.15); 7.6862 (0.58); 7.6823 (0.66); 7.6769 (0.37); 7.6664

(0.41); 7.6610 (0.64); 7.6569 (0.55); 7.5498 (0.32); 7.5460 (0.57); 7.5423 (0.38); 7.5300 (0.92); 7.5261 (0.99); 7.5138 (0.45); 7.5101 (0.69);

7.3844 (0.46); 7.3807 (0.47); 7.3719 (0.45); 7.3681 (0.49); 7.3639 (0.66); 7.3603 (0.67); 7.3513 (0.64); 7.3480 (0.65); 7.3436 (0.34); 7.1635

(1.74); 7.1461 (1.67); 5.4045 (6.13); 4.0421 (0.67); 4.0243 (0.68); 3.3924 (0.88); 3.3424 (77.23); 3.2925 (0.82); 3.1764 (16.00); 2.5304 (0.40);

2.5256 (0.66); 2.5169 (9.30); 2.5125 (19.45); 2.5080 (26.44); 2.5035 (18.66); 2.4990 (8.55); 2.4075 (1.74); 2.3892 (3.15); 2.3705 (1.92); 1.9943

(3.03); 1.5952 (0.45); 1.5770 (1.28); 1.5582 (1.78); 1.5400 (1.32); 1.5208 (0.55); 1.3307 (1.06); 1.3117 (1.65); 1.2930 (1.68); 1.2748 (1.04);

1.1968 (0.85); 1.1790 (1.70); 1.1612 (0.83); 0.9046 (4.01); 0.8864 (8.31); 0.8679 (3.39)

›Example 442, Solvent: DMSO, Spectrometer: 400.13 MHz

12.5729 (2.54); 7.6843 (1.28); 7.6818 (2.35); 7.6792 (1.44); 7.6636 (2.21); 7.6618 (2.12); 7.6252 (0.49); 7.6156 (4.44); 7.6131 (4.76); 7.6066

(3.50); 7.6052 (3.44); 7.6030 (3.29); 7.5993 (2.30); 7.5827 (0.39); 7.5791 (0.37); 7.5308 (1.54); 7.5219 (1.39); 7.5179 (1.15); 7.5117 (1.39);

7.5091 (1.21); 7.5038 (1.15); 7.4978 (0.97); 7.4899 (0.84); 7.4050 (5.45); 7.0215 (1.58); 7.0200 (1.56); 7.0025 (2.18); 7.0003 (2.04); 6.9469

(0.32); 6.9258 (0.70); 6.9207 (1.10); 6.9131 (1.20); 6.9056 (1.32); 6.8982 (2.05); 6.8941 (0.82); 6.8861 (1.16); 6.8818 (1.70); 6.8789 (2.45);

6.8689 (6.04); 6.8643 (4.65); 6.8532 (1.58); 6.8490 (1.86); 6.8458 (1.21); 6.8400 (0.72); 6.8355 (0.63); 6.8294 (0.39); 6.8236 (0.41); 5.7632

(16.00); 5.3970 (7.78); 5.1698 (1.47); 5.1616 (2.59); 5.1515 (1.50); 5.0500 (0.32); 5.0416 (0.55); 5.0342 (0.34); 4.4778 (0.39); 4.4674 (0.34);

4.4480 (2.63); 4.4411 (3.44); 4.4380 (3.33); 4.4334 (3.02); 4.4121 (0.82); 4.4035 (0.69); 4.2844 (0.43); 4.2773 (0.43); 4.2553 (0.33); 4.2483

(0.33); 3.4069 (2.55); 3.3569 (173.53); 3.3071 (2.33); 3.2639 (0.47); 3.2139 (21.67); 2.6774 (0.36); 2.5628 (0.49); 2.5583 (0.67); 2.5538 (0.49);

2.5307 (0.97); 2.5172 (22.00); 2.5128 (45.68); 2.5083 (61.93); 2.5038 (44.10); 2.4994 (20.54); 2.4674 (0.37); 2.4629 (0.57); 2.4585 (0.72);

2.4539 (0.53); 2.3351 (0.40)

›Example 444, Solvent: DMSO, Spectrometer: 400.13 MHz

10.1810 (2.80); 7.8181 (2.56); 7.8134 (2.63); 7.8054 (5.69); 7.7925 (0.45); 7.7299 (0.60); 7.7257 (0.69); 7.7109 (1.14); 7.7065 (1.41); 7.6907

(0.69); 7.6868 (0.75); 7.6549 (0.36); 7.6505 (0.36); 7.6414 (0.42); 7.6366 (0.77); 7.6338 (0.61); 7.6321 (0.60); 7.6296 (0.52); 7.6217 (0.74);

7.6183 (0.64); 7.6157 (0.82); 7.6110 (0.48); 7.6019 (0.52); 7.5975 (0.45); 7.3961 (0.82); 7.3941 (0.90); 7.3751 (0.84); 7.3727 (0.97); 7.3679

(2.29); 7.3505 (1.85); 7.3480 (2.05); 7.3445 (0.95); 7.3320 (0.97); 7.3293 (0.81); 7.1218 (1.28); 7.1137 (1.33); 7.1092 (1.11); 7.1011 (1.26);

5.3642 (6.35); 4.1042 (1.90); 4.0874 (4.16); 4.0707 (1.98); 3.4274 (7.09); 3.4174 (0.61); 3.3778 (477.76); 3.3546 (4.45); 3.3452 (1.68); 3.3280

(8.75); 3.3155 (1.05); 3.1925 (16.00); 2.5576 (0.34); 2.5305 (0.76); 2.5257 (1.12); 2.5172 (10.43); 2.5127 (21.52); 2.5082 (29.41); 2.5037

(21.37); 2.4992 (10.64); 2.4677 (0.37); 2.4630 (0.47); 2.4584 (0.55); 2.4539 (0.42); 1.6310 (0.86); 1.6139 (1.40); 1.6083 (0.94); 1.5967 (1.04);

1.5798 (0.37); 1.3464 (1.11); 1.3436 (1.07); 1.3359 (1.79); 1.3284 (3.68); 1.3196 (2.75); 1.3104 (2.57); 1.2585 (0.32); 0.9005 (1.82); 0.8941

(1.10); 0.8831 (5.10); 0.8716 (1.24); 0.8651 (1.56)

›Example 449, Solvent: DMSO, Spectrometer: 400.13 MHz

10.5144 (2.11); 8.1062 (1.48); 8.0856 (1.80); 7.8463 (1.28); 7.8270 (1.81); 7.8131 (0.35); 7.8067 (1.27); 7.7266 (0.62); 7.7224 (0.70); 7.7074

(1.16); 7.7032 (1.39); 7.6872 (0.61); 7.6834 (0.71); 7.6579 (0.36); 7.6536 (0.36); 7.6444 (0.42); 7.6396 (0.78); 7.6369 (0.66); 7.6246 (0.69);

7.6214 (0.70); 7.6188 (0.83); 7.6141 (0.47); 7.6049 (0.47); 7.6006 (0.42); 7.3978 (0.97); 7.3766 (0.95); 7.3706 (2.60); 7.3506 (2.78); 7.3332

(0.93); 7.3307 (0.81); 7.1678 (1.83); 7.1501 (1.76); 5.3952 (6.38); 5.3592 (0.36); 3.4051 (3.56); 3.3552 (250.07); 3.3152 (0.86); 3.3053 (2.59);

3.1977 (0.93); 3.1820 (16.00); 2.6938 (0.54); 2.6773 (0.70); 2.6628 (0.39); 2.5581 (0.37); 2.5306 (0.43); 2.5171 (10.44); 2.5127 (21.58); 2.5082

(29.22); 2.5038 (20.80); 2.4994 (9.69); 1.5945 (0.47); 1.5899 (0.40); 1.5804 (0.48); 1.5739 (0.56); 1.5686 (0.41); 1.5591 (0.55); 1.3328 (0.41);

1.3210 (0.50); 1.3149 (0.39); 1.3076 (0.76); 1.3029 (0.59); 1.2937 (0.84); 1.2881 (0.96); 1.2737 (1.49); 1.2599 (1.58); 1.2538 (1.55); 1.2444

(1.63); 1.2389 (1.27); 1.2256 (0.49); 1.2211 (0.53); 1.2136 (0.37); 1.0708 (6.10); 1.0538 (6.09); 0.8836 (2.90); 0.8657 (5.89); 0.8477 (2.34)

›Example 460, Solvent: DMSO, Spectrometer: 400.13 MHz

9.8085 (1.01); 8.1598 (1.38); 7.7943 (0.33); 7.7736 (0.65); 7.7552 (0.64); 7.7280 (0.92); 7.7072 (0.43); 7.5742 (0.32); 7.3320 (0.36); 7.3130

(0.46); 7.3082 (0.34); 7.3009 (0.62); 7.2990 (0.64); 7.2891 (0.36); 7.2790 (0.44); 7.2649 (3.66); 7.2626 (3.50); 7.1349 (0.56); 7.1170 (0.55);

5.2629 (2.06); 5.2442 (0.60); 4.0426 (0.47); 4.0247 (0.48); 2.5628 (0.36); 2.5583 (0.43); 2.5305 (0.69); 2.5170 (11.70); 2.5127 (23.94); 2.5082

(32.26); 2.5038 (23.18); 2.4995 (10.88); 1.9948 (1.61); 1.4828 (0.57); 1.4639 (16.00); 1.3390 (0.76); 1.2383 (0.53); 1.1973 (0.45); 1.1795 (0.87);

1.1617 (0.43)

›Example 464, Solvent: DMSO, Spectrometer: 400.13 MHz

10.5149 (2.05); 8.0915 (1.24); 8.0708 (1.47); 7.8463 (1.24); 7.8270 (1.69); 7.8068 (1.16); 7.6858 (0.58); 7.6819 (0.67); 7.6766 (0.38); 7.6661

(0.41); 7.6611 (0.64); 7.6566 (0.56); 7.6400 (0.32); 7.5497 (0.33); 7.5459 (0.58); 7.5422 (0.39); 7.5299 (0.93); 7.5260 (0.99); 7.5136 (0.45);

7.5100 (0.69); 7.3841 (0.48); 7.3804 (0.48); 7.3715 (0.46); 7.3678 (0.50); 7.3634 (0.66); 7.3599 (0.68); 7.3509 (0.64); 7.3475 (0.66); 7.3434

(0.35); 7.1638 (1.76); 7.1464 (1.67); 7.1452 (1.65); 5.4044 (6.09); 4.0421 (0.96); 4.0243 (0.98); 4.0065 (0.32); 3.3926 (0.75); 3.3426 (74.92);

3.2928 (0.83); 3.1761 (16.00); 2.5305 (0.35); 2.5257 (0.59); 2.5170 (8.84); 2.5125 (18.52); 2.5080 (25.27); 2.5035 (17.91); 2.4990 (8.28);

2.3976 (1.63); 2.3793 (3.06); 2.3607 (1.79); 1.9943 (4.35); 1.6128 (0.34); 1.5942 (1.04); 1.5758 (1.46); 1.5578 (1.01); 1.5396 (0.35); 1.3240

(0.36); 1.3086 (0.78); 1.2917 (1.62); 1.2842 (2.50); 1.2769 (2.04); 1.2664 (1.65); 1.2575 (1.21); 1.2468 (0.66); 1.2394 (0.48); 1.1968 (1.23);

1.1790 (2.42); 1.1612 (1.20); 0.8845 (2.40); 0.8674 (6.29); 0.8497 (2.53)

›Example 480, Solvent: DMSO, Spectrometer: 400.13 MHz

10.5120 (2.13); 8.0883 (1.33); 8.0675 (1.61); 7.8429 (1.24); 7.8235 (1.79); 7.8034 (1.26); 7.7253 (0.60); 7.7211 (0.68); 7.7061 (1.13); 7.7019

(1.41); 7.6859 (0.66); 7.6822 (0.76); 7.6564 (0.37); 7.6521 (0.37); 7.6429 (0.42); 7.6381 (0.78); 7.6354 (0.69); 7.6232 (0.75); 7.6198 (0.71);

7.6173 (0.85); 7.6126 (0.50); 7.6034 (0.48); 7.5991 (0.44); 7.3963 (0.95); 7.3751 (0.97); 7.3695 (2.52); 7.3494 (2.60); 7.3327 (0.96); 7.3302

(0.81); 7.1621 (1.83); 7.1443 (1.75); 5.7601 (2.18); 5.3896 (6.41); 3.4083 (1.59); 3.3580 (127.96); 3.3120 (0.85); 3.3081 (1.79); 3.1982 (0.60);

3.1790 (16.00); 2.5167 (5.65); 2.5124 (11.37); 2.5079 (15.19); 2.5035 (10.91); 2.4992 (5.18); 2.4164 (0.34); 2.4071 (1.83); 2.3889 (3.28);

2.3702 (1.98); 1.5951 (0.46); 1.5769 (1.34); 1.5581 (1.88); 1.5397 (1.41); 1.5207 (0.57); 1.3301 (1.09); 1.3112 (1.76); 1.2924 (1.77); 1.2742

(1.06); 1.2589 (0.62); 1.2433 (0.54); 0.9031 (3.97); 0.8848 (8.04); 0.8664 (3.35); 0.7719 (0.53)

›Example 481, Solvent: DMSO, Spectrometer: 400.13 MHz

12.1354 (3.63); 7.6863 (1.77); 7.6839 (3.15); 7.6813 (1.94); 7.6657 (2.98); 7.6640 (2.88); 7.6223 (0.63); 7.6130 (6.12); 7.6104 (6.40); 7.6038

(4.90); 7.6023 (4.91); 7.6005 (4.72); 7.5968 (3.22); 7.5801 (0.54); 7.5766 (0.51); 7.5407 (0.43); 7.5297 (2.12); 7.5205 (1.92); 7.5170 (1.59);

7.5105 (1.95); 7.5079 (1.63); 7.5025 (1.57); 7.4969 (1.34); 7.4888 (1.20); 7.2990 (8.24); 5.3716 (11.47); 4.0415 (0.41); 4.0237 (0.41); 3.4112

(0.57); 3.4046 (3.66); 3.3904 (0.45); 3.3547 (297.76); 3.3048 (3.10); 3.2635 (0.41); 3.2136 (29.99); 2.5624 (0.43); 2.5579 (0.57); 2.5533 (0.42);

2.5304 (0.77); 2.5169 (16.75); 2.5125 (34.20); 2.5080 (45.90); 2.5035 (32.38); 2.4990 (14.91); 2.4626 (0.45); 2.4579 (0.58); 2.4535 (0.51);

2.4428 (3.59); 2.4245 (6.31); 2.4057 (3.93); 1.9937 (1.83); 1.6132 (0.89); 1.5949 (2.58); 1.5905 (1.24); 1.5762 (3.50); 1.5577 (2.66); 1.5387

(1.12); 1.3472 (0.62); 1.3286 (2.09); 1.3097 (3.33); 1.2910 (3.44); 1.2728 (2.26); 1.2543 (1.20); 1.2490 (1.22); 1.1961 (0.56); 1.1783 (1.02);

1.1605 (0.51); 0.9016 (7.73); 0.8833 (16.00); 0.8648 (6.91); 0.8611 (2.73); 0.8432 (1.04)

›Example 493, Solvent: DMSO, Spectrometer: 400.13 MHz

12.5522 (2.06); 7.6803 (3.75); 7.6777 (2.34); 7.6621 (3.55); 7.6602 (3.42); 7.6238 (0.78); 7.6142 (7.21); 7.6117 (7.59); 7.6052 (5.61); 7.6014

(5.09); 7.5977 (3.66); 7.5811 (0.63); 7.5775 (0.71); 7.5390 (0.52); 7.5277 (2.56); 7.5189 (2.26); 7.5147 (1.86); 7.5086 (2.32); 7.5060 (2.00);

7.5009 (1.88); 7.4946 (1.62); 7.4869 (1.47); 7.4742 (0.32); 7.4653 (0.32); 7.3691 (10.44); 7.3166 (0.70); 7.3107 (4.17); 7.3055 (1.91); 7.2991

(2.41); 7.2922 (6.41); 7.2891 (6.51); 7.2808 (2.88); 7.2770 (3.47); 7.2706 (5.57); 7.2644 (1.46); 7.2591 (2.02); 6.9692 (2.45); 6.9508 (4.41);

6.9365 (2.15); 6.9324 (3.27); 6.9265 (6.15); 6.9241 (7.08); 6.9189 (2.74); 6.9046 (6.50); 6.8958 (0.92); 6.8721 (1.91); 6.8696 (2.30); 6.8501

(2.05); 6.8480 (1.68); 5.7594 (16.00); 5.3876 (12.97); 5.2756 (0.34); 5.0820 (1.00); 5.0655 (3.48); 5.0490 (3.48); 5.0324 (0.97); 4.8317 (0.35);

4.8148 (1.18); 4.7978 (1.19); 4.7809 (0.37); 3.7201 (0.33); 3.4243 (4.78); 3.3745 (216.51); 3.3264 (4.65); 3.2665 (0.91); 3.2163 (35.02); 3.1665

(0.49); 3.0693 (0.41); 2.8342 (0.35); 2.6816 (0.32); 2.6771 (0.45); 2.6725 (0.34); 2.5627 (0.60); 2.5582 (0.78); 2.5537 (0.53); 2.5304 (1.08);

2.5256 (1.83); 2.5169 (26.82); 2.5125 (56.25); 2.5080 (76.63); 2.5035 (54.45); 2.4991 (25.21); 2.4674 (0.52); 2.4629 (0.71); 2.4583 (0.78);

2.4538 (0.51); 2.3393 (0.33); 2.3349 (0.47); 2.3302 (0.35); 1.9929 (1.17); 1.5613 (12.89); 1.5448 (13.20); 1.5181 (0.50); 1.5052 (5.79); 1.4882

(5.66); 1.2371 (0.52); 1.1954 (0.35); 1.1776 (0.65); 1.1598 (0.33)

›Example 499, Solvent: DMSO, Spectrometer: 400.13 MHz

11.9277 (4.49); 7.6901 (4.46); 7.6877 (2.89); 7.6718 (4.46); 7.6704 (4.25); 7.6192 (0.96); 7.6102 (8.62); 7.6077 (9.21); 7.5988 (8.49); 7.5945

(4.78); 7.5777 (0.67); 7.5742 (0.66); 7.5382 (0.64); 7.5273 (2.96); 7.5177 (2.87); 7.5151 (2.48); 7.5081 (2.83); 7.5056 (2.41); 7.4997 (2.26);

7.4948 (1.95); 7.4864 (1.64); 7.3081 (11.76); 5.7619 (7.50); 5.3377 (16.00); 4.2889 (0.49); 4.2726 (0.33); 4.2568 (5.17); 4.2405 (11.56); 4.2242

(5.38); 3.4191 (0.55); 3.4134 (0.51); 3.4078 (3.57); 3.3872 (0.48); 3.3578 (290.56); 3.3254 (0.53); 3.3079 (2.91); 3.2915 (0.61); 3.2416 (40.76);

3.1915 (0.56); 3.1884 (0.70); 2.9337 (3.59); 2.9271 (8.15); 2.9205 (3.78); 2.6071 (3.14); 2.6005 (3.29); 2.5908 (6.69); 2.5842 (6.51); 2.5745

(3.35); 2.5679 (3.14); 2.5584 (0.83); 2.5540 (0.67); 2.5380 (0.50); 2.5309 (0.99); 2.5171 (15.11); 2.5128 (30.62); 2.5083 (41.00); 2.5038 (29.40);

2.4995 (13.88); 2.4628 (0.41); 2.4585 (0.47); 2.4540 (0.35); 1.9936 (1.06); 1.1779 (0.58)

›Example 508, Solvent: DMSO, Spectrometer: 400.13 MHz

7.6971 (0.71); 7.6934 (0.75); 7.6763 (1.46); 7.6728 (1.69); 7.6675 (0.93); 7.6565 (1.04); 7.6514 (1.65); 7.6305 (0.77); 7.6270 (0.75); 7.5544

(1.38); 7.5383 (2.26); 7.5346 (2.37); 7.5185 (1.62); 7.4095 (2.84); 7.3911 (3.87); 7.3893 (3.82); 7.3810 (1.20); 7.3774 (1.28); 7.3707 (3.72);

7.3651 (1.37); 7.3606 (1.72); 7.3572 (1.69); 7.3478 (1.63); 7.3449 (1.68); 7.3366 (0.81); 7.3273 (0.73); 7.3245 (0.72); 6.5282 (4.45); 6.5105

(4.26); 6.4053 (4.50); 6.3848 (4.33); 6.0324 (7.56); 5.7609 (1.95); 5.2252 (16.00); 4.0204 (0.32); 3.3866 (0.69); 3.3361 (45.64); 3.2858 (0.58);

3.2638 (0.51); 3.2134 (34.60); 3.1630 (0.46); 2.9992 (0.44); 2.5586 (0.39); 2.5542 (0.53); 2.5497 (0.39); 2.5121 (15.31); 2.5081 (30.66); 2.5037

(40.81); 2.4993 (29.29); 2.4579 (0.41); 2.4534 (0.51); 2.4489 (0.36); 1.9903 (1.39); 1.2789 (0.45); 1.2453 (2.12); 1.1928 (0.44); 1.1750 (0.74);

1.1572 (0.37); 0.8748 (0.95); 0.8580 (2.85); 0.8404 (1.17); −0.0002 (5.13)

›Example 510, Solvent: DMSO, Spectrometer: 400.13 MHz

7.8076 (0.58); 7.7990 (0.35); 7.7956 (0.33); 7.7338 (1.50); 7.7296 (1.66); 7.7147 (2.92); 7.7104 (3.29); 7.6947 (1.70); 7.6909 (1.72); 7.6457

(0.89); 7.6415 (0.89); 7.6321 (1.11); 7.6274 (1.95); 7.6248 (1.72); 7.6126 (1.82); 7.6092 (1.75); 7.6067 (2.02); 7.6020 (1.20); 7.5928 (1.16);

7.5885 (1.00); 7.5825 (0.35); 7.5790 (0.36); 7.4060 (2.96); 7.3877 (6.18); 7.3668 (6.66); 7.3460 (4.65); 7.3447 (4.64); 7.3277 (2.16); 7.3252

(1.85); 6.5268 (4.43); 6.5091 (4.24); 6.4031 (4.49); 6.3827 (4.29); 6.0269 (7.18); 5.9794 (0.51); 5.7555 (12.51); 5.3534 (0.71); 5.2080 (16.00);

5.1456 (0.70); 3.4050 (1.11); 3.3901 (0.72); 3.3537 (88.85); 3.3129 (0.65); 3.3041 (1.48); 3.2646 (0.43); 3.2135 (34.42); 3.1926 (1.86); 3.1638

(0.55); 3.1483 (0.33); 2.5057 (22.11); 2.5013 (28.75); 2.4970 (21.00); 2.4606 (0.32); 2.4560 (0.41); 2.4516 (0.45); 1.9867 (1.17); 1.5305 (2.66);

1.3700 (1.17); 1.3544 (1.16); 1.2528 (1.57); 1.2372 (1.62); 1.1889 (0.35); 1.1711 (0.65); 1.1533 (0.33)

›Example 512, Solvent: CDCl3, Spectrometer: 300.16 MHz

7.6104 (2.40); 7.6053 (1.28); 7.5941 (0.85); 7.5874 (3.11); 7.5821 (2.41); 7.4879 (0.37); 7.4632 (1.44); 7.4550 (0.50); 7.4446 (0.99); 7.4398

(1.50); 7.4349 (0.83); 7.4170 (2.71); 7.3971 (1.53); 7.3918 (2.74); 7.3745 (0.52); 7.3689 (1.00); 7.3634 (0.63); 7.2621 (3.61); 6.9361 (4.17);

5.3797 (7.09); 3.3237 (2.13); 3.2992 (3.25); 3.2745 (2.30); 3.0246 (16.00); 1.7509 (0.48); 1.7274 (1.18); 1.7020 (1.98); 1.6940 (0.95); 1.6776

(1.39); 1.6519 (0.71); 1.5092 (0.36); 1.4846 (1.13); 1.4595 (1.71); 1.4341 (1.70); 1.4101 (1.04); 1.3862 (0.36); 1.3052 (1.25); 1.2531 (1.10);

0.9659 (3.84); 0.9416 (7.60); 0.9171 (3.27); −0.0002 (2.05)

›Example 513, Solvent: DMSO, Spectrometer: 400.13 MHz

10.5079 (2.05); 8.0859 (1.25); 8.0652 (1.51); 7.8428 (1.24); 7.8236 (1.72); 7.8032 (1.24); 7.7233 (0.60); 7.7190 (0.68); 7.7042 (1.09); 7.6999

(1.35); 7.6839 (0.63); 7.6801 (0.70); 7.6564 (0.36); 7.6520 (0.36); 7.6429 (0.41); 7.6380 (0.76); 7.6354 (0.62); 7.6336 (0.60); 7.6312 (0.52);

7.6231 (0.71); 7.6197 (0.63); 7.6172 (0.79); 7.6125 (0.44); 7.6034 (0.45); 7.5990 (0.39); 7.3959 (0.92); 7.3747 (0.92); 7.3692 (2.44); 7.3491

(2.44); 7.3325 (0.93); 7.3299 (0.76); 7.1614 (1.74); 7.1440 (1.68); 5.3873 (6.13); 3.4294 (6.56); 3.4165 (0.47); 3.4126 (0.48); 3.4078 (0.68);

3.3795 (451.85); 3.3544 (1.07); 3.3478 (0.56); 3.3449 (0.47); 3.3384 (0.35); 3.3297 (5.58); 3.3100 (0.76); 3.1961 (0.72); 3.1769 (16.00); 2.5579

(0.33); 2.5304 (0.40); 2.5255 (0.72); 2.5169 (9.83); 2.5125 (20.41); 2.5080 (27.65); 2.5035 (19.57); 2.4990 (9.03); 2.4581 (0.33); 2.3954 (1.65);

2.3770 (3.07); 2.3584 (1.79); 1.6111 (0.33); 1.5925 (1.02); 1.5741 (1.45); 1.5562 (1.01); 1.5379 (0.34); 1.3218 (0.35); 1.3059 (0.77); 1.2896

(1.63); 1.2823 (2.54); 1.2749 (2.08); 1.2643 (1.74); 1.2579 (1.66); 1.2426 (1.10); 0.8822 (2.38); 0.8651 (6.24); 0.8475 (2.53); 0.7930 (0.33)

›Example 519, Solvent: DMSO, Spectrometer: 400.13 MHz

11.7891 (2.69); 7.6904 (1.74); 7.6881 (3.03); 7.6856 (1.88); 7.6698 (2.90); 7.6682 (2.75); 7.6295 (0.53); 7.6269 (0.69); 7.6203 (1.05); 7.6117

(5.99); 7.6092 (6.15); 7.6022 (4.81); 7.6004 (5.39); 7.5958 (3.35); 7.5791 (0.42); 7.5756 (0.41); 7.5389 (0.45); 7.5280 (2.12); 7.5186 (1.96);

7.5157 (1.58); 7.5088 (1.91); 7.5063 (1.57); 7.5006 (1.51); 7.4954 (1.31); 7.4871 (1.11); 7.2904 (8.13); 7.2392 (0.69); 5.4325 (0.74); 5.3335

(10.81); 4.2500 (0.59); 4.1799 (3.66); 4.1634 (7.84); 4.1468 (3.74); 4.0693 (0.61); 3.4046 (5.19); 3.3914 (0.38); 3.3814 (0.61); 3.3547 (404.79);

3.3344 (1.04); 3.3229 (0.54); 3.3150 (0.34); 3.3047 (4.39); 3.2843 (0.43); 3.2345 (28.39); 3.1929 (2.23); 3.1846 (0.38); 2.6772 (0.34); 2.5627

(0.45); 2.5582 (0.64); 2.5537 (0.45); 2.5307 (0.81); 2.5259 (1.37); 2.5172 (20.14); 2.5128 (42.22); 2.5083 (57.50); 2.5038 (40.91); 2.4994

(19.00); 2.4675 (0.35); 2.4629 (0.54); 2.4584 (0.65); 2.4540 (0.48); 2.3350 (0.37); 1.9942 (0.96); 1.6517 (0.79); 1.6346 (2.47); 1.6280 (0.95);

1.6170 (3.20); 1.5975 (2.85); 1.5810 (1.38); 1.4156 (0.58); 1.3970 (2.04); 1.3780 (3.27); 1.3591 (3.36); 1.3409 (2.07); 1.3226 (0.66); 1.2811

(0.44); 1.2491 (1.92); 1.1967 (0.33); 1.1788 (0.55); 0.9310 (7.70); 0.9126 (16.00); 0.8941 (6.74); 0.8797 (1.73); 0.8708 (0.80); 0.8618 (3.82);

0.8442 (1.70)

›Example 525, Solvent: DMSO, Spectrometer: 400.13 MHz

10.3136 (2.88); 7.8476 (0.58); 7.8266 (1.98); 7.8102 (4.65); 7.8058 (2.87); 7.7890 (0.77); 7.7846 (0.40); 7.7313 (0.61); 7.7271 (0.70); 7.7123

(1.18); 7.7079 (1.45); 7.6922 (0.68); 7.6883 (0.74); 7.6544 (0.34); 7.6500 (0.35); 7.6408 (0.42); 7.6360 (0.77); 7.6332 (0.63); 7.6212 (0.73);

7.6153 (0.83); 7.6105 (0.46); 7.6014 (0.51); 7.5972 (0.44); 7.3935 (0.94); 7.3675 (2.23); 7.3501 (1.89); 7.3482 (2.01); 7.3318 (0.92); 7.3293

(0.78); 7.1370 (1.39); 7.1328 (1.42); 7.1207 (1.31); 7.1164 (1.34); 5.7579 (1.89); 5.3679 (6.56); 4.1954 (2.03); 4.1788 (4.53); 4.1621 (2.09);

3.4791 (0.33); 3.4282 (6.97); 3.3788 (426.80); 3.3442 (0.56); 3.3295 (6.85); 3.3159 (0.86); 3.1958 (16.00); 2.9130 (1.33); 2.9064 (3.02); 2.8998

(1.41); 2.5794 (1.21); 2.5727 (1.29); 2.5627 (2.74); 2.5562 (2.81); 2.5463 (1.36); 2.5395 (1.30); 2.5303 (0.78); 2.5168 (10.27); 2.5125 (20.83);

2.5080 (27.94); 2.5035 (19.75); 2.4991 (9.11); 2.4631 (0.35); 2.4586 (0.43)

›Example 530, Solvent: DMSO, Spectrometer: 400.13 MHz

11.7847 (4.18); 7.6882 (4.37); 7.6859 (2.81); 7.6699 (4.32); 7.6684 (4.17); 7.6264 (0.51); 7.6202 (1.08); 7.6114 (8.54); 7.6089 (8.99); 7.6000

(8.05); 7.5956 (4.71); 7.5787 (0.61); 7.5753 (0.61); 7.5387 (0.63); 7.5277 (2.92); 7.5182 (2.71); 7.5155 (2.34); 7.5085 (2.72); 7.5061 (2.33);

7.5003 (2.13); 7.4952 (1.86); 7.4869 (1.60); 7.2901 (11.92); 7.2385 (0.36); 5.7631 (1.84); 5.4332 (0.35); 5.3336 (16.00); 4.1711 (5.02); 4.1544

(10.81); 4.1377 (5.09); 3.4131 (0.38); 3.4046 (7.16); 3.3546 (450.31); 3.3182 (0.37); 3.3043 (3.32); 3.2855 (0.81); 3.2355 (40.34); 3.2071 (0.33);

3.1920 (1.08); 3.1851 (0.37); 2.6774 (0.41); 2.5626 (0.67); 2.5582 (1.01); 2.5537 (0.81); 2.5492 (0.50); 2.5307 (1.17); 2.5171 (25.22); 2.5128

(51.74); 2.5083 (69.75); 2.5039 (50.03); 2.4996 (23.67); 2.4624 (0.43); 2.4580 (0.58); 2.3398 (0.33); 2.3351 (0.45); 1.6687 (0.73); 1.6510 (2.53);

1.6337 (4.05); 1.6164 (2.91); 1.5993 (1.03); 1.3616 (0.67); 1.3464 (2.78); 1.3365 (5.10); 1.3284 (9.52); 1.3191 (8.57); 1.3102 (6.18); 1.3017

(2.54); 1.2779 (0.77); 0.9014 (5.01); 0.8840 (14.37); 0.8662 (4.55); 0.8519 (0.91); 0.8338 (0.41)

›Example 534, Solvent: DMSO, Spectrometer: 400.13 MHz

10.3216 (2.76); 7.8511 (0.57); 7.8346 (0.44); 7.8301 (1.91); 7.8139 (4.58); 7.8096 (2.73); 7.7930 (0.64); 7.6835 (0.59); 7.6796 (0.68); 7.6743

(0.38); 7.6637 (0.42); 7.6590 (0.65); 7.6544 (0.55); 7.5530 (0.58); 7.5494 (0.39); 7.5370 (0.93); 7.5331 (0.99); 7.5208 (0.46); 7.5171 (0.67);

7.3835 (0.41); 7.3798 (0.44); 7.3708 (0.43); 7.3672 (0.49); 7.3629 (0.65); 7.3593 (0.67); 7.3503 (0.62); 7.3470 (0.66); 7.3428 (0.34); 7.1387

(1.35); 7.1343 (1.38); 7.1224 (1.27); 7.1180 (1.28); 5.7638 (7.80); 5.3856 (6.21); 4.1966 (1.95); 4.1800 (4.43); 4.1633 (2.01); 3.4009 (2.37);

3.3508 (229.28); 3.3194 (0.33); 3.3009 (2.19); 3.2434 (0.35); 3.1948 (16.00); 2.9199 (1.33); 2.9133 (3.15); 2.9066 (1.40); 2.5805 (1.16); 2.5738

(1.21); 2.5638 (2.74); 2.5572 (2.80); 2.5473 (1.29); 2.5406 (1.13); 2.5304 (0.63); 2.5256 (0.97); 2.5169 (13.21); 2.5125 (27.64); 2.5080 (37.59);

2.5034 (26.53); 2.4990 (12.15); 2.4625 (0.32); 2.4580 (0.41)

›Example 538, Solvent: DMSO, Spectrometer: 400.13 MHz

12.1325 (5.11); 7.6841 (4.02); 7.6815 (2.50); 7.6658 (3.80); 7.6641 (3.72); 7.6228 (0.80); 7.6135 (7.73); 7.6109 (8.18); 7.6042 (6.16); 7.6027

(6.36); 7.6012 (6.15); 7.5974 (4.07); 7.5808 (0.61); 7.5772 (0.61); 7.5411 (0.54); 7.5301 (2.70); 7.5208 (2.44); 7.5174 (2.02); 7.5109 (2.45);

7.5083 (2.08); 7.5029 (1.95); 7.4973 (1.70); 7.4892 (1.50); 7.2994 (10.05); 5.3716 (14.60); 4.0419 (0.38); 4.0242 (0.38); 3.4109 (0.69); 3.4057

(6.88); 3.3899 (0.77); 3.3557 (585.31); 3.3258 (0.86); 3.3057 (7.09); 3.2629 (0.54); 3.2128 (38.11); 3.1628 (0.47); 2.6819 (0.38); 2.6773 (0.50);

2.6728 (0.37); 2.5629 (0.65); 2.5583 (0.90); 2.5539 (0.73); 2.5307 (1.29); 2.5172 (28.69); 2.5128 (59.14); 2.5083 (79.86); 2.5038 (56.71);

2.4994 (26.29); 2.4630 (0.79); 2.4583 (1.00); 2.4538 (0.78); 2.4491 (0.53); 2.4337 (4.29); 2.4152 (8.10); 2.3966 (4.66); 2.3397 (0.44); 2.3351

(0.70); 1.9941 (1.67); 1.6315 (0.86); 1.6130 (2.66); 1.5946 (3.69); 1.5766 (2.57); 1.5582 (0.88); 1.3214 (1.02); 1.3054 (2.15); 1.2890 (4.40);

1.2818 (7.02); 1.2742 (5.74); 1.2636 (5.22); 1.2547 (4.45); 1.2449 (3.99); 1.2168 (0.67); 1.1966 (0.68); 1.1788 (1.03); 1.1610 (0.51); 0.8840

(6.22); 0.8669 (16.00); 0.8619 (6.17); 0.8493 (6.72); 0.8444 (2.66); 0.8170 (0.36)

›Example 539, Solvent: DMSO, Spectrometer: 400.13 MHz

12.4467 (0.49); 7.7288 (1.42); 7.7161 (0.46); 7.7111 (1.81); 7.7073 (1.24); 7.5464 (0.89); 7.5317 (0.52); 7.5283 (0.80); 7.5248 (0.41); 7.5019

(1.33); 7.4867 (0.89); 7.4828 (1.64); 7.4653 (0.62); 7.4618 (0.34); 7.2866 (1.15); 5.7567 (3.06); 5.3019 (2.79); 3.4665 (0.36); 3.4168 (6.80);

3.3669 (522.30); 3.3171 (5.64); 3.0140 (8.63); 2.5545 (0.43); 2.5271 (0.55); 2.5136 (14.16); 2.5092 (29.42); 2.5047 (39.85); 2.5002 (28.41);

2.4958 (13.26); 2.4594 (0.35); 2.4549 (0.44); 2.4503 (0.32); 2.0750 (0.62); 1.4895 (16.00)

›Example 543, Solvent: DMSO, Spectrometer: 400.13 MHz

12.4396 (2.27); 7.6840 (1.99); 7.6815 (1.27); 7.6658 (1.92); 7.6640 (1.91); 7.6234 (0.41); 7.6138 (3.82); 7.6114 (4.07); 7.6047 (3.12); 7.6035

(3.11); 7.6013 (2.97); 7.5976 (2.08); 7.5810 (0.35); 7.5774 (0.34); 7.5292 (1.32); 7.5202 (1.21); 7.5163 (1.02); 7.5100 (1.26); 7.5075 (1.11);

7.5022 (1.00); 7.4962 (0.85); 7.4883 (0.78); 7.3600 (0.39); 7.3576 (0.47); 7.3533 (0.34); 7.3382 (4.24); 7.3337 (4.71); 7.3250 (16.00); 7.3185

(6.34); 7.3049 (0.38); 7.2988 (0.67); 7.2968 (0.67); 7.2840 (1.06); 7.2770 (1.13); 7.2747 (1.24); 7.2658 (1.37); 7.2626 (1.42); 7.2574 (0.86);

7.2490 (0.88); 7.2413 (0.41); 5.3809 (7.22); 4.0420 (0.87); 4.0242 (0.89); 3.7676 (8.88); 3.5650 (1.20); 3.4075 (1.86); 3.3955 (0.32); 3.3576

(152.35); 3.3076 (1.72); 3.2186 (18.39); 2.5306 (0.50); 2.5171 (10.66); 2.5128 (21.73); 2.5083 (29.16); 2.5038 (20.82); 2.4995 (9.74); 2.4584

(0.33); 1.9942 (3.82); 1.2476 (1.36); 1.1964 (1.07); 1.1786 (2.07); 1.1608 (1.01); 0.8782 (0.63); 0.8614 (2.01); 0.8437 (0.79)

›Example 552, Solvent: DMSO, Spectrometer: 400.13 MHz

10.1835 (2.74); 7.8187 (2.69); 7.8149 (2.69); 7.8064 (5.53); 7.7299 (0.61); 7.7256 (0.69); 7.7109 (1.15); 7.7065 (1.41); 7.6907 (0.67); 7.6868

(0.72); 7.6548 (0.36); 7.6504 (0.35); 7.6413 (0.42); 7.6365 (0.77); 7.6338 (0.60); 7.6321 (0.58); 7.6296 (0.50); 7.6216 (0.73); 7.6181 (0.62);

7.6156 (0.80); 7.6109 (0.45); 7.6018 (0.50); 7.5975 (0.41); 7.3942 (0.93); 7.3727 (0.98); 7.3679 (2.34); 7.3504 (1.88); 7.3480 (2.11); 7.3319

(0.93); 7.3293 (0.78); 7.1218 (1.28); 7.1131 (1.37); 7.1097 (1.10); 7.1010 (1.21); 5.7587 (0.88); 5.3644 (6.44); 4.1131 (2.04); 4.0965 (4.36);

4.0799 (2.06); 3.4259 (4.59); 3.4205 (0.49); 3.4039 (0.64); 3.3759 (406.79); 3.3504 (0.68); 3.3259 (5.60); 3.3153 (0.88); 3.1924 (16.00); 2.5304

(0.42); 2.5255 (0.71); 2.5170 (9.17); 2.5125 (19.04); 2.5080 (25.79); 2.5035 (18.12); 2.4990 (8.26); 2.4579 (0.35); 1.6317 (0.42); 1.6145 (1.30);

1.6081 (0.52); 1.5972 (1.66); 1.5918 (1.07); 1.5776 (1.39); 1.5610 (0.58); 1.3981 (1.06); 1.3790 (1.65); 1.3653 (0.76); 1.3602 (1.72); 1.3421

(1.01); 1.2583 (0.82); 1.2427 (0.84); 0.9288 (4.20); 0.9104 (8.58); 0.8919 (3.51)

Intensity of sharp signals correlates with the height of the signals in a printed example of a NMR spectrum in cm and shows the real relations of signal intensities. From broad signals several peaks or the middle of the signal and their relative intensity in comparison to the most intensive signal in the spectrum can be shown.

For calibrating chemical shift for 1H spectra, we use tetramethylsilane and/or the chemical shift of the solvent used, especially in the case of spectra measured in DMSO. Therefore in NMR peak lists, tetramethylsilane peak can occur but not necessarily.

The 1H-NMR peak lists are similar to classical 1H-NMR prints and contain therefore usually all peaks, which are listed at classical NMR-interpretation.

Additionally they can show like classical 1H-NMR prints signals of solvents, stereoisomers of the target compounds, which are also object of the invention, and/or peaks of impurities.

To show compound signals in the delta-range of solvents and/or water the usual peaks of solvents, for example peaks of DMSO in DMSO-D 6 and the peak of water are shown in our 1H-NMR peak lists and have usually on average a high intensity.

The peaks of stereoisomers of the target compounds and/or peaks of impurities have usually on average a lower intensity than the peaks of target compounds (for example with a purity>90%).

Such stereoisomers and/or impurities can be typical for the specific preparation process. Therefore their peaks can help to recognize the reproduction of our preparation process via “side-products-fingerprints”.

An expert, who calculates the peaks of the target compounds with known methods (MestreC. ACD-simulation, but also with empirically evaluated expectation values) can isolate the peaks of the target compounds as needed optionally using additional intensity filters. This isolation would be similar to relevant peak picking at classical 1H-NMR interpretation.

Further details of NMR-data description with peak lists you find in the publication “Citation of NMR Peaklist Data within Patent Applications” of the Research Disclosure Database Number 564025.

The following table 2 illustrates in a non limiting manner examples of compounds of formula (V) according to the invention.

In table 2 we use the following abbreviations for specified claimed elements “A 1 ” and “A 2 ” of the generic structure (I) of the invention:

We describe the double bond geometry of the examples of table 2 as shown here:

V (Z, U)

V (U, U)

›V (E, U)

NMR-Peak Lists

The peak list of an example has therefore the form:

δ 1 (intensity 1 ); δ 2 (intensity 2 ); . . . ; δ i (intensity i ); . . . ; δ n (intensity n )

NMR Peak List Table 2

›Example V-1, Solvent: DMSO, Spectrometer: 400.13 MHz

10.2384 (6.32); 9.5810 (13.93); 7.7909 (1.47); 7.7700 (3.84); 7.7525 (4.80); 7.7422 (5.37); 7.7243 (1.83); 7.5899 (3.91);

7.5855 (5.01); 7.5774 (2.97); 7.5723 (4.42); 7.5658 (5.73); 7.5505 (0.33); 7.4352 (0.38); 7.4304 (0.45); 7.4142 (2.59); 7.4070

(9.61); 7.4032 (8.91); 7.3964 (3.44); 7.3887 (5.02); 7.3806 (1.29); 7.3763 (1.37); 7.3706 (0.64); 7.3662 (0.71); 7.1661 (3.23);

7.1511 (3.03); 5.9854 (8.22); 5.4365 (0.34); 5.2038 (13.23); 4.1935 (4.30); 4.1769 (9.43); 4.1602 (4.47); 4.0603 (1.21); 4.0426

(3.71); 4.0247 (3.76); 4.0070 (1.26); 3.3392 (422.26); 3.3159 (2.65); 2.9149 (2.89); 2.9084 (6.35); 2.9018 (3.09); 2.6756

(0.55); 2.5771 (2.62); 2.5705 (2.80); 2.5605 (5.58); 2.5538 (5.57); 2.5438 (3.33); 2.5371 (3.44); 2.5112 (71.28); 2.5068

(94.61); 2.5024 (68.57); 2.3336 (0.58); 1.9937 (16.00); 1.2371 (0.41); 1.1971 (4.22); 1.1793 (8.32); 1.1615 (4.08); 1.0499

(0.39); 1.0347 (0.37)

›Example V-2, Solvent: DMSO, Spectrometer: 400.13 MHz

9.5491

›Tables in the description — 16

TABLE 1

Ex-

Ster-

Y 1

Y 2

Y 3

Y 4

Y 5

X 1

Z 1

Z 2

Z 3

Z 4

LogP

CH 3

amino

1.14 [a]

CH 3

[(pentyloxy)carbonyl]amino

4.44 [a]

CH 3

[(but-3-yn-1-yloxy)carbonyl]amino

3.27 [a]

CH 3

amino

1.54 [a]

CH 3

[(2-cyclohexylethoxy)carbonyl]amino

5.27 [a]

CH 3

[(pent-4-en-1-yloxy)carbonyl]amino

4.06 [a]

CH 3

[(2-phenylethoxy)carbonyl]amino

4.15 [a]

CH 3

heptanoylamino

4.3 [a]

CH 3

heptanoylamino

4.13 [a]

CH 3

(2,3-dihydro-1,4-benzodioxin-2-ylcarbonyl)amino

3.62 [a]

CH 3

(3,4-dihydro-2H-chromen-2-ylcarbonyl)amino

3.94 [a]

CH 3

[(pentyloxy)carbonyl]amino

4.11 [a]

CH 3

pentanoylamino

3.37 [a]

CH 3

(butoxycarbonyl)amino

3.73 [a]

CH 3

pentanoylamino

3.51 [a]

CH 3

[(cyclopentylmethoxy)carbonyl]amino

4.53 [a]

CH 3

(3-fluorobenzoyl)amino

3.69 [a]

CH 3

(butoxycarbonyl)amino

4.04 [a]

CH 3

(2-phenoxypropanoyl)amino

3.71 [a]

CH 3

(3-fluorobenzoyl)amino

3.6 [a]

CH 3

(tert-butoxycarbonyl)amino

3.96 [a]

[(but-3-yn-1-yloxy)carbonyl]amino

3.09 [a]

amino

1.36 [a]

amino

1.58 [a]

CH 3

amino

1.14 [a]

CH 3

[(pentyloxy)carbonyl]amino

4.24 [a]

CH 3

(2-fluorobenzoyl)amino

3.44 [a]

CH 3

[(2-fluorophenoxy)acetyl]amino

3.51 [a]

CH 3

[(2-chlorophenyl)acetyl]amino

3.76 [a]

CH 3

amino

1.45 [a]

CH 3

[(2-methoxyphenoxy)acetyl]amino

3.8 [a]

CH 3

octanoylamino

4.71 [a]

CH 3

(propoxycarbonyl)amino

3.62 [a]

CH 3

(4-chlorobutanoyl)amino

3.27 [a]

CH 3

(cyclopropylcarbonyl)amino

2.92 [a]

methoxy

CH 3

[(pentyloxy)carbonyl]amino

4.46 [a]

CH 3

hept-6-ynoylamino

3.37 [a]

CH 3

[(4-fluorophenoxy)acetyl]amino

3.53 [a]

CH 3

{[(2-methylpent-4-yn-2-yl)oxy]carbonyl}amino

3.94 [a]

CH 3

[(1-methylcyclohexyl)carbonyl]amino

4.36 [a]

CH 3

[(pentyloxy)carbonyl]amino

4.41 [a]

fluoro

CH 3

(3-fluorobenzoyl)amino

3.79 [a]

CH 3

(1-phenylethyl)amino

2.86 [a]

CH 3

(3-methoxybenzoyl)amino

3.62 [a]

CH 3

{[(4-methylpentyl)oxy]carbonyl}amino

4.81 [a]

CH 3

(diphenylacetyl)amino

4.48 [a]

CH 3

[(3-methylbutoxy)carbonyl]amino

4.06 [a]

CH 3

(3-ethoxypropanoyl)amino

2.96 [a]

CH 3

{[2-(3-bromophenyl)ethoxy]carbonyl}amino

4.61 [a]

CH 3

[2-(3-methoxyphenoxy)propanoyl]amino

3.71 [a]

CH 3

[(3-methoxyphenoxy)acetyl]amino

3.73 [a]

CH 3

acetylamino

2.44 [a]

CH 3

[(hexyloxy)carbonyl]amino

4.51 [a]

CH 3

(phenylcarbonyl)amino

3.51 [a]

CH 3

[(4-bromophenoxy)acetyl]amino

3.94 [a]

CH 3

{[(3-methylpentyl)oxy]carbonyl}amino

4.78 [a]

CH 3

(2-chlorobenzoyl)amino

3.46 [a]

difluoromethyl

[(but-3-yn-1-yloxy)carbonyl]amino

3.64 [a]

CH 3

(4,4-dimethylpentanoyl)amino

4.15 [a]

CH 3

{[(1-phenylpropan-2-yl)oxy]carbonyl}amino

4.49 [a]

ethyl

[(cyclohexyloxy)carbonyl]amino

4.77 [a]

CH 3

(3-cyclopropylpropanoyl)amino

3.51 [a]

CH 3

(3-chloropropanoyl)amino

3.02 [a]

CH 3

[2-(3-chlorophenoxy)propanoyl]amino

4.38 [a]

CH 3

[(4-bromophenoxy)acetyl]amino

4.2 [a]

CH 3

[(4-fluorophenoxy)acetyl]amino

3.73 [a]

CH 3

4-[5-(pyridinium-1-yl)pentanoyl]amino formate

1.67 [a]

CH 3

[(1-phenylethoxy)carbonyl]amino

4.23 [a]

CH 3

[2-(3-methoxyphenoxy)propanoyl]amino

3.97 [a]

cyanomethyl

[(but-3-yn-1-yloxy)carbonyl]amino

3.31 [a]

CH 3

propanoylamino

2.77 [a]

CH 3

[(2,2-dimethylpropoxy)carbonyl]amino

4.01 [a]

CH 3

(5-bromopentanoyl)amino

3.59 [a]

CH 3

(2-phenylethyl)amino

2.78 [a]

CH 3

(phenoxycarbonyl)amino

3.48 [a]

CH 3

[(2-methylphenoxy)acetyl]amino

4.17 [a]

CH 3

(3-cyclohexylpropanoyl)amino

4.73 [a]

CH 3

(bicyclo[2.2.1]hept-2-ylacetyl)amino

4.39 [a]

CH 3

[(2-methyl-2-phenylpropoxy)carbonyl]amino

4.71 [a]

CH 3

[2-(3-methylphenoxy)propanoyl]amino

3.99 [a]

CH 3

(2-bromobenzoyl)amino

3.51 [a]

CH 3

[2-(2-methylphenoxy)propanoyl]amino

4.12 [a]

fluoro

CH 3

amino

1.34 [a]

CH 3

(3-cyclopentylpropanoyl)amino

4.36 [a]

CH 3

(3,4-dihydro-1H-isochromen-3-ylcarbonyl)amino

4.17 [a]

prop-2-yn-1-yl

[(but-3-yn-1-yloxy)carbonyl]amino

3.46 [a]

CH 3

bis(tert-butoxycarbonyl)amino

4.77 [a]

ethyl

[(4-methoxyphenyl)acetyl]amino

3.7 [a]

CH 3

{[2-(4-fluorophenyl)ethoxy]carbonyl}amino

4.19 [a]

chloro

CH 3

amino

1.72 [a]

CH 3

(2-methoxybenzoyl)amino

3.71 [a]

fluoro

CH 3

[(but-3-yn-1-yloxy)carbonyl]amino

3.39 [a]

CH 3

(2-butoxypropanoyl)amino

4.3 [a]

CH 3

[(cyclopentyloxy)acetyl]amino

4.04 [a]

CH 3

(5-methylhexanoyl)amino

4.25 [a]

amino

1.2 [a]

fluoro

CH 3

(tert-butoxycarbonyl)amino

3.92 [a]

CH 3

nonanoylamino

5.11 [a]

CH 3

oct-7-enoylamino

4.3 [a]

100

CH 3

[(3-fluorophenoxy)acetyl]amino

3.58 [a]

101

methoxy

CH 3

[(4-methoxyphenyl)acetyl]amino

3.51 [a]

102

CH 3

(4-methylpentanoyl)amino

3.85 [a]

103

CH 3

[(cyclopentyloxy)carbonyl]amino

3.76 [a]

104

ethyl

[(but-3-yn-1-yloxy)carbonyl]amino

3.51 [a]

105

CH 3

[(3-chlorophenoxy)acetyl]amino

4.1 [a]

106

CH 3

{[2-(2-chlorophenyl)ethoxy]carbonyl}amino

4.56 [a]

107

CH 3

[(hexyloxy)carbonyl]amino

4.85 [a]

108

methoxy

CH 3

amino

1.32 [a]

109

CH 3

[(prop-2-en-1-yloxy)carbonyl]amino

3.42 [a]

110

CH 3

[(cyclopentyloxy)carbonyl]amino

4.09 [a]

111

CH 3

hexanoylamino

3.89 [a]

112

methoxy

CH 3

[(cyclohexyloxy)carbonyl]amino

4.49 [a]

113

CH 3

[2-(2-bromophenoxy)propanoyl]amino

4.2 [a]

114

CH 3

(2-fluorobenzoyl)amino

3.73 [a]

115

CH 3

[2-(2-methoxyphenoxy)propanoyl]amino

4.15 [a]

116

CH 3

(cyclohexylmethyl)amino

3.02 [a]

117

CH 3

[(benzyloxy)carbonyl]amino

4.31 [a]

118

CH 3

(cyclobutylcarbonyl)amino

3.27 [a]

119

CH 3

{[(1-methoxy-1-oxopropan-2-

3.17 [a]

yl)oxy]carbonyl}amino

120

CH 3

{[(2-methylbutan-2-yl)oxy]carbonyl}amino

1.99 [a]

121

CH 3

amino

1.47 [a]

122

CH 3

{[(5,5,5-trifluoropentyl)oxy]carbonyl}amino

4.06 [a]

123

CH 3

[(2,4-dichlorophenoxy)acetyl]amino

4.23 [a]

124

CH 3

(2-ethylbutanoyl)amino

3.71 [a]

125

CH 3

[(2-fluorophenoxy)acetyl]amino

3.76 [a]

126

CH 3

[2-(benzyloxy)propanoyl]amino

3.85 [a]

127

ethyl

[(pent-4-yn-2-yloxy)carbonyl]amino

3.81 [a]

128

CH 3

[2-(3-methylphenoxy)propanoyl]amino

4.35 [a]

129

fluoro

amino

1.35 [a]

130

ethyl

(2,3-dihydro-1,4-benzodioxin-2-ylcarbonyl)amino

4.14 [a]

131

methoxy

CH 3

(tert-butoxycarbonyl)amino

3.99 [a]

132

CH 3

(2-methylbutanoyl)amino

3.41 [a]

133

CH 3

{[2-(2-methylphenyl)ethoxy]carbonyl}amino

4.51 [a]

134

CH 3

2-furoylamino

3.13 [a]

135

(tert-butoxycarbonyl)amino

3.76 [a]

136

CH 3

{(2E)-2-(benzyloxy)imino]ethyl}amino

3.35 [a]

137

CH 3

[(1-methylcyclopropyl)carbonyl]amino

3.31 [a]

138

CH 3

(phenoxycarbonyl)amino

3.73 [a]

139

fluoro

CH 3

(2,2-dimethylpropanoyl)amino

3.61 [a]

140

fluoro

CH 3

pentanoylamino

3.61 [a]

141

methoxy

CH 3

bis(tert-butoxycarbonyl)amino

4.44 [a]

142

CH 3

(tert-butoxycarbonyl)amino

4.34 [a]

143

CH 3

(3-iodobenzoyl)amino

4.19 [a]

144

CH 3

(4-methylbenzoyl)amino

3.85 [a]

145

CH 3

[(2-phenylpropoxy)carbonyl]amino

4.46 [a]

146

CH 3

[(3S,5S,7S)-adamantan-1-ylacetyl]amino

5.08 [a]

147

CH 3

(cyclohexylcarbonyl)amino

3.92 [a]

148

CH 3

(2,2-dimethylpropanoyl)amino

3.48 [a]

149

methoxy

CH 3

{[(4-methylpentan-2-yl)oxy]carbonyl}amino

4.72 [a]

150

fluoro

CH 3

[(pentyloxy)carbonyl]amino

4.19 [a]

151

CH 3

{[2-(3-methoxyphenyl)ethoxy]carbonyl}amino

4.11 [a]

152

ethyl

(tert-butoxycarbonyl)amino

4.26 [a]

153

CH 3

(4-methylpent-3-enoyl)amino

3.59 [a]

154

CH 3

(2,2-dimethylpropanoyl)amino

3.42 [a]

155

CH 3

[2-(3-bromophenoxy)propanoyl]amino

4.17 [a]

156

CH 3

[2-(benzyloxy)propanoyl]amino

4.15 [a]

157

methoxy

CH 3

amino

1.35 [a]

158

CH 3

(2-iodobenzoyl)amino

3.6 [a]

159

CH 3

[(2-bromophenoxy)acetyl]amino

3.89 [a]

160

CH 3

(2,2-dimethylhexanoyl)amino

4.48 [a]

161

fluoro

CH 3

[(pentyloxy)carbonyl]amino

4.51 [a]

162

CH 3

[(tert-butylsulfanyl)carbonyl]amino

4.39 [a]

163

CH 3

hexylamino

2.64 [a]

164

CH 3

[(4-chlorophenoxy)acetyl]amino

3.85 [a]

165

CH 3

[(1-phenylcyclopropyl)carbonyl]amino

4.43 [a]

166

CH 3

[3-(1-methylcyclopropyl)propanoyl]amino

3.87 [a]

167

CH 3

hept-6-enoylamino

3.89 [a]

168

CH 3

[(benzyloxy)carbonyl]amino

3.99 [a]

169

CH 3

pentanoylamino

3.7 [a]

170

CH 3

(3-methyl-2-furoyl)amino

3.71 [a]

171

CH 3

[(2-methoxyphenoxy)acetyl]amino

3.55 [a]

172

ethyl

(2-methylpentanoyl)amino

4.06 [a]

173

CH 3

(3,3-dimethylbutanoyl)amino

3.78 [a]

174

CH 3

(4-iodobenzoyl)amino

4.29 [a]

175

CH 3

{[2-(2-methoxyphenyl)ethoxy]carbonyl}amino

4.31 [a]

176

ethyl

pentanoylamino

3.76 [a]

177

CH 3

isobutyrylamino

3.11 [a]

178

CH 3

(2-chlorobenzoyl)amino

3.64 [a]

179

CH 3

[2-(3-bromophenoxy)propanoyl]amino

4.46 [a]

180

CH 3

(4-methylbenzoyl)amino

3.76 [a]

181

CH 3

(2-methoxybenzoyl)amino

3.87 [a]

182

CH 3

[(3-methylbutoxy)carbonyl]amino

4.39 [a]

183

CH 3

(butoxycarbothioyl)amino

4.53 [a]

184

CH 3

[3-(2-methoxyphenyl)propanoyl]amino

3.87 [a]

185

methoxy

CH 3

{[(4-methylpentan-2-yl)oxy]carbonyl}amino

4.72 [a]

186

CH 3

{[2-(2-fluorophenyl)ethoxy]carbonyl}amino

4.21 [a]

187

CH 3

(4-bromobenzoyl)amino

4.14 [a]

188

CH 3

[3-(methylsulfanyl)propanoyl]amino

3.09 [a]

189

CH 3

[(2,2-dichloro-1-ethyl-3-

4.35 [a]

methylcyclopropyl)carbonyl]amino

190

CH 3

[(2,5-dimethoxyphenyl)acetyl]amino

3.6 [a]

191

methoxy

CH 3

(trifluoroacetyl)amino

3.37 [a]

192

CH 3

[(2-ethylbutoxy)carbonyl]amino

4.78 [a]

193

fluoro

(tert-butoxycarbonyl)amino

3.68 [a]

194

CH 3

[(benzyloxy)acetyl]amino

3.6 [a]

195

CH 3

[(cyclopentyloxy)acetyl]amino

3.73 [a]

196

CH 3

[(4-chlorophenyl)acetyl]amino

3.92 [a]

197

CH 3

diethylamino

2.63 [a]

198

CH 3

hexanoylamino

3.76 [a]

199

CH 3

{[(1-ethoxypropan-2-yl)oxy]carbonyl}amino

3.53 [a]

200

CH 3

[(hexan-2-yloxy)carbonyl]amino

4.78 [a]

201

ethyl

[(benzyloxy)carbonyl]amino

4.24 [a]

202

CH 3

(3,5-difluorobenzoyl)amino

3.92 [a]

203

fluoro

CH 3

(phenylacetyl)amino

3.46 [a]

204

CH 3

[2-(4-bromophenoxy)propanoyl]amino

4.46 [a]

205

CH 3

[(4,4,4-trifluorobutoxy)carbonyl]amino

3.85 [a]

206

fluoro

CH 3

(tert-butoxycarbonyl)amino

4.09 [a]

207

ethyl

[(hex-5-yn-2-yloxy)carbonyl]amino

4.04 [a]

208

CH 3

(cyclohexylacetyl)amino

4.26 [a]

209

ethyl

amino

1.42 [a]

210

CH 3

{[2-(3-methylphenyl)ethoxy]carbonyl}amino

4.53 [a]

211

methoxy

CH 3

hexanoylamino

3.92 [a]

212

CH 3

(3-methoxybenzoyl)amino

3.58 [a]

213

CH 3

[(2-methylphenoxy)acetyl]amino

3.85 [a]

214

fluoro

(tert-butoxycarbonyl)amino

3.78 [a]

215

CH 3

(butoxycarbonyl)amino

4.36 [a]

216

CH 3

[2-(4-bromophenoxy)propanoyl]amino

4.17 [a]

217

CH 3

(4-methoxybenzoyl)amino

3.53 [a]

218

CH 3

[methoxy(phenyl)acetyl]amino

3.85 [a]

219

CH 3

[2-(2-methoxyphenoxy)propanoyl]amino

3.89 [a]

220

CH 3

[difluoro(phenoxy)acetyl]amino

3.89 [a]

221

CH 3

(2,2-dimethylbutanoyl)amino

3.8 [a]

222

CH 3

{[1-(2,4-

4.96 [a]

dichlorophenyl)cyclopropyl]carbonyl}amino

223

CH 3

{[(4-methylpentan-2-yl)oxy]carbonyl}amino

5.05 [a]

224

CH 3

[(pentyloxy)carbonyl]amino

4.78 [a]

225

CH 3

[(2-methylpropoxy)carbonyl]amino

4.01 [a]

226

CH 3

[(pent-4-yn-2-yloxy)carbonyl]amino

3.57 [a]

227

CH 3

(3,4-dihydro-1H-isochromen-1-ylcarbonyl)amino

4.1 [a]

228

methoxy

CH 3

[(but-3-yn-1-yloxy)carbonyl]amino

3.33 [a]

229

CH 3

[(4-methylphenoxy)acetyl]amino

3.8 [a]

230

CH 3

l-4-({[(1R,2R)-2-phenylcyclopropyl]carbonyl}amino)

4.04 [a]

231

CH 3

[2-(2-chlorophenoxy)propanoyl]amino

4.41 [a]

232

CH 3

(2-phenoxypropanoyl)amino

3.96 [a]

233

CH 3

{[(2-methylpentan-2-yl)oxy]carbonyl}amino

4.77 [a]

234

fluoro

CH 3

(2,3-dihydro-1,4-benzodioxin-2-ylcarbonyl)amino

3.7 [a]

235

CH 3

(3,7-dimethyloct-6-enoyl)amino

4.88 [a]

236

CH 3

(1-cyclohexylpropan-2-yl)amino

5.14 [a]

237

CH 3

(3,3,3-trifluoropropanoyl)amino

3.19 [a]

238

CH 3

{[2-(4-bromophenyl)ethoxy]carbonyl}amino

4.63 [a]

239

CH 3

[(benzyloxy)carbonyl]amino

3.73 [a]

240

CH 3

(butoxyacetyl)amino

3.97 [a]

241

CH 3

{[(2-methylpropyl)sulfanyl]carbonyl}amino

4.39 [a]

242

CH 3

[(but-3-yn-2-yloxy)carbonyl]amino

3.41 [a]

243

CH 3

(2-bromobenzoyl)amino

3.67 [a]

244

CH 3

(2-methylhexanoyl)amino

4.2 [a]

245

CH 3

(4-chlorobenzoyl)amino

4.01 [a]

246

fluoro

CH 3

(tert-butoxycarbonyl)amino

4.06 [a]

247

CH 3

(5,5-dimethylhexanoyl)amino

4.53 [a]

248

CH 3

(2-methylpentanoyl)amino

3.8 [a]

249

fluoro

CH 3

(tert-butoxycarbonyl)amino

3.94 [a]

250

CH 3

[(cyclohexyloxy)carbonyl]amino

4.82 [a]

251

CH 3

(4-fluorobenzoyl)amino

3.55 [a]

252

CH 3

(phenylacetyl)amino

3.65 [a]

253

CH 3

(2-cyclohexylethyl)amino

2.96 [a]

254

fluoro

CH 3

(tert-butoxycarbonyl)amino

4.01 [a]

255

CH 3

[(2,5-difluorophenyl)acetyl]amino

3.62 [a]

256

CH 3

pent-4-enoylamino

3.25 [a]

257

CH 3

(phenylcarbonyl)amino

3.44 [a]

258

fluoro

CH 3

[(2-phenylethoxy)carbonyl]amino

4.24 [a]

259

fluoro

CH 3

amino

1.41 [a]

260

CH 3

[2-(4-chlorophenoxy)propanoyl]amino

4.35 [a]

261

fluoro

CH 3

bis(tert-butoxycarbonyl)amino

4.51 [a]

262

CH 3

(2,4-dichlorobenzoyl)amino

3.94 [a]

263

CH 3

(3,5-difluorobenzoyl)amino

3.8 [a]

264

CH 3

(thiophen-2-ylacetyl)amino

3.42 [a]

265

CH 3

(propoxycarbonyl)amino

3.35 [a]

266

CH 3

butanoylamino

3.13 [a]

267

CH 3

(4-cyclohexylbutanoyl)amino

5.14 [a]

268

CH 3

[(6E)-8-methylnon-6-enoyl]amino

5.06 [a]

269

CH 3

[(2-bromophenoxy)acetyl]amino

4.25 [a]

270

ethyl

[(2-phenylethoxy)carbonyl]amino

4.41 [a]

271

CH 3

butanoylamino

3.02 [a]

272

CH 3

[(2-phenylethoxy)carbonyl]amino

4.49 [a]

273

CH 3

{[(4-methylpentan-2-yl)oxy]carbonyl}amino

4.68 [a]

274

CH 3

[(2,4-dichlorophenoxy)acetyl]amino

4.61 [a]

275

CH 3

[2-(2-bromophenoxy)propanoyl]amino

4.53 [a]

276

CH 3

[2-(4-chlorophenoxy)propanoyl]amino

4.07 [a]

277

CH 3

[4-(4-chloro-2-methylphenoxy)butanoyl]amino

4.73 [a]

278

CH 3

[(benzyloxy)acetyl]amino

3.87 [a]

279

CH 3

(tert-butoxycarbonyl)(2-cyclohexylethyl)amino

6.73 [a]

280

ethyl

(3-methylbutanoyl)amino

3.7 [a]

281

CH 3

(3-iodobenzoyl)amino

4.31 [a]

282

CH 3

[(pentan-2-yloxy)carbonyl]amino

4.36 [a]

283

CH 3

(propoxycarbothioyl)amino

4.11 [a]

284

CH 3

(2-ethylhexanoyl)amino

4.49 [a]

285

CH 3

[(heptan-2-yloxy)carbonyl]amino

5.19 [a]

286

CH 3

[(2-methylpropoxy)carbonyl]amino

3.71 [a]

287

CH 3

[2-(4-methylphenoxy)propanoyl]amino

4.35 [a]

288

CH 3

[(2-cyanoethoxy)carbonyl]amino

2.78 [a]

289

CH 3

(3-bromobenzoyl)amino

4.04 [a]

290

methoxy

CH 3

[(benzyloxy)carbonyl]amino

4.04 [a]

291

CH 3

[(4-methyl-3,4-dihydro-1H-isochromen-3-

4.35 [a]

yl)carbonyl]amino

292

CH 3

{[(3-methylbutan-2-yl)oxy]carbonyl}amino

4.27 [a]

293

CH 3

{[(4,4,5,5,5-pentafluoropentyl)oxy]carbonyl}amino

4.29 [a]

294

CH 3

(2-phenoxybenzoyl)amino

4.76 [a]

295

fluoro

CH 3

(butoxycarbonyl)amino

4.14 [a]

296

CH 3

[(4-methylphenoxy)acetyl]amino

4.07 [a]

297

fluoro

CH 3

[(2-phenylethoxy)carbonyl]amino

4.26 [a]

298

CH 3

{[2-(2-bromophenyl)ethoxy]carbonyl}amino

4.66 [a]

299

CH 3

(tert-butoxycarbonyl)(hexyl)amino

6.57 [a]

300

ethyl

[(pentyloxy)carbonyl]amino

4.72 [a]

301

CH 3

[3-(4-fluorophenyl)propanoyl]amino

3.81 [a]

302

CH 3

hex-5-ynoylamino

3.17 [a]

303

CH 3

decanoylamino

5.54 [a]

304

CH 3

acryloylamino

2.77 [a]

305

CH 3

{[(3,3-dimethylbutan-2-yl)oxy]carbonyl}amino

4.56 [a]

306

CH 3

{[(1,3-dichloropropan-2-yl)oxy]carbonyl}amino

3.83 [a]

307

CH 3

[difluoro(phenoxy)acetyl]amino

4.08 [a]

308

CH 3

amino

1.84 [a]

309

CH 3

[(1-fluorocyclopropyl)carbonyl]amino

3.31 [a]

310

CH 3

{[2-(4-methoxyphenyl)ethoxy]carbonyl}amino

4.08 [a]

311

CH 3

[(3-fluorophenoxy)acetyl]amino

3.78 [a]

312

CH 3

[2-(4-methylphenoxy)propanoyl]amino

4.02 [a]

313

CH 3

(phenoxyacetyl)amino

3.73 [a]

314

CH 3

[(3-bromophenoxy)acetyl]amino

3.94 [a]

315

CH 3

(phenoxyacetyl)amino

3.51 [a]

316

CH 3

(2,2-dimethylhexanoyl)amino

4.63 [a]

317

CH 3

{[(2-methylbut-3-yn-2-yl)oxy]carbonyl}amino

3.6 [a]

318

CH 3

[(3-methoxyphenoxy)acetyl]amino

3.53 [a]

319

CH 3

(2-phenoxypropanoyl)amino

3.99 [a]

320

CH 3

[(butylsulfanyl)carbonyl]amino

4.41 [a]

321

CH 3

[2-(3-chlorophenoxy)propanoyl]amino

4.1 [a]

322

CH 3

(2-phenoxybutanoyl)amino

3.99 [a]

323

CH 3

(bicyclo[2.2.1]hept-5-en-2-ylcarbonyl)amino

3.68 [a]

324

fluoro

CH 3

(3-phenylpropanoyl)amino

3.87 [a]

325

methoxy

CH 3

[(2-phenylethoxy)carbonyl]amino

4.19 [a]

326

CH 3

amino

1.82 [a]

327

CH 3

(2,5-dimethylbenzoyl)amino

4.06 [a]

328

methoxy

CH 3

(2-methylpentanoyl)amino

3.87 [a]

329

CH 3

(3-phenoxybenzoyl)amino

4.61 [a]

330

CH 3

bis[(4-fluorophenoxy)carbonyl]amino

4.2 [a]

331

CH 3

(2-iodobenzoyl)amino

3.76 [a]

332

CH 3

(2,4-dichlorobenzoyl)amino

4.14 [a]

333

methoxy

(tert-butoxycarbonyl)amino

3.69 [a]

334

CH 3

[(3-methylphenoxy)acetyl]amino

4.07 [a]

335

CH 3

[(2-bromophenyl)acetyl]amino

3.85 [a]

336

CH 3

(2,5-dimethylbenzoyl)amino

3.94 [a]

337

CH 3

{[(2-methylpentyl)oxy]carbonyl}amino

4.83 [a]

338

fluoro

CH 3

(2-phenoxypropanoyl)amino

3.76 [a]

339

CH 3

[(cyclohexyloxy)carbonyl]amino

4.48 [a]

340

CH 3

(3-methylbutanoyl)amino

3.44 [a]

341

CH 3

(phenylacetyl)amino

3.53 [a]

342

CH 3

[(prop-2-yn-1-yloxy)carbonyl]amino

3.13 [a]

343

CH 3

[(but-3-yn-1-yloxy)carbonyl]amino

3.59 [a]

344

CH 3

(3-methylbenzoyl)amino

3.87 [a]

345

CH 3

(5-methyl-2-furoyl)amino

3.46 [a]

346

CH 3

[3-(4-chlorophenyl)propanoyl]amino

4.17 [a]

347

CH 3

(3-phenylpropanoyl)amino

3.78 [a]

348

CH 3

(2,2,3,3,4,4,4-heptafluorobutanoyl)amino

4.17 [a]

349

CH 3

{[2-(4-chlorophenyl)ethoxy]carbonyl}amino

4.53 [a]

350

CH 3

[(2-methylbutoxy)carbonyl]amino

4.44 [a]

351

fluoro

CH 3

[(cyclohexyloxy)carbonyl]amino

4.54 [a]

352

CH 3

(3,4-dichlorobenzoyl)amino

4.54 [a]

353

CH 3

{[(2-methylhexan-2-yl)oxy]carbonyl}amino

5.1 [a]

354

methoxy

amino

1.29 [a]

355

CH 3

hexanoylamino

4.24 [a]

356

CH 3

[(3-methylphenoxy)acetyl]amino

3.8 [a]

357

CH 3

(4-phenoxybenzoyl)amino

4.58 [a]

358

methoxy

CH 3

pentanoylamino

3.55 [a]

359

CH 3

{[2-(3-chlorophenyl)ethoxy]carbonyl}amino

4.51 [a]

360

CH 3

formyl(methyl)amino

3.06 [a]

361

methoxy

CH 3

(butoxycarbonyl)amino

4.06 [a]

362

methoxy

CH 3

(3-methylbutanoyl)amino

3.46 [a]

363

CH 3

[(but-3-en-1-yloxy)carbonyl]amino

3.71 [a]

364

CH 3

(4-fluorobenzoyl)amino

3.62 [a]

365

CH 3

(cyclopentylacetyl)amino

3.92 [a]

366

CH 3

[2-(2-chlorophenoxy)propanoyl]amino

4.07 [a]

367

CH 3

(2-acetoxy-2-methylpropanoyl)amino

3.15 [a]

368

CH 3

[(3-chlorophenoxy)acetyl]amino

3.87 [a]

369

CH 3

{[2-(4-methylphenyl)ethoxy]carbonyl}amino

4.53 [a]

370

fluoro

CH 3

pentanoylamino

3.48 [a]

371

CH 3

[(2,2-dichloro-1-isopropylcyclopropyl)carbonyl]amino

4.35 [a]

372

CH 3

[(2,2-dimethylpropoxy)carbonyl]amino

4.36 [a]

373

CH 3

(4-bromobenzoyl)amino

4.01 [a]

374

CH 3

(6-bromohexanoyl)amino

3.85 [a]

375

CH 3

[(4-methylphenyl)acetyl]amino

3.85 [a]

376

fluoro

CH 3

hexanoylamino

3.99 [a]

377

CH 3

(4-phenylbutanoyl)amino

4.04 [a]

378

CH 3

(phenylacetyl)amino

3.37 [a]

379

CH 3

(methoxyacetyl)amino

2.73 [a]

380

CH 3

(3-bromobenzoyl)amino

4.16 [a]

381

CH 3

(2-naphthylacetyl)amino

4.12 [a]

382

CH 3

[(3-bromophenoxy)acetyl]amino

4.2 [a]

383

fluoro

CH 3

{[(4-methylpentan-2-yl)oxy]carbonyl}amino

4.77 [a]

384

CH 3

pentanoylamino

3.83 [a]

385

CH 3

[(butylsulfanyl)carbothioyl]amino

4.8 [a]

386

CH 3

(2-phenylbutanoyl)amino

4.23 [a]

387

CH 3

(2,2-dimethylpropanoyl)amino

3.85 [a]

388

CH 3

(cyclopentylcarbonyl)amino

3.62 [a]

389

CH 3

(3-cyclobutylpropanoyl)amino

4.02 [a]

390

CH 3

[2-(cyclopropylmethoxy)propanoyl]amino

3.78 [a]

391

CH 3

(3-fluorobenzoyl)amino

3.99 [a]

392

CH 3

(2,3-dihydro-1,4-benzodioxin-2-ylcarbonyl)amino

3.9 [a]

393

CH 3

(4-methoxybenzoyl)amino

3.48 [a]

394

CH 3

[(but-3-en-1-yloxy)carbonyl]amino

3.44 [a]

395

CH 3

[(hex-5-yn-2-yloxy)carbonyl]amino

3.8 [a]

396

methoxy

CH 3

(tert-butoxycarbonyl)amino

3.96 [a]

397

CH 3

{[1-(4-methylphenyl)cyclopropyl]carbonyl}amino

4.76 [a]

398

CH 3

[2-(2-methylphenoxy)propanoyl]amino

4.46 [a]

399

methoxy

CH 3

(3-fluorobenzoyl)amino

3.72 [a]

400

CH 3

[(2-ethoxyethoxy)carbonyl]amino

3.17 [a]

401

CH 3

(3,4-dimethylbenzoyl)amino

4.16 [a]

402

CH 3

[(4-chlorophenoxy)acetyl]amino

4.1 [a]

403

ethyl

(3-phenylpropanoyl)amino

4.01 [a]

404

CH 3

(5-chloropentanoyl)amino

3.44 [a]

405

prop-2-en-1-yl

[(but-3-yn-1-yloxy)carbonyl]amino

3.61 [a]

406

fluoro

CH 3

[(pentyloxy)carbonyl]amino

4.53 [a]

407

methoxy

CH 3

(2,2-dimethylpropanoyl)amino

3.55 [a]

408

CH 3

[(3-cyclopentylpropoxy)carbonyl]amino

5.31 [a]

409

CH 3

{[(2-methoxybenzyl)oxy]carbonyl}amino

4.06 [a]

410

CH 3

(butoxycarbothioyl)amino

4.56 [a]

411

CH 3

[(pyridin-4-ylmethoxy)carbonyl]amino

2.01 [a]

412

CH 3

{[(3-methyloxetan-3-yl)methoxy]carbonyl}amino

2.96 [a]

413

CH 3

{[(2-chlorobenzyl)oxy]carbonyl}amino

4.34 [a]

414

CH 3

[(but-2-yn-1-yloxy)carbonyl]amino

3.42 [a]

415

CH 3

[(oct-2-yn-1-yloxy)carbonyl]amino

4.86 [a]

416

fluoro

CH 3

amino

1.26 [a]

417

fluoro

CH 3

[(cyclohexyloxy)carbonyl]amino

4.46 [a]

418

CH 3

[(hept-2-yn-1-yloxy)carbonyl]amino

4.51 [a]

419

CH 3

[(heptyloxy)carbonyl]amino

5.25 [a]

420

fluoro

CH 3

pentanoylamino

3.55 [a]

421

CH 3

(ethoxycarbonyl)amino

3.21 [a]

422

CH 3

{[3-(trimethylsilyl)propoxy]carbonyl}amino

5.28 [a]

423

CH 3

[(3,3-dimethylbutoxy)carbonyl]amino

4.68 [a]

424

CH 3

{[3-chloro-2-(hydroxymethyl)-2-

3.19 [a]

methylpropoxy]carbonyl}amino

425

CH 3

[(4-methylphenoxy)carbonyl]amino

4.03 [a]

426

CH 3

[(2-propylphenoxy)carbonyl]amino

4.54 [a]

427

CH 3

[(propan-2-yloxy)carbonyl]amino

3.55 [a]

428

CH 3

{[(2,6-dichlorobenzyl)oxy]carbonyl}amino

4.56 [a]

429

CH 3

[(3-methoxybutoxy)carbonyl]amino

3.37 [a]

430

CH 3

[(2-ethylphenoxy)carbonyl]amino

4.25 [a]

431

CH 3

[(3-ethoxypropoxy)carbonyl]amino

3.44 [a]

432

CH 3

{[(4-cyanobenzyl)oxy]carbonyl}amino

3.61 [a]

433

CH 3

[(tetrahydro-2H-pyran-2-ylmethoxy)carbonyl]amino

3.5 [a]

434

CH 3

[(pyridin-3-ylmethoxy)carbonyl]amino

2.17 [a]

435

CH 3

[(3-ethylphenoxy)carbonyl]amino

4.34 [a]

436

CH 3

[(pent-4-yn-1-yloxy)carbonyl]amino

3.51 [a]

437

CH 3

[(pyridin-2-ylmethoxy)carbonyl]amino

2.64 [a]

438

CH 3

[(2-cyclopropylethoxy)carbonyl]amino

4.01 [a]

439

CH 3

{[2-(2-ethoxyethoxy)ethoxy]carbonyl}amino

3.13 [a]

440

CH 3

{[(trimethylsilyl)methoxy]carbonyl}amino

4.53 [a]

441

CH 3

{[(3-methoxybenzyl)oxy]carbonyl}amino

3.96 [a]

442

chloro

CH 3

(2,3-dihydro-1,4-benzodioxin-2-ylcarbonyl)amino

3.73 [a]

443

CH 3

({[3-(trimethylsilyl)prop-2-yn-1-

4.63 [a]

yl]oxy}carbonyl)amino

444

fluoro

CH 3

[(pentyloxy)carbonyl]amino

4.34 [a]

445

CH 3

{[(1,1,1-trichloro-2-methylpropan-2-

4.91 [a]

yl)oxy]carbonyl}amino

446

CH 3

{[(4-oxopenty)oxy]carbonyl}amino

2.96 [a]

447

CH 3

{[2-(2-chloroethoxy)ethoxy]carbonyl}amino

3.29 [a]

448

CH 3

{[(4-methylpent-3-en-1-yl)oxy]carbonyl}amino

4.39 [a]

449

fluoro

CH 3

(2-methylpentanoyl)amino

3.73 [a]

450

CH 3

{[(4-methoxybenzyl)oxy]carbonyl}amino

3.92 [a]

451

CH 3

{[(2,4,4-trimethylpentyl)oxy]carbonyl}amino

5.39 [a]

452

CH 3

[(hept-6-en-3-yn-1-yloxy)carbonyl]amino

4.01 [a]

453

CH 3

{[(3Z)-hept-3-en-1-yloxy]carbonyl}amino

4.81 [a]

454

CH 3

[(hex-5-en-1-yloxy)carbonyl]amino

4.39 [a]

455

CH 3

[(hex-4-yn-2-yloxy)carbonyl]amino

3.89 [a]

456

CH 3

[(2-phenoxyethoxy)carbonyl]amino

3.94 [a]

457

CH 3

[(3-methoxy-3-methylbutoxy)carbonyl]amino

3.59 [a]

458

CH 3

{[(3-methylbenzyl)oxy]carbonyl}amino

4.34 [a]

459

CH 3

[(2-bromoethoxy)carbonyl]amino

3.42 [a]

460

fluoro

(tert-butoxycarbonyl)amino

3.76 [a]

461

CH 3

[(2,2-dichloroethoxy)carbonyl]amino

3.74 [a]

462

CH 3

l-4-[({[(1R,2S,5R)-2-isopropyl-5-

5.9 [a]

methylcyclohexyl]oxy}carbonyl)amino]

463

CH 3

{[(2-ethylhexyl)oxy]carbonyl}amino

5.54 [a]

464

fluoro

CH 3

hexanoylamino

3.92 [a]

465

CH 3

[(octyloxy)carbonyl]amino

5.65 [a]

466

CH 3

[(prop-1-en-2-yloxy)carbonyl]amino

3.37 [a]

467

CH 3

[(4-propylphenoxy)carbonyl]amino

4.74 [a]

468

CH 3

{[(3-phenylprop-2-yn-1-yl)oxy]carbonyl}amino

4.25 [a]

469

CH 3

[(3-propylphenoxy)carbonyl]amino

4.72 [a]

470

CH 3

[(mesityloxy)carbonyl]amino

4.56 [a]

471

CH 3

{[2-(pyridin-2-yl)ethoxy]carbonyl}amino

2.07 [a]

472

CH 3

{[3-(dimethylamino)propoxy]carbonyl}amino

1.88 [a]

473

CH 3

[(cyclopropylmethoxy)carbonyl]amino

3.64 [a]

474

CH 3

{[(2-oxo-1,3-dioxolan-4-yl)methoxy]carbonyl}amino

2.75 [a]

475

CH 3

{[(1-cyclopropylpropan-2-yl)oxy]carbonyl}amino

4.32 [a]

476

CH 3

4-{[(4-nitrobenzyl)oxy]carbonyl}amino

3.83 [a]

477

CH 3

{[(3-cyanobenzyl)oxy]carbonyl}amino

3.65 [a]

478

CH 3

[(4-ethylphenoxy)carbonyl]amino

4.39 [a]

479

CH 3

[(pent-4-en-2-yloxy)carbonyl]amino

4.01 [a]

480

fluoro

CH 3

pentanoylamino

3.44 [a]

481

chloro

CH 3

pentanoylamino

3.53 [a]

482

CH 3

[(vinyloxy)carbonyl]amino

3.33 [a]

483

CH 3

[(tetrahydrofuran-2-ylmethoxy)carbonyl]amino

3.11 [a]

484

CH 3

[(hex-5-yn-1-yloxy)carbonyl]amino

3.78 [a]

485

CH 3

[(1-cyclohexylethoxy)carbonyl]amino

5.25 [a]

486

CH 3

{[(6-chlorohexyl)oxy]carbonyl}amino

4.49 [a]

487

CH 3

{[(2-methylbenzyl)oxy]carbonyl}amino

4.29 [a]

488

CH 3

{[(4Z)-hept-4-en-1-yloxy]carbonyl}amino

4.78 [a]

489

CH 3

[(3-methoxy-2,2-dimethyl-3-

3.65 [a]

oxopropoxy)carbonyl]amino

490

CH 3

{[2-(allyloxy)ethoxy]carbonyl}amino

3.37 [a]

491

CH 3

[(3-methoxy-2-methyl-3-oxopropoxy)carbonyl]amino

3.33 [a]

492

CH 3

[(4-isopropylphenoxy)carbonyl]amino

4.67 [a]

493

chloro

CH 3

(2-phenoxypropanoyl)amino

3.81 [a]

494

CH 3

[(2,6-dimethylphenoxy)carbonyl]amino

4.2 [a]

495

CH 3

{[(2-fluorobenzyl)oxy]carbonyl}amino

4.01 [a]

496

CH 3

{[2-(cyclohexyloxy)ethoxy]carbonyl}amino

4.31 [a]

497

CH 3

{[3-(pyridin-3-yl)propoxy]carbonyl}amino

2.11 [a]

498

CH 3

{[(3,5-dimethylbenzyl)oxy]carbonyl}amino

4.68 [a]

499

chloro

CH 3

[(but-3-yn-1-yloxy)carbonyl]amino

3.19 [a]

500

CH 3

[(2,2,2-trifluoroethoxy)carbonyl]amino

3.57 [a]

501

CH 3

{[(3-fluorobenzyl)oxy]carbonyl}amino

4.01 [a]

502

CH 3

[(1-cyclopentylethoxy)carbonyl]amino

4.82 [a]

503

CH 3

[(pent-2-yn-1-yloxy)carbonyl]amino

3.78 [a]

504

CH 3

{[(2-methylprop-2-en-1-yl)oxy]carbonyl}amino

3.73 [a]

505

CH 3

{[(4Z)-hex-4-en-1-yloxy]carbonyl}amino

4.39 [a]

506

CH 3

{[(5-methylhexyl)oxy]carbonyl}amino

5.17 [a]

507

CH 3

{[(2E)-hex-2-en-1-yloxy]carbonyl}amino

4.56 [a]

508

fluoro

CH 3

amino

1.34 [a]

509

CH 3

{[(4E)-hex-4-en-1-yloxy]carbonyl}amino

4.44 [a]

510

fluoro

CH 3

amino

1.23 [a]

511

CH 3

[(hept-3-yn-1-yloxy)carbonyl]amino

4.31 [a]

512

CH 3

[(butylsulfanyl)carbothioyl]amino

4.81 [a]

513

fluoro

CH 3

hexanoylamino

3.81 [a]

514

CH 3

[(4-acetoxybutoxy)carbonyl]amino

3.35 [a]

515

CH 3

{[2-(acryloyloxy)ethoxy]carbonyl}amino

3.21 [a]

516

CH 3

{[3-(methylsulfanyl)propoxy]carbonyl}amino

3.68 [a]

517

CH 3

l-4-[({[(1R,2S,5R)-2-isopropyl-5-

5.9 [a]

methylcyclohexyl]oxy}carbonyl)amino]

518

CH 3

[(2-chloroethoxy)carbonyl]amino

3.29 [a]

519

chloro

CH 3

(butoxycarbonyl)amino

3.85 [a]

520

CH 3

{[(3-ethyloxetan-3-yl)methoxy]carbonyl}amino

3.27 [a]

521

CH 3

[(2-methylphenoxy)carbonyl]amino

3.96 [a]

522

CH 3

{[(3E)-hex-3-en-1-yloxy]carbonyl}amino

4.46 [a]

523

CH 3

[(3-cyclohexylpropoxy)carbonyl]amino

5.71 [a]

524

CH 3

[(tetrahydrofuran-3-ylmethoxy)carbonyl]amino

2.98 [a]

525

fluoro

CH 3

[(but-3-yn-1-yloxy)carbonyl]amino

3.21 [a]

526

CH 3

[(cyclohex-3-en-1-ylmethoxy)carbonyl]amino

4.51 [a]

527

CH 3

[(2-thienylmethoxy)carbonyl]amino

3.83 [a]

528

CH 3

{[(4-fluorobenzyl)oxy]carbonyl}amino

3.99 [a]

529

CH 3

[(1,3-dioxolan-4-ylmethoxy)carbonyl]amino

2.73 [a]

530

chloro

CH 3

[(pentyloxy)carbonyl]amino

4.25 [a]

531

CH 3

[(2-propoxyethoxy)carbonyl]amino

3.57 [a]

532

CH 3

[(4-methoxyphenoxy)carbonyl]amino

3.69 [a]

533

CH 3

[(2-cyclopentylethoxy)carbonyl]amino

4.9 [a]

534

fluoro

CH 3

[(but-3-yn-1-yloxy)carbonyl]amino

3.31 [a]

535

CH 3

{[(2Z)-hex-2-en-1-yloxy]carbonyl}amino

4.53 [a]

536

CH 3

[(2,2,2-trichloroethoxy)carbonyl]amino

4.15 [a]

537

CH 3

{[2-(tetrahydro-2H-pyran-4-

3.44 [a]

yl)ethoxy]carbonyl}amino

538

chloro

CH 3

hexanoylamino

3.89 [a]

539

CH 3

[(tert-butylsulfanyl)carbonyl]amino

4.04 [a]

540

CH 3

{[(3Z)-hex-3-en-1-yloxy]carbonyl}amino

4.44 [a]

541

CH 3

[(cyclohexylmethoxy)carbonyl]amino

4.88 [a]

542

CH 3

{[2-(trimethylsilyl)ethoxy]carbonyl}amino

4.88 [a]

543

chloro

CH 3

(phenylacetyl)amino

3.51 [a]

544

CH 3

[(3-chloropropoxy)carbonyl]amino

3.6 [a]

545

CH 3

[(2-isopropoxyethoxy)carbonyl]amino

3.44 [a]

546

CH 3

{[(4-methylbenzyl)oxy]carbonyl}amino

4.31 [a]

547

CH 3

(methoxycarbonyl)amino

2.84 [a]

548

CH 3

[(pent-3-yn-1-yloxy)carbonyl]amino

3.58 [a]

549

CH 3

[(3-cyclopropylpropoxy)carbonyl]amino

4.37 [a]

550

CH 3

[(4-chlorobutoxy)carbonyl]amino

3.83 [a]

551

CH 3

[(2-fluoroethoxy)carbonyl]amino

2.96 [a]

552

fluoro

CH 3

(butoxycarbonyl)amino

3.92 [a]

553

CH 3

[(3-isopropylphenoxy)carbonyl]amino

4.64 [a]

554

CH 3

[(2-ethoxy-2-oxoethoxy)carbonyl]amino

3.21 [a]

TABLE 2

Ex-no

Y 1

Y 2

Y 3

Y 4

Y 5

Z 1

Z 2

Z 3

Z 4

Stereo

LogP

V-1

[(but-3-yn-1-yloxy)carbonyl]amino

Z, U

2.1 [a]

V-2

amino

Z, U

0.43 [a]

V-3

amino

Z, U

0.41 [a]

V-5

fluoro

(tert-butoxycarbonyl)amino

Z, U

2.68 [a]

V-6

methoxy

amino

U, U

0.58 [a]

V-7

CH 3

amino

U, U

0.75 [a]

V-8

fluoro

(tert-butoxycarbonyl)amino

Z, U

2.68 [a]

V-9

amino

U, U

0.39 [a]

V-10

chloro

amino

Z, U

0.73 [a]

V-11

(tert-butoxycarbonyl)amino

Z, U

2.54 [a]

V-12

fluoro

amino

U, U

0.56 [a]

V-13

methoxy

(tert-butoxycarbonyl)amino

Z, U

2.51 [a]

V-14

(tert-butoxycarbonyl)amino

Z, U

2.57 [a]

V-15

CH 3

amino

Z, U

0.89 [a]

V-16

fluoro

(tert-butoxycarbonyl)amino

U, U

2.9 [a]

TABLE 3

Ex.	Y 1	Y 2	Y 3	Y 4	Y 5	X 1	LogP
VII-1	H	H	H	H	H	Me	3.21 [a]

Ex_no.	Eff. %
2	100
3	98
5	95
6	98
7	95
8	98
9	95
10	95
11	100
12	95
13	95
14	95
15	98
16	98
17	98
18	95
19	95
20	95
21	97
26	93
58	80
70	84
74	95
86	90
104	93
111	95
136	95
148	97
154	95
163	95
168	92
198	95
199	97
226	92
282	92
322	75
342	92
347	92
405	95

TABLE Plasmopara test (grapevines)/preventive

Ex_no.	Eff. %
2	97
3	100
5	88
6	100
7	96
8	99
9	94
10	96
11	98
12	94
13	93
14	96
15	97
16	94
17	94
18	100
19	97
20	94
21	100
37	80
39	97
44	98
50	95
51	91
54	93
59	98
68	90
74	94
80	98
85	73
92	93
95	100
100	74
102	91
104	100
111	100
116	93
120	84
136	75
140	85
148	100
152	70
163	96
166	95
167	86
168	100
173	86
180	95
195	95
198	100
199	100
206	81
208	91
226	100
228	93
233	78
240	80
244	86
245	93
248	85
281	97
282	96
284	79
291	77
292	90
295	89
296	74
302	92
307	98
312	95
316	84
317	91
318	93
321	82
325	84
327	95
336	91
340	79
342	100
343	95
344	93
347	100
352	79
355	75
364	100
365	98
376	93
378	95
380	95
389	100
395	93
401	90
404	87
405	85
406	79

Ex_no.	Eff. %
2	98
3	95
15	98
168	92
199	99
226	99
282	100
342	100

Ex_no.	Eff. %
2	89
3	93
15	96
92	100
168	70
199	96
226	93
342	100

Ex_no.	Eff. %
2	100
3	100
15	100
168	100
199	100
226	90
282	90
342	100

Ex_no.	Eff. %
8	100
15	99
27	100
29	100
30	100
32	100
33	100
34	99
36	85
37	100
39	100
40	100
42	92
43	100
44	100
47	100
48	98
50	94
52	100
53	73
54	100
55	100
56	100
57	85
59	100
61	100
62	99
63	100
67	89
68	100
71	99
72	97
73	100
75	90
77	100
78	100
79	88
80	98
81	78
82	99
83	100
84	100
85	99
87	95
88	98
89	99
91	85
92	100
93	99
95	100
98	99
99	99
101	97
102	100
103	80
106	75
107	100
108	100
109	93
110	98
111	100
112	73
113	90
114	100
118	100
119	97
120	100
123	98
124	99
127	100
130	100
131	100
132	97
133	88
134	99
137	98
138	97
139	100
140	100
142	100
143	75
144	95
145	83
146	93
147	100
148	100
151	85
152	95
153	100
155	92
158	85
161	92
165	70
166	99
167	98
168	99
170	100
171	100
172	100
173	100
175	93
176	100
177	100
178	99
180	98
182	100
184	99
185	83
186	83
187	80
188	99
190	100
191	95
192	100
197	100
200	98
201	100
202	98
206	100
207	100
208	100
209	84
210	75
211	91
212	73
215	98
216	95
218	80
219	85
221	100
224	93
225	99
226	100
227	100
228	100
229	100
230	95
232	100
233	99
235	100
236	100
237	97
239	84
240	100
243	99
244	99
246	100
247	99
248	100
250	80
251	98
255	98
256	100
257	100
258	89
261	100
262	78
263	78
264	94
265	93
266	100
267	97
268	100
270	100
271	80
272	88
276	98
278	100
280	100
281	97
282	98
284	95
285	88
286	97
288	97
289	98
290	75
291	100
292	99
295	97
297	95
300	100
301	100
302	100
303	98
304	83
306	100
308	89
309	100
310	70
312	94
313	100
317	98
318	99
321	97
323	100
324	94
325	99
327	100
328	75
329	93
331	98
332	85
335	99
336	99
337	99
340	100
341	100
342	99
343	100
344	100
345	99
346	97
347	100
348	100
350	98
351	93
352	100
355	100
357	92
358	100
361	90
362	71
363	99
364	98
365	100
366	94
367	100
369	70
372	100
373	97
374	100
375	97
376	100
377	99
378	100
379	100
380	93
381	75
383	70
384	100
386	80
387	100
388	100
389	99
390	100
394	90
395	99
396	73
400	100
401	99
403	100
404	98
406	94
407	95

Ex_no.	Eff. %
35	71
36	86
67	80
83	73
180	83
211	84
278	78
332	71
354	71
373	85

Ex_no.	Eff. %
83	85
124	80
190	98
197	80
209	75
211	72
212	100

Ex_no.	Eff. %
39	81
43	75
62	71
83	75
99	71
111	72
113	79
140	73
171	82
185	75
190	83
197	89
206	91
212	100
216	71
228	70
258	93
276	89
280	83
295	70
400	94
406	79

Ex_no.	Eff. %
35	100
36	71
53	70
71	70
84	70
117	79
212	97
250	79
255	70
256	90
268	96
379	100

Ex_no.	Eff. %
30	86
43	91
57	79
67	90
71	88
77	71
83	93
108	71
111	100
117	90
130	86
151	92
158	80
172	86
173	73
190	100
197	96
207	79
212	100
223	80
248	86
250	96
255	88
270	86
308	100
330	83
341	70
384	70
406	79

Ex_no.	Eff. %
36	75
39	98
43	94
63	75
67	98
73	81
83	89
88	78
120	98
131	81
140	86
172	89
173	89
185	78
190	94
191	89
197	94
209	88
211	71
212	89
215	81
228	81
233	98
258	81
280	98
292	75
308	94
317	81
324	75
325	75
351	75
384	79
395	72
406	81

Ex_no.	Eff. %
34	100
39	83
111	70
209	70
212	70
262	83
308	90
364	92

description truncated at 500,000 characters

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Claims as granted

21 claims

Classifications

18 codes

IPC · International Patent Classification

Section A — Human necessities

A01N43/836
A01N43/82
A01N55/00

Section C — Chemistry; metallurgy

C07D413/12
C07D213/73
C07F7/08
C07F7/10
C07D413/14
C07D213/74
C07D277/40
C07D231/16
C07D277/48
C07D417/12
C07D271/07
C07D417/14
C07D213/75
C07D277/46
C07D231/38

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2.9 y

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Examiner

Matthew Coughlin

art unit 1626 · TC 1600

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Ex_no.	Eff. %
2	100
3	98
5	95
6	98
7	95
8	98
9	95
10	95
11	100
12	95
13	95
14	95
15	98
16	98
17	98
18	95
19	95
20	95
21	97
26	93
58	80
70	84
74	95
86	90
104	93
111	95
136	95
148	97
154	95
163	95
168	92
198	95
199	97
226	92
282	92
322	75
342	92
347	92
405	95

Ex_no.	Eff. %
2	97
3	100
5	88
6	100
7	96
8	99
9	94
10	96
11	98
12	94
13	93
14	96
15	97
16	94
17	94
18	100
19	97
20	94
21	100
37	80
39	97
44	98
50	95
51	91
54	93
59	98
68	90
74	94
80	98
85	73
92	93
95	100
100	74
102	91
104	100
111	100
116	93
120	84
136	75
140	85
148	100
152	70
163	96
166	95
167	86
168	100
173	86
180	95
195	95
198	100
199	100
206	81
208	91
226	100
228	93
233	78
240	80
244	86
245	93
248	85
281	97
282	96
284	79
291	77
292	90
295	89
296	74
302	92
307	98
312	95
316	84
317	91
318	93
321	82
325	84
327	95
336	91
340	79
342	100
343	95
344	93
347	100
352	79
355	75
364	100
365	98
376	93
378	95
380	95
389	100
395	93
401	90
404	87
405	85
406	79

Ex_no.	Eff. %
8	100
15	99
27	100
29	100
30	100
32	100
33	100
34	99
36	85
37	100
39	100
40	100
42	92
43	100
44	100
47	100
48	98
50	94
52	100
53	73
54	100
55	100
56	100
57	85
59	100
61	100
62	99
63	100
67	89
68	100
71	99
72	97
73	100
75	90
77	100
78	100
79	88
80	98
81	78
82	99
83	100
84	100
85	99
87	95
88	98
89	99
91	85
92	100
93	99
95	100
98	99
99	99
101	97
102	100
103	80
106	75
107	100
108	100
109	93
110	98
111	100
112	73
113	90
114	100
118	100
119	97
120	100
123	98
124	99
127	100
130	100
131	100
132	97
133	88
134	99
137	98
138	97
139	100
140	100
142	100
143	75
144	95
145	83
146	93
147	100
148	100
151	85
152	95
153	100
155	92
158	85
161	92
165	70
166	99
167	98
168	99
170	100
171	100
172	100
173	100
175	93
176	100
177	100
178	99
180	98
182	100
184	99
185	83
186	83
187	80
188	99
190	100
191	95
192	100
197	100
200	98
201	100
202	98
206	100
207	100
208	100
209	84
210	75
211	91
212	73
215	98
216	95
218	80
219	85
221	100
224	93
225	99
226	100
227	100
228	100
229	100
230	95
232	100
233	99
235	100
236	100
237	97
239	84
240	100
243	99
244	99
246	100
247	99
248	100
250	80
251	98
255	98
256	100
257	100
258	89
261	100
262	78
263	78
264	94
265	93
266	100
267	97
268	100
270	100
271	80
272	88
276	98
278	100
280	100
281	97
282	98
284	95
285	88
286	97
288	97
289	98
290	75
291	100
292	99
295	97
297	95
300	100
301	100
302	100
303	98
304	83
306	100
308	89
309	100
310	70
312	94
313	100
317	98
318	99
321	97
323	100
324	94
325	99
327	100
328	75
329	93
331	98
332	85
335	99
336	99
337	99
340	100
341	100
342	99
343	100
344	100
345	99
346	97
347	100
348	100
350	98
351	93
352	100
355	100
357	92
358	100
361	90
362	71
363	99
364	98
365	100
366	94
367	100
369	70
372	100
373	97
374	100
375	97
376	100
377	99
378	100
379	100
380	93
381	75
383	70
384	100
386	80
387	100
388	100
389	99
390	100
394	90
395	99
396	73
400	100
401	99
403	100
404	98
406	94
407	95

Ex_no.	Eff. %
39	81
43	75
62	71
83	75
99	71
111	72
113	79
140	73
171	82
185	75
190	83
197	89
206	91
212	100
216	71
228	70
258	93
276	89
280	83
295	70
400	94
406	79

Ex_no.	Eff. %
30	86
43	91
57	79
67	90
71	88
77	71
83	93
108	71
111	100
117	90
130	86
151	92
158	80
172	86
173	73
190	100
197	96
207	79
212	100
223	80
248	86
250	96
255	88
270	86
308	100
330	83
341	70
384	70
406	79

Ex_no.	Eff. %
36	75
39	98
43	94
63	75
67	98
73	81
83	89
88	78
120	98
131	81
140	86
172	89
173	89
185	78
190	94
191	89
197	94
209	88
211	71
212	89
215	81
228	81
233	98
258	81
280	98
292	75
308	94
317	81
324	75
325	75
351	75
384	79
395	72
406	81

Ex_no.	Eff. %
2	100
3	98
5	95
6	98
7	95
8	98
9	95
10	95
11	100
12	95
13	95
14	95
15	98
16	98
17	98
18	95
19	95
20	95
21	97
26	93
58	80
70	84
74	95
86	90
104	93
111	95
136	95
148	97
154	95
163	95
168	92
198	95
199	97
226	92
282	92
322	75
342	92
347	92
405	95

Ex_no.	Eff. %
2	97
3	100
5	88
6	100
7	96
8	99
9	94
10	96
11	98
12	94
13	93
14	96
15	97
16	94
17	94
18	100
19	97
20	94
21	100
37	80
39	97
44	98
50	95
51	91
54	93
59	98
68	90
74	94
80	98
85	73
92	93
95	100
100	74
102	91
104	100
111	100
116	93
120	84
136	75
140	85
148	100
152	70
163	96
166	95
167	86
168	100
173	86
180	95
195	95
198	100
199	100
206	81
208	91
226	100
228	93
233	78
240	80
244	86
245	93
248	85
281	97
282	96
284	79
291	77
292	90
295	89
296	74
302	92
307	98
312	95
316	84
317	91
318	93
321	82
325	84
327	95
336	91
340	79
342	100
343	95
344	93
347	100
352	79
355	75
364	100
365	98
376	93
378	95
380	95
389	100
395	93
401	90
404	87
405	85
406	79

Ex_no.	Eff. %
8	100
15	99
27	100
29	100
30	100
32	100
33	100
34	99
36	85
37	100
39	100
40	100
42	92
43	100
44	100
47	100
48	98
50	94
52	100
53	73
54	100
55	100
56	100
57	85
59	100
61	100
62	99
63	100
67	89
68	100
71	99
72	97
73	100
75	90
77	100
78	100
79	88
80	98
81	78
82	99
83	100
84	100
85	99
87	95
88	98
89	99
91	85
92	100
93	99
95	100
98	99
99	99
101	97
102	100
103	80
106	75
107	100
108	100
109	93
110	98
111	100
112	73
113	90
114	100
118	100
119	97
120	100
123	98
124	99
127	100
130	100
131	100
132	97
133	88
134	99
137	98
138	97
139	100
140	100
142	100
143	75
144	95
145	83
146	93
147	100
148	100
151	85
152	95
153	100
155	92
158	85
161	92
165	70
166	99
167	98
168	99
170	100
171	100
172	100
173	100
175	93
176	100
177	100
178	99
180	98
182	100
184	99
185	83
186	83
187	80
188	99
190	100
191	95
192	100
197	100
200	98
201	100
202	98
206	100
207	100
208	100
209	84
210	75
211	91
212	73
215	98
216	95
218	80
219	85
221	100
224	93
225	99
226	100
227	100
228	100
229	100
230	95
232	100
233	99
235	100
236	100
237	97
239	84
240	100
243	99
244	99
246	100
247	99
248	100
250	80
251	98
255	98
256	100
257	100
258	89
261	100
262	78
263	78
264	94
265	93
266	100
267	97
268	100
270	100
271	80
272	88
276	98
278	100
280	100
281	97
282	98
284	95
285	88
286	97
288	97
289	98
290	75
291	100
292	99
295	97
297	95
300	100
301	100
302	100
303	98
304	83
306	100
308	89
309	100
310	70
312	94
313	100
317	98
318	99
321	97
323	100
324	94
325	99
327	100
328	75
329	93
331	98
332	85
335	99
336	99
337	99
340	100
341	100
342	99
343	100
344	100
345	99
346	97
347	100
348	100
350	98
351	93
352	100
355	100
357	92
358	100
361	90
362	71
363	99
364	98
365	100
366	94
367	100
369	70
372	100
373	97
374	100
375	97
376	100
377	99
378	100
379	100
380	93
381	75
383	70
384	100
386	80
387	100
388	100
389	99
390	100
394	90
395	99
396	73
400	100
401	99
403	100
404	98
406	94
407	95

Ex_no.	Eff. %
39	81
43	75
62	71
83	75
99	71
111	72
113	79
140	73
171	82
185	75
190	83
197	89
206	91
212	100
216	71
228	70
258	93
276	89
280	83
295	70
400	94
406	79

Ex_no.	Eff. %
30	86
43	91
57	79
67	90
71	88
77	71
83	93
108	71
111	100
117	90
130	86
151	92
158	80
172	86
173	73
190	100
197	96
207	79
212	100
223	80
248	86
250	96
255	88
270	86
308	100
330	83
341	70
384	70
406	79

Ex_no.	Eff. %
36	75
39	98
43	94
63	75
67	98
73	81
83	89
88	78
120	98
131	81
140	86
172	89
173	89
185	78
190	94
191	89
197	94
209	88
211	71
212	89
215	81
228	81
233	98
258	81
280	98
292	75
308	94
317	81
324	75
325	75
351	75
384	79
395	72
406	81

Ex_no.	Eff. %
2	100
3	98
5	95
6	98
7	95
8	98
9	95
10	95
11	100
12	95
13	95
14	95
15	98
16	98
17	98
18	95
19	95
20	95
21	97
26	93
58	80
70	84
74	95
86	90
104	93
111	95
136	95
148	97
154	95
163	95
168	92
198	95
199	97
226	92
282	92
322	75
342	92
347	92
405	95

Ex_no.	Eff. %
2	97
3	100
5	88
6	100
7	96
8	99
9	94
10	96
11	98
12	94
13	93
14	96
15	97
16	94
17	94
18	100
19	97
20	94
21	100
37	80
39	97
44	98
50	95
51	91
54	93
59	98
68	90
74	94
80	98
85	73
92	93
95	100
100	74
102	91
104	100
111	100
116	93
120	84
136	75
140	85
148	100
152	70
163	96
166	95
167	86
168	100
173	86
180	95
195	95
198	100
199	100
206	81
208	91
226	100
228	93
233	78
240	80
244	86
245	93
248	85
281	97
282	96
284	79
291	77
292	90
295	89
296	74
302	92
307	98
312	95
316	84
317	91
318	93
321	82
325	84
327	95
336	91
340	79
342	100
343	95
344	93
347	100
352	79
355	75
364	100
365	98
376	93
378	95
380	95
389	100
395	93
401	90
404	87
405	85
406	79

Ex_no.	Eff. %
8	100
15	99
27	100
29	100
30	100
32	100
33	100
34	99
36	85
37	100
39	100
40	100
42	92
43	100
44	100
47	100
48	98
50	94
52	100
53	73
54	100
55	100
56	100
57	85
59	100
61	100
62	99
63	100
67	89
68	100
71	99
72	97
73	100
75	90
77	100
78	100
79	88
80	98
81	78
82	99
83	100
84	100
85	99
87	95
88	98
89	99
91	85
92	100
93	99
95	100
98	99
99	99
101	97
102	100
103	80
106	75
107	100
108	100
109	93
110	98
111	100
112	73
113	90
114	100
118	100
119	97
120	100
123	98
124	99
127	100
130	100
131	100
132	97
133	88
134	99
137	98
138	97
139	100
140	100
142	100
143	75
144	95
145	83
146	93
147	100
148	100
151	85
152	95
153	100
155	92
158	85
161	92
165	70
166	99
167	98
168	99
170	100
171	100
172	100
173	100
175	93
176	100
177	100
178	99
180	98
182	100
184	99
185	83
186	83
187	80
188	99
190	100
191	95
192	100
197	100
200	98
201	100
202	98
206	100
207	100
208	100
209	84
210	75
211	91
212	73
215	98
216	95
218	80
219	85
221	100
224	93
225	99
226	100
227	100
228	100
229	100
230	95
232	100
233	99
235	100
236	100
237	97
239	84
240	100
243	99
244	99
246	100
247	99
248	100
250	80
251	98
255	98
256	100
257	100
258	89
261	100
262	78
263	78
264	94
265	93
266	100
267	97
268	100
270	100
271	80
272	88
276	98
278	100
280	100
281	97
282	98
284	95
285	88
286	97
288	97
289	98
290	75
291	100
292	99
295	97
297	95
300	100
301	100
302	100
303	98
304	83
306	100
308	89
309	100
310	70
312	94
313	100
317	98
318	99
321	97
323	100
324	94
325	99
327	100
328	75
329	93
331	98
332	85
335	99
336	99
337	99
340	100
341	100
342	99
343	100
344	100
345	99
346	97
347	100
348	100
350	98
351	93
352	100
355	100
357	92
358	100
361	90
362	71
363	99
364	98
365	100
366	94
367	100
369	70
372	100
373	97
374	100
375	97
376	100
377	99
378	100
379	100
380	93
381	75
383	70
384	100
386	80
387	100
388	100
389	99
390	100
394	90
395	99
396	73
400	100
401	99
403	100
404	98
406	94
407	95

Ex_no.	Eff. %
39	81
43	75
62	71
83	75
99	71
111	72
113	79
140	73
171	82
185	75
190	83
197	89
206	91
212	100
216	71
228	70
258	93
276	89
280	83
295	70
400	94
406	79

Ex_no.	Eff. %
30	86
43	91
57	79
67	90
71	88
77	71
83	93
108	71
111	100
117	90
130	86
151	92
158	80
172	86
173	73
190	100
197	96
207	79
212	100
223	80
248	86
250	96
255	88
270	86
308	100
330	83
341	70
384	70
406	79

Ex_no.	Eff. %
36	75
39	98
43	94
63	75
67	98
73	81
83	89
88	78
120	98
131	81
140	86
172	89
173	89
185	78
190	94
191	89
197	94
209	88
211	71
212	89
215	81
228	81
233	98
258	81
280	98
292	75
308	94
317	81
324	75
325	75
351	75
384	79
395	72
406	81